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2,4-Dimethoxyphenol

2,4-Dimethoxyphenol Structure
2,4-Dimethoxyphenol structure
CAS No.
13330-65-9
Chemical Name:
2,4-Dimethoxyphenol
Synonyms
2,4-Dimethoxyphenol;Nimesulide Impurity 5;Phenol, 2,4-diMethoxy-
CBNumber:
CB5947522
Molecular Formula:
C8H10O3
Molecular Weight:
154.16
MDL Number:
MFCD00060637
MOL File:
13330-65-9.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:45
Product description Number Pack Size Price
2,4-Dimethoxyphenol D5629 1G $151
2,4-Dimethoxyphenol D480968 500mg $130
2,4-Dimethoxyphenol X9852 100g $1757
2,4-Dimethoxyphenol 95+% 074013 5g $320
2,4-Dimethoxyphenol FD139659 5G $350
More product size
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2,4-Dimethoxyphenol Properties

Melting point 28 °C
Boiling point 219-222.5 °C
Density 1.092 g/cm3(Temp: 25 °C)
storage temp. Sealed in dry,Room Temperature
pka 10.46±0.18(Predicted)
form powder to lump
color White to Orange to Green

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352-P321-P332+P313-P362-P264-P280-P305+P351+P338-P337+P313P
HS Code  2909500090
NFPA 704
0
2 0

2,4-Dimethoxyphenol price More Price(24)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical D5629 2,4-Dimethoxyphenol 13330-65-9 1G $151 2025-07-31 Buy
TRC D480968 2,4-Dimethoxyphenol 13330-65-9 500mg $130 2021-12-16 Buy
AK Scientific X9852 2,4-Dimethoxyphenol 13330-65-9 100g $1757 2021-12-16 Buy
Matrix Scientific 074013 2,4-Dimethoxyphenol 95+% 13330-65-9 5g $320 2021-12-16 Buy
Biosynth Carbosynth FD139659 2,4-Dimethoxyphenol 13330-65-9 5G $350 2021-12-16 Buy
Product number Packaging Price Buy
D5629 1G $151 Buy
D480968 500mg $130 Buy
X9852 100g $1757 Buy
074013 5g $320 Buy
FD139659 5G $350 Buy

2,4-Dimethoxyphenol Chemical Properties,Uses,Production

Synthesis Reference(s)

Synthesis, p. 1046, 1983 DOI: 10.1055/s-1983-30624

Synthesis

2,4-Dimethoxybenzaldehyde

613-45-6

2,4-Dimethoxyphenol

13330-65-9

General procedure for the synthesis of 2,4-dimethoxyphenol from 2,4-dimethoxybenzaldehyde: To 0.5 mL of formic acid was added slowly and dropwise a 50 mL methanol solution containing 2,4-dimethoxybenzaldehyde (5.0 g, 30 mmol) and 5 mL of 30% H2O2. The reaction mixture was stirred at room temperature for 20 hours. Upon completion of the reaction, about 45 mL of methanol was evaporated using a rotary evaporator. Subsequently, the remaining solution was subjected to liquid-liquid partitioning with dichloromethane and distilled water. The aqueous phase was further extracted with 3 x 50 mL of dichloromethane. The organic phases were combined, washed with 3 x 50 mL of distilled water, dried over anhydrous sodium sulfate, filtered and the organic solvent was evaporated. The crude product was purified by column chromatography (eluent: chloroform) to afford 2,4-dimethoxyphenol as a light yellow oil (4.33 g, 94% yield).The structure of 2,4-dimethoxyphenol was confirmed by the following characterization data: IR νmax (cm-1, KBr): 3443, 2997, 2939, 2835, 1610, 1512, 1461, 1433, 1374, 1299. 1433, 1374, 1299, 1263, 1228, 1202, 1151, 1116, 1033, 918, 830, 792.1H NMR (300.13 MHz, CDCl3) δ (ppm): 6.75 (d, J = 5.2 Hz), 6.42 (d, J = 1.7 Hz), 6.31 (dd, J = 5.2, 1.7 Hz), 3.79 (s, OCH3), 3.69 (s, OCH3) EIMS m/z (relative abundance): 156 (4, [M+2]+.), 155 (40, [M+2]+.) , 155 (40, [M+1]+.) , 154 (100, [M]+.) , 140 (4), 139 (58), 112 (4), 111 (90), 96 (22), 79 (10), 69 (10), 51 (20).

