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ChemicalBook >> CAS DataBase List >>2-Chloro-1,10-phenanthroline

2-Chloro-1,10-phenanthroline

2-Chloro-1,10-phenanthroline Structure
2-Chloro-1,10-phenanthroline structure
CAS No.
7089-68-1
Chemical Name:
2-Chloro-1,10-phenanthroline
Synonyms
VUF 7730;chlorophenanthroline;2-Chloro-1,10-phenan;2-Chloro-1,10-phenthroline;2-CHLORO-1,10-PHENANTHROLINE;1,10-Phenanthroline, 2-chloro-;2-Chloro-1,10-diazaphenanthrene;2-Chloro-1,10-phenanthroline >2-Chloro-1,10-phenanthroline Cas: 7089-68-1
CBNumber:
CB6483144
Molecular Formula:
C12H7ClN2
Molecular Weight:
214.65
MDL Number:
MFCD00185678
MOL File:
7089-68-1.mol
Last updated:2025-08-20 18:06:30
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2-Chloro-1,10-phenanthroline Properties

Melting point 130 °C
Boiling point 391.8±22.0 °C(Predicted)
Density 1.375
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
solubility soluble in Methanol
form powder to crystal
pka 4.22±0.10(Predicted)
color White to Yellow to Orange
InChI InChI=1S/C12H7ClN2/c13-10-6-5-9-4-3-8-2-1-7-14-11(8)12(9)15-10/h1-7H
InChIKey JHRMQHFRVPVGHL-UHFFFAOYSA-N
SMILES N1C2C(=CC=C3C=2N=CC=C3)C=CC=1Cl

SAFETY

Risk and Safety Statements

Symbol(GHS)  GHS hazard pictograms
GHS07
Signal word  Warning
Hazard statements  H302-H315-H319-H335
Precautionary statements  P261-P305+P351+P338
Safety Statements  24/25
HS Code  29339900

2-Chloro-1,10-phenanthroline price More Price(30)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical C1560 2-Chloro-1,10-phenanthroline >98.0%(HPLC)(T) 7089-68-1 1g $666 2025-07-31 Buy
TCI Chemical C1560 2-Chloro-1,10-phenanthroline >98.0%(HPLC)(T) 7089-68-1 100mg $171 2025-07-31 Buy
TRC B419493 2-Chloro-1,10-phenanthroline 7089-68-1 50mg $200 2021-12-16 Buy
TRC B419493 2-Chloro-1,10-phenanthroline 7089-68-1 100mg $310 2021-12-16 Buy
AK Scientific 0994AC 2-Chloro-1,10-phenanthroline 7089-68-1 5g $330 2021-12-16 Buy
Product number Packaging Price Buy
C1560 1g $666 Buy
C1560 100mg $171 Buy
B419493 50mg $200 Buy
B419493 100mg $310 Buy
0994AC 5g $330 Buy

2-Chloro-1,10-phenanthroline Chemical Properties,Uses,Production

Chemical Properties

Light yellow solid

Synthesis

1,10-Phenanthroline 1-oxide

1891-19-6

2-Chloro-1,10-phenanthroline

7089-68-1

General procedure for the synthesis of 2-chloro-1,10-phenanthroline from 1,10-phenanthroline 1-oxide: the procedure was similar to General Procedure I, with the difference that the reaction conditions were adjusted to be carried out at room temperature using 1,10-phenanthroline 1-oxide (1.00 eq.), POBr3 (3.00 eq.), and DMF (1.50 eq.) at a concentration of 0.2M. General procedure I (0013) for the bromination of acridazine N-oxide was carried out as follows: an appropriate amount of acridazine N-oxide was dissolved in anhydrous CH2Cl2 (0.1 M) at 0 °C, POBr3 (1.2 eq.) was added with stirring, followed by a slow, dropwise addition of DMF (0.5 eq.) under argon gas protection. The reaction mixture was gradually warmed to 25 °C with continuous stirring until TLC showed completion of the reaction. Upon completion of the reaction, the pH was adjusted to 7-8 by slow addition of saturated aqueous sodium carbonate solution. the mixture was separated and the aqueous phase was fully extracted with CH2Cl2. All organic phases were combined, washed with brine, dried over anhydrous Na2SO4, filtered and concentrated under reduced pressure to obtain the crude product. The crude product was purified by fast column chromatography with PE/EA (100:1) as eluent.

