4,7-Dichloro-1,10-phenanthroline
- CAS No.
- 5394-23-0
- Chemical Name:
- 4,7-Dichloro-1,10-phenanthroline
- Synonyms
- NSC 626;4,7-dichloro;4,7-Dichloro-o-phenanthroline;4,7-Dichloro-1,10-phenthroline;4,7-Dichloro-1,1-phenanthroline;1,10-Phenanthroline,4,7-dichloro;4,7-Dichloro-1,10-phenanthroline;4,7-Dichloro-1,10-phenanthroline 97%;4,7-Dichloro-1,10-phenanthroline Hydrate;4,7-Dichloro-1,10-phenanthroline Hydrate >
- CBNumber:
- CB62102111
- Molecular Formula:
- C12H6Cl2N2
- Molecular Weight:
- 249.1
- MDL Number:
- MFCD00233882
- MOL File:
- 5394-23-0.mol
- MSDS File:
- SDS
- TDS File:
- TDS
| Product description | Number | Pack Size | Price |
| 4,7-Dichloro-1,10-phenanthroline 97% | 678015 | 250mg | $198 |
| 4,7-Dichloro-1,10-phenanthroline 97% | 678015 | 1g | $470 |
| 4,7-Dichloro-1,10-phenanthroline min. 98.0 % | D5690 | 200MG | $37 |
| 4,7-Dichloro-1,10-phenanthroline | D5690 | 1G | $129 |
| 4,7-Dichloro-1,10-phenanthroline Hydrate >98.0%(GC)(T) | D4421 | 200mg | $66 |
| More product size | |||
| Melting point | 243-247 °C |
|---|---|
| Boiling point | 395.9±37.0 °C(Predicted) |
| Density | 1.482±0.06 g/cm3(Predicted) |
| storage temp. | under inert gas (nitrogen or Argon) at 2-8°C |
| pka | 3.29±0.10(Predicted) |
| form | solid |
| color | white to tan |
| InChI | InChI=1S/C12H6Cl2N2/c13-9-3-5-15-11-7(9)1-2-8-10(14)4-6-16-12(8)11/h1-6H |
| InChIKey | GIEQBYJCGYHHSU-UHFFFAOYSA-N |
| SMILES | N1C2C(=CC=C3C=2N=CC=C3Cl)C(Cl)=CC=1 |
| UNSPSC Code | 12352300 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) | ![]() ![]() GHS05,GHS06 |
|---|---|
| Signal word | Danger |
| Hazard statements | H301-H315-H318-H335 |
| Precautionary statements | P261-P264-P280-P301+P310-P302+P352-P305+P351+P338 |
| target organs | Respiratory system |
| PPE | dust mask type N95 (US), Eyeshields, Faceshields, Gloves |
| Hazard Codes | Xn |
| Risk Statements | 22-37/38-41 |
| Safety Statements | 26-39 |
| RIDADR | UN 2811 6.1/PG 3 |
| WGK Germany | 3 |
| TSCA | No |
| HazardClass | 6.1 |
| HS Code | 29339900 |
| Storage Class | 6.1C - Combustible acute toxic Cat.3 toxic compounds or compounds which causing chronic effects |
| Hazard Classifications | Acute Tox. 3 Oral Eye Dam. 1 Skin Irrit. 2 STOT SE 3 |
| Limited Quantities | 5.0 kg (11 lbs) (solid) |
| Excepted Quantities | Max Inner Pack (30g or 30ml) and Max Outer Pack (1Kg or 1L) |
4,7-Dichloro-1,10-phenanthroline price More Price(55)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 678015 | 4,7-Dichloro-1,10-phenanthroline 97% | 5394-23-0 | 250mg | $198 | 2026-04-30 | Buy |
| Sigma-Aldrich | 678015 | 4,7-Dichloro-1,10-phenanthroline 97% | 5394-23-0 | 1g | $470 | 2026-04-30 | Buy |
| TCI Chemical | D5690 | 4,7-Dichloro-1,10-phenanthroline min. 98.0 % | 5394-23-0 | 200MG | $37 | 2026-04-30 | Buy |
| TCI Chemical | D5690 | 4,7-Dichloro-1,10-phenanthroline | 5394-23-0 | 1G | $129 | 2026-04-30 | Buy |
| TCI Chemical | D4421 | 4,7-Dichloro-1,10-phenanthroline Hydrate >98.0%(GC)(T) | 5394-23-0 | 200mg | $66 | 2021-12-16 | Buy |
4,7-Dichloro-1,10-phenanthroline Chemical Properties,Uses,Production
Application