References

[1] European Journal of Medicinal Chemistry, 2013, vol. 69, p. 798 - 816
[2] Journal of Organic Chemistry, 1984, vol. 49, # 24, p. 4740 - 4741
[3] Organic Letters, 2012, vol. 14, # 11, p. 2806 - 2809
[4] Tetrahedron Letters, 1999, vol. 40, # 15, p. 3037 - 3040
[5] Journal of the Chemical Society, Perkin Transactions 1, 2000, # 5, p. 799 - 811

2,4-Dimethoxyphenol Preparation Products And Raw materials

Raw materials

2,4-Dimethoxyiodobenzene 2,4-Dimethoxybenzaldehyde Hydrogen peroxide Methanol Sulfuric acid

Preparation Products

METHOXYBENZOQUINONE

2,4-Dimethoxyphenol Suppliers

Global( 84)Suppliers
Supplier Tel Email Country ProdList Advantage
ATK CHEMICAL COMPANY LIMITED 		+undefined-21-51877795 ivan@atkchemical.com China 33024 60
Alchem Pharmtech,Inc. 		8485655694 sales@alchempharmtech.com United States 63687 58
CONIER CHEM AND PHARMA LIMITED 		+8618523575427 sales@conier.com China 49977 58
Hefei TNJ Chemical Industry Co.,Ltd. 		+86-0551-65418671 +8618949823763 sales@tnjchem.com China 34563 58
Dayang Chem (Hangzhou) Co.,Ltd. 		+86-0571-88938639 +8617705817739 info@dycnchem.com China 52846 58
CR Corporation Limited 		+8613062833949 fred.wen@crcorporation.cn China 8645 58
Changzhou Helios Biomedical Science and Technology Co.,LTD. 		+8618961213068 gaoxue@czhelios.com China 512 58
Hangzhou MolCore BioPharmatech Co.,Ltd. 		+86-057181025280; +8617767106207 sales@molcore.com China 49734 58
PT CHEM GROUP LIMITED 		+86-85511178; peter68@ptchemgroup.com China 35425 58
ZHEJIANG JIUZHOU CHEM CO., LTD 		+86-0576225566889 +86-13454675544 admin@jiuzhou-chem.com；jamie@jiuzhou-chem.com；alice@jiuzhou-chem.com China 12272 58
Supplier Advantage
ATK CHEMICAL COMPANY LIMITED 		60
Alchem Pharmtech,Inc. 		58
CONIER CHEM AND PHARMA LIMITED 		58
Hefei TNJ Chemical Industry Co.,Ltd. 		58
Dayang Chem (Hangzhou) Co.,Ltd. 		58
CR Corporation Limited 		58
Changzhou Helios Biomedical Science and Technology Co.,LTD. 		58
Hangzhou MolCore BioPharmatech Co.,Ltd. 		58
PT CHEM GROUP LIMITED 		58
ZHEJIANG JIUZHOU CHEM CO., LTD 		58

View Lastest Price from 2,4-Dimethoxyphenol manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2,4-Dimethoxyphenol pictures 2022-01-26 2,4-Dimethoxyphenol
13330-65-9
 US $0.00 / KG 1KG 98.5% 100 tons Honest Joy Holdings Limited

2,4-Dimethoxyphenol Spectrum

2,4-Dimethoxyphenol(13330-65-9)1HNMR

13330-65-9(2,4-Dimethoxyphenol)Related Search:

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2,4-Dimethoxyphenol Phenol, 2,4-diMethoxy- Nimesulide Impurity 5 13330-65-9