3-BroMo-2,6-diMetylaniline
- CAS No.
- 53874-26-3
- Chemical Name:
- 3-BroMo-2,6-diMetylaniline
- Synonyms
- 3-BroMo-2,6-diMetylaniline;3-Bromo-2,6-dimethylaniline;3-bromo-2,6-dimethylbenzenamine;Benzenamine, 3-bromo-2,6-dimethyl-
- CBNumber:
- CB72705744
- Molecular Formula:
- C8H10BrN
- Molecular Weight:
- 200.08
- MDL Number:
- MFCD16658602
- MOL File:
- 53874-26-3.mol
- MSDS File:
- SDS
3-BroMo-2,6-diMetylaniline price More Price(32)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Matrix Scientific | 116350 | 3-Bromo-2,6-dimethylaniline | 53874-26-3 | 500.00mg | $544 | 2026-05-18 | Buy |
| Matrix Scientific | 116350 | 3-Bromo-2,6-dimethylaniline | 53874-26-3 | 1.00g | $730 | 2026-05-18 | Buy |
| Synthonix | B46732 | 3-Bromo-2,6-dimethylaniline 95+% | 53874-26-3 | 250mg | $63 | 2026-05-06 | Buy |
| Synthonix | B46732 | 3-Bromo-2,6-dimethylaniline 95+% | 53874-26-3 | 1g | $200 | 2026-05-06 | Buy |
| Synthonix | B46732 | 3-Bromo-2,6-dimethylaniline 95+% | 53874-26-3 | 5g | $730 | 2026-05-06 | Buy |
3-BroMo-2,6-diMetylaniline Chemical Properties, Uses, Production
Synthesis
39053-43-5
53874-26-3
General procedure for the synthesis of 3-bromo-2,6-dimethylaniline from 1-bromo-2,4-dimethyl-3-nitrobenzene: 1-bromo-2,4-dimethyl-3-nitrobenzene (2.66 g, 11.6 mmol) was dissolved in acetic acid (48 mL) under stirring conditions, followed by the addition of iron powder (2.58 g, 46.3 mmol). The reaction mixture was heated at 80 °C for 18 hours. After completion of the reaction, it was cooled to room temperature and filtered. The filtrate was concentrated to dryness under reduced pressure and the resulting residue was alkalized with aqueous sodium hydroxide and then extracted three times with ethyl acetate. The organic phases were combined and dried with anhydrous magnesium sulfate. The dried organic phase was concentrated to dryness under reduced pressure. The crude product was purified by fast column chromatography using a gradient elution of 0-30% ethyl acetate in hexane to afford the target product 3-bromo-2,6-dimethylaniline (1.28 g, 6.40 mmol, 55.3% yield).
References
[1] Journal of Medicinal Chemistry, 2018, vol. 61, # 16, p. 7202 - 7217
[2] Patent: WO2015/79251, 2015, A1. Location in patent: Paragraph 00215
[3] Patent: KR2015/124677, 2015, A. Location in patent: Paragraph 0334; 0339-0342
[4] Patent: WO2009/44311, 2009, A1. Location in patent: Page/Page column 39
3-BroMo-2,6-diMetylaniline Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Sichuan Yuehe Bio-Pharmaceutical Co.,Ltd | 028-82729560 17365561851 | tangzhichen@yuehepharm.com | China | 215 | 58 |
| Porse Fine Chemical Co.,LTD | 20-66003216 18666003216 | info@porsefinechemical.com | China | 1963 | 62 |
| Chengdu Firster Pharmaceutical Co., Ltd. | 028-87078428 028-87074958 | chengzhenyong@cdfirster.com | China | 2580 | 60 |
| Tianjin Anhao Biological Technology Co., Ltd. | sales@ahpharmatech.com | China | 5734 | 55 | |
| ShangHai Angti Biotechnology Co., Ltd. | 13764913901 | info@angtibio.com | China | 4975 | 55 |
| NanJing Xienuo bio Co.,Ltd. | 025-84112752 13805181430 | 154301870@qq.com | China | 999 | 55 |
| Zhengzhou Acme Chemical Co., Ltd. | 0371-0371-55629727 13323845623 | 2885676761@qq.com | China | 9957 | 58 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Capot Chemical Co.,Ltd. | +86-（0）57185586718 +86-13336195806 | sales@capot.com | China | 29626 | 60 |
| Aikon International Limited | 025-58859352 13913916777 | dt3@aikonchem.com | China | 15490 | 58 |
View Latest Price from 3-BroMo-2,6-diMetylaniline manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2020-01-13 | 3-BroMo-2,6-diMetylaniline
53874-26-3
|
$1.00 | 1g | 99.0% | 100kg | Career Henan Chemical Co |
-
- 3-BroMo-2,6-diMetylaniline
53874-26-3
- $1.00
- 99.0%
- Career Henan Chemical Co