1,10-phenanthroline can be used as an intermediate in fluorescent materials, mainly in the fields of life sciences and medicine, catalysis, and novel optoelectronic materials.
Synthesis
Take 4.16g (10mmol) of 1,2-bis-[(2,2-dimethyl-4,6-dioxo-1,3-dioxane-5-ylidenemethyl)amino]benzene in 300mL of p-phenylene ether reflux for 30min, the mixture was cooled down to room temperature, when added to cyclohexane there was a large amount of precipitate precipitation precipitation, filtration and washed out of the p-phenylene ether with cyclohexane, vacuum drying to obtain 32.43g of light yellow powder crude The product was dried under vacuum to give 32.43g of light yellow powder crude product with a yield of about 99%. This product does not need to be purified, and can be directly carried out the next step of the reaction. Take 2.1g (10mmol) 4,7-dioxo-1,10-o-phenanthroline, add to 60g (210mmo1) phosphorus trichloride, under the protection of nitrogen reaction for 30min, the reaction solution was poured into 400mL of ice-water mixture, adjusted to pH 7-8 with 10% NaOH, extracted with dichloromethane (100mLx3), the organic layer was combined, dried with anhydrous magnesium sulfate, rotary evaporation with column chromatography. Drying, rotary evaporation and column chromatography gave 1.74 g of white powder product 4,7-dichloro-1,10-phenanthroline in 70% yield.
4,7-Dichloro-1,10-phenanthroline Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai UCHEM Inc. | +862156762820 +86-13564624040 | sales@myuchem.com | China | 8741 | 58 |
| ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD | +86-13017695106 +86-13676922317 | jiuyitime@fdachem.com | China | 16512 | 58 |
| Springchem New Material Technology Co.,Limited | +86-021-62885108 +8613917661608 | info@spring-chem.com | China | 2068 | 57 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| AB PharmaTech,LLC | 323-480-4688 | sales@acrospharmatech.com | United States | 989 | 55 |
| Shenzhen Nexconn Pharmatechs Ltd | +86-755-89396905 +86-15013857715 | admin@nexconn.com | China | 10403 | 58 |
| BAYNOE CHEM CO.,LTD | +86-21-34783353 +8615000719740 | baynoe@baynoe.com | CHINA | 934 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49979 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29792 | 58 |
| Richest Group Ltd | 18017061086 | oled@richest-group.com | CHINA | 5600 | 58 |
View Lastest Price from 4,7-Dichloro-1,10-phenanthroline manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
![]() |
2026-06-05 | 4,7-Dichloro-1,10-phenanthroline
5394-23-0
|
$63.00-289.00 | 1g | 0.98 | 20 | Shanghai UCHEM Inc. | |
![]() |
2026-04-17 | 4,7-Dichloro-1,10-phenanthroline
5394-23-0
|
$2.20-8.80 | 1kg | 99%min | 100kg | ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD | |
![]() |
2020-01-08 | 4,7-Dichloro-1,10-phenanthroline
5394-23-0
|
1KG | 98%; 99% | 1kg;10kg; 25kg | Career Henan Chemical Co |
-

- 4,7-Dichloro-1,10-phenanthroline
5394-23-0
- $63.00-289.00
- 0.98
- Shanghai UCHEM Inc.
-

- 4,7-Dichloro-1,10-phenanthroline
5394-23-0
- $2.20-8.80
- 99%min
- ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
-

- 4,7-Dichloro-1,10-phenanthroline
5394-23-0
- $0.01
- 98%; 99%
- Career Henan Chemical Co
5394-23-0(4,7-Dichloro-1,10-phenanthroline)Related Search:
1of4