References

[1] Tetrahedron, 2016, vol. 72, # 38, p. 5762 - 5768
[2] Journal of Organic Chemistry, 2007, vol. 72, # 7, p. 2318 - 2328
[3] Chemistry - A European Journal, 2017, vol. 23, # 27, p. 6499 - 6503
[4] Journal of Organic Chemistry, 2017, vol. 82, # 8, p. 4203 - 4215

2-Chloro-1,10-phenanthroline Preparation Products And Raw materials

Raw materials

1,10-Phenanthrolin-2(1H)-one, 1-methyl- 1,10-Phenanthroline 1-oxide Dichloromethane trichlorophosphate N,N-Dimethylformamide

Preparation Products

2,9-Dichloro-1,10-phenanthroline

2-Chloro-1,10-phenanthroline Suppliers

Global( 174)Suppliers
Supplier Tel Email Country ProdList Advantage
Shanghai UCHEM Inc. 		+862156762820 +86-13564624040 sales@myuchem.com China 8318 58
Hebei Xinsheng New Material Technology Co., LTD. 		+86-16632316109 xinshengkeji@xsmaterial.com China 1085 58
ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD 		+86-13017695106 +86-13676922317 jiuyitime@fdachem.com China 8973 58
Springchem New Material Technology Co.,Limited 		+86-021-62885108 +8613917661608 info@spring-chem.com China 2068 57
Shanghai Daken Advanced Materials Co.,Ltd 		+86-2158073036 info@dakenam.com China 12933 58
Henan Tianfu Chemical Co.,Ltd. 		+86-0371-55170693 +86-19937530512 info@tianfuchem.com China 21622 55
ATK CHEMICAL COMPANY LIMITED 		+undefined-21-51877795 ivan@atkchemical.com China 33024 60
AB PharmaTech,LLC 		323-480-4688 sales@acrospharmatech.com United States 989 55
career henan chemical co 		+86-0371-86658258 +8613203830695 sales@coreychem.com China 29855 58
Zhengzhou HQ Material CO.,LTD. 		+86-371-55919009 +8615225108189 sale1@hqmat.com China 1001 58
Supplier Advantage
Shanghai UCHEM Inc. 		58
Hebei Xinsheng New Material Technology Co., LTD. 		58
ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD 		58
Springchem New Material Technology Co.,Limited 		57
Shanghai Daken Advanced Materials Co.,Ltd 		58
Henan Tianfu Chemical Co.,Ltd. 		55
ATK CHEMICAL COMPANY LIMITED 		60
AB PharmaTech,LLC 		55
career henan chemical co 		58
Zhengzhou HQ Material CO.,LTD. 		58

View Lastest Price from 2-Chloro-1,10-phenanthroline manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2-chloro-1,10-phenanthroline pictures 2025-09-09 2-chloro-1,10-phenanthroline
7089-68-1
 US $15.00-65.00 / g 5g 0.98 25kg Shanghai UCHEM Inc.
2-Chloro[1,10]phenanthroline pictures 2025-08-20 2-Chloro[1,10]phenanthroline
7089-68-1
 US $1.10-9.90 / KG 1KG 99%min 100KG ZHENGZHOU JIUYI TIME NEW MATERIALS CO,.LTD
2-Chloro-1,10-phenanthroline pictures 2025-04-04 2-Chloro-1,10-phenanthroline
7089-68-1
 US $0.00-0.00 / KG 1KG 98% 1ton Henan Aochuang Chemical Co.,Ltd.

2-Chloro-1,10-phenanthroline Spectrum

2-Chloro-1,10-phenanthroline(7089-68-1)1HNMR

7089-68-1(2-Chloro-1,10-phenanthroline)Related Search:

o-Phenanthroline 1,10-Phenanthroline hydrate 1,7-PHENANTHROLINE Difluorochloromethane 4-Chloro-1,10-phenanthroline
5-CHLORO-1,10-PHENANTHROLINE o-Phenanthroline monohydrochloride monohydrate 2,9-Dichloro-1,10-phenanthroline 2-Chloro-1,10-phenanthroline

1of2

chlorophenanthroline 2-CHLORO-1,10-PHENANTHROLINE 2-Chloro-1,10-diazaphenanthrene VUF 7730 2-Chloro-1,10-phenan 1,10-Phenanthroline, 2-chloro- 2-Chloro-1,10-phenthroline 2-Chloro-1,10-phenanthroline > 2-Chloro-1,10-phenanthroline Cas: 7089-68-1 7089-68-1