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ChemicalBook >> CAS DataBase List >>5-Methyl-6-nitrobenzo[d][1,3]dioxole

5-Methyl-6-nitrobenzo[d][1,3]dioxole

5-Methyl-6-nitrobenzo[d][1,3]dioxole Structure
5-Methyl-6-nitrobenzo[d][1,3]dioxole structure
CAS No.
32996-27-3
Chemical Name:
5-Methyl-6-nitrobenzo[d][1,3]dioxole
Synonyms
1,3-Benzodioxole, 5-methyl-6-nitro-;5-Methyl-6-nitrobenzo[d][1,3]dioxole
CBNumber:
CB82735922
Molecular Formula:
C8H7NO4
Molecular Weight:
181.15
MDL Number:
MFCD00229114
MOL File:
32996-27-3.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:46
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5-Methyl-6-nitrobenzo[d][1,3]dioxole Properties

Melting point 102-104 °C
Boiling point 289.8±39.0 °C(Predicted)
Density 1.407±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
Appearance Light yellow to yellow Solid

SAFETY

Risk and Safety Statements

HS Code  2932990090

5-Methyl-6-nitrobenzo[d][1,3]dioxole price

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Apolloscientific OR957738 5-Methyl-6-nitro-1,3-benzodioxole 95% 32996-27-3 250mg $150 2026-06-04 Buy
Apolloscientific OR957738 5-Methyl-6-nitro-1,3-benzodioxole 95% 32996-27-3 1g $252 2026-06-04 Buy
Matrix Scientific 155905 5-Methyl-6-nitro-1,3-benzodioxole 32996-27-3 1.00g $300 2026-05-18 Buy
aablocks AA00CN20 5-Methyl-6-Nitrobenzo[D][1,3]Dioxole 95% 32996-27-3 250mg $90 2026-05-28 Buy
aablocks AA00CN20 5-Methyl-6-Nitrobenzo[D][1,3]Dioxole 95% 32996-27-3 1g $116 2026-05-28 Buy
Product number Packaging Price Buy
OR957738 250mg $150 Buy
OR957738 1g $252 Buy
155905 1.00g $300 Buy
AA00CN20 250mg $90 Buy
AA00CN20 1g $116 Buy

5-Methyl-6-nitrobenzo[d][1,3]dioxole Chemical Properties, Uses, Production

Synthesis

5-METHYL-1,3-BENZODIOXOLE

7145-99-5

5-Methyl-6-nitrobenzo[d][1,3]dioxole

32996-27-3

Step A: 5-methyl-1,3-benzodioxