ChemicalBook >> CAS DataBase List >>4,7-Dichloro-1,10-phenanthroline

4,7-Dichloro-1,10-phenanthroline

CAS No.
5394-23-0
Chemical Name:
4,7-Dichloro-1,10-phenanthroline
Synonyms
NSC 626;4,7-dichloro;4,7-Dichloro-o-phenanthroline;4,7-Dichloro-1,10-phenthroline;4,7-Dichloro-1,1-phenanthroline;1,10-Phenanthroline,4,7-dichloro;4,7-Dichloro-1,10-phenanthroline;4,7-Dichloro-1,10-phenanthroline 97%;4,7-Dichloro-1,10-phenanthroline Hydrate;4,7-Dichloro-1,10-phenanthroline Hydrate >
CBNumber:
CB62102111
Molecular Formula:
C12H6Cl2N2
Molecular Weight:
249.1
MDL Number:
MFCD00233882
MOL File:
5394-23-0.mol
MSDS File:
SDS
TDS File:
TDS
Last updated:2026-06-04 16:00:12
Product description Number Pack Size Price
4,7-Dichloro-1,10-phenanthroline 97% 678015 250mg $198
4,7-Dichloro-1,10-phenanthroline 97% 678015 1g $470
4,7-Dichloro-1,10-phenanthroline min. 98.0 % D5690 200MG $37
4,7-Dichloro-1,10-phenanthroline D5690 1G $129
4,7-Dichloro-1,10-phenanthroline Hydrate >98.0%(GC)(T) D4421 200mg $66
More product size

4,7-Dichloro-1,10-phenanthroline Properties

Melting point 243-247 °C
Boiling point 395.9±37.0 °C(Predicted)
Density 1.482±0.06 g/cm3(Predicted)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
pka 3.29±0.10(Predicted)
form solid
color white to tan
InChI InChI=1S/C12H6Cl2N2/c13-9-3-5-15-11-7(9)1-2-8-10(14)4-6-16-12(8)11/h1-6H
InChIKey GIEQBYJCGYHHSU-UHFFFAOYSA-N
SMILES N1C2C(=CC=C3C=2N=CC=C3Cl)C(Cl)=CC=1
UNSPSC Code 12352300
NACRES NA.22

SAFETY

Risk and Safety Statements

Symbol(GHS)  Corrosion (GHS05)Skull and Crossbones (GHS06)
GHS05,GHS06
Signal word  Danger
Hazard statements  H301-H315-H318-H335
Precautionary statements  P261-P264-P280-P301+P310-P302+P352-P305+P351+P338
target organs Respiratory system
PPE dust mask type N95 (US), Eyeshields, Faceshields, Gloves
Hazard Codes  Xn
Risk Statements  22-37/38-41
Safety Statements  26-39
RIDADR  UN 2811 6.1/PG 3
WGK Germany  3
TSCA  No
HazardClass  6.1
HS Code  29339900
Storage Class 6.1C - Combustible acute toxic Cat.3
toxic compounds or compounds which causing chronic effects
Hazard Classifications Acute Tox. 3 Oral
Eye Dam. 1
Skin Irrit. 2
STOT SE 3
Limited Quantities 5.0 kg (11 lbs) (solid)
Excepted Quantities Max Inner Pack (30g or 30ml) and Max Outer Pack (1Kg or 1L)

4,7-Dichloro-1,10-phenanthroline price More Price(55)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Sigma-Aldrich 678015 4,7-Dichloro-1,10-phenanthroline 97% 5394-23-0 250mg $198 2026-04-30 Buy
Sigma-Aldrich 678015 4,7-Dichloro-1,10-phenanthroline 97% 5394-23-0 1g $470 2026-04-30 Buy
TCI Chemical D5690 4,7-Dichloro-1,10-phenanthroline min. 98.0 % 5394-23-0 200MG $37 2026-04-30 Buy
TCI Chemical D5690 4,7-Dichloro-1,10-phenanthroline 5394-23-0 1G $129 2026-04-30 Buy
TCI Chemical D4421 4,7-Dichloro-1,10-phenanthroline Hydrate >98.0%(GC)(T) 5394-23-0 200mg $66 2021-12-16 Buy
Product number Packaging Price Buy
678015 250mg $198 Buy
678015 1g $470 Buy
D5690 200MG $37 Buy
D5690 1G $129 Buy
D4421 200mg $66 Buy

4,7-Dichloro-1,10-phenanthroline Chemical Properties,Uses,Production

Application

1,10-phenanthroline can be used as an intermediate in fluorescent materials, mainly in the fields of life sciences and medicine, catalysis, and novel optoelectronic materials.

Synthesis

Take 4.16g (10mmol) of 1,2-bis-[(2,2-dimethyl-4,6-dioxo-1,3-dioxane-5-ylidenemethyl)amino]benzene in 300mL of p-phenylene ether reflux for 30min, the mixture was cooled down to room temperature, when added to cyclohexane there was a large amount of precipitate precipitation precipitation, filtration and washed out of the p-phenylene ether with cyclohexane, vacuum drying to obtain 32.43g of light yellow powder crude The product was dried under vacuum to give 32.43g of light yellow powder crude product with a yield of about 99%. This product does not need to be purified, and can be directly carried out the next step of the reaction. Take 2.1g (10mmol) 4,7-dioxo-1,10-o-phenanthroline, add to 60g (210mmo1) phosphorus trichloride, under the protection of nitrogen reaction for 30min, the reaction solution was poured into 400mL of ice-water mixture, adjusted to pH 7-8 with 10% NaOH, extracted with dichloromethane (100mLx3), the organic layer was combined, dried with anhydrous magnesium sulfate, rotary evaporation with column chromatography. Drying, rotary evaporation and column chromatography gave 1.74 g of white powder product 4,7-dichloro-1,10-phenanthroline in 70% yield.

4,7-Dichloro-1,10-phenanthroline Preparation Products And Raw materials

Raw materials

Preparation Products

Global( 147)Suppliers
Supplier Tel Email Country ProdList Advantage
Shanghai UCHEM Inc.
+862156762820 +86-13564624040 sales@myuchem.com China 8741 58
ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
+86-13017695106 +86-13676922317 jiuyitime@fdachem.com China 16512 58
Springchem New Material Technology Co.,Limited
+86-021-62885108 +8613917661608 info@spring-chem.com China 2068 57
ATK CHEMICAL COMPANY LIMITED
+undefined-21-51877795 ivan@atkchemical.com China 33024 60
AB PharmaTech,LLC
323-480-4688 sales@acrospharmatech.com United States 989 55
Shenzhen Nexconn Pharmatechs Ltd
+86-755-89396905 +86-15013857715 admin@nexconn.com China 10403 58
BAYNOE CHEM CO.,LTD
+86-21-34783353 +8615000719740 baynoe@baynoe.com CHINA 934 58
CONIER CHEM AND PHARMA LIMITED
+8618523575427 sales@conier.com China 49979 58
career henan chemical co
+86-0371-86658258 +8613203830695 factory@coreychem.com China 29792 58
Richest Group Ltd
18017061086 oled@richest-group.com CHINA 5600 58

View Lastest Price from 4,7-Dichloro-1,10-phenanthroline manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4,7-Dichloro-1,10-phenanthroline pictures 2026-06-05 4,7-Dichloro-1,10-phenanthroline
5394-23-0
$63.00-289.00 1g 0.98 20 Shanghai UCHEM Inc.
4,7-Dichloro-1,10-phenanthroline pictures 2026-04-17 4,7-Dichloro-1,10-phenanthroline
5394-23-0
$2.20-8.80 1kg 99%min 100kg ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
4,7-Dichloro-1,10-phenanthroline pictures 2020-01-08 4,7-Dichloro-1,10-phenanthroline
5394-23-0
1KG 98%; 99% 1kg;10kg; 25kg Career Henan Chemical Co
4,7-Dichloro-1,10-phenanthroline 4,7-Dichloro-o-phenanthroline NSC 626 1,10-Phenanthroline,4,7-dichloro 4,7-Dichloro-1,10-phenanthroline Hydrate 4,7-Dichloro-1,10-phenanthroline 97% 4,7-Dichloro-1,10-phenthroline 4,7-Dichloro-1,10-phenanthroline Hydrate > 4,7-dichloro 4,7-Dichloro-1,1-phenanthroline 5394-23-0 C12H6Cl2N2xH2O Building Blocks Catalysis and Inorganic Chemistry Chemical Synthesis Halogenated Heterocycles Heterocyclic Building Blocks N-Containing Other Ligands N-ContainingChemical Synthesis Other LigandsHeterocyclic Building Blocks Catalysis and Inorganic Chemistry Halogenated Heterocycles Heterocyclic Building Blocks Others