2'-Methyl[1,1'-biphenyl]-2-ol
![2'-Methyl[1,1'-biphenyl]-2-ol Structure](StructureFile/ChemBookStructure8/GIF/CB7117343.gif)
- CAS No.
- 77897-02-0
- Chemical Name:
- 2'-Methyl[1,1'-biphenyl]-2-ol
- Synonyms
- AKOS BAR-1256;2-Methyl-2'-hydroxybiphenyl;2'-Methyl[1,1'-biphenyl]-2-ol;[1,1'-Biphenyl]-2-ol, 2'-methyl-
- CBNumber:
- CB7117343
- Molecular Formula:
- C13H12O
- Molecular Weight:
- 184.23
- MDL Number:
- MFCD06802466
- MOL File:
- Mol file
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
2'-Methyl[1,1'-biphenyl]-2-ol price More Price(19)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS115723 | 2'-Methyl-[1,1'-biphenyl]-2-ol 95% | 77897-02-0 | 1g | $106 | 2026-06-04 | Buy |
| Activate Scientific | AS115723 | 2'-Methyl-[1,1'-biphenyl]-2-ol 95% | 77897-02-0 | 5g | $322 | 2026-06-04 | Buy |
| Matrix Scientific | 295171 | 2'-Methyl-[1,1'-biphenyl]-2-ol | 77897-02-0 | 250.00mg | $38 | 2026-05-19 | Buy |
| Matrix Scientific | 295171 | 2'-Methyl-[1,1'-biphenyl]-2-ol | 77897-02-0 | 1.00g | $78 | 2026-05-19 | Buy |
| Matrix Scientific | 295171 | 2'-Methyl-[1,1'-biphenyl]-2-ol | 77897-02-0 | 5.00g | $252 | 2026-05-19 | Buy |
2'-Methyl[1,1'-biphenyl]-2-ol Chemical Properties, Uses, Production
Synthesis
132-64-9
75-24-1
![2'-METHYL[1,1'-BIPHENYL]-2-OL](/StructureFile/ChemBookStructure8/GIF/CB7117343.gif)
77897-02-0
The general procedure for the synthesis of 2'-methyl-[1,1'-biphenyl]-2-ol from dibenzofuran and trimethylaluminum was as follows: to a 10 mL sample vial in a nitrogen-protected glove box, Ni(cod)2 (3.4 mg, 0.025 mmol), ICy-HBF4 (4.0 mg, 0.025 mmol), NaOtBu ( 48 mg, 0.50 mmol) and toluene (0.50 mL), followed by a Teflon-sealed screw cap. The mixture was stirred at room temperature for 3 minutes. Next, a toluene solution (0.50 mL) of aryl methyl ether (0.25 mmol) and AlMe3 (1.8 M toluene solution, 0.14 mL, 0.25 mmol) were added to the vial and resealed. The reaction mixture was stirred at 80 °C for 6 to 18 hours. After completion of the reaction, the mixture was cooled to room temperature and the crude product was treated with ethanol (EtOH). The reaction mixture was filtered through a silica gel pad and subsequently analyzed by GC. The filtrate was concentrated under vacuum and the residue obtained was purified by rapid column chromatography on silica gel.
References
[1] Chemistry Letters, 2015, vol. 44, # 12, p. 1729 - 1731
2'-Methyl[1,1'-biphenyl]-2-ol Preparation Products And Raw materials
Raw materials
1of2
Preparation Products
2'-Methyl[1,1'-biphenyl]-2-ol Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
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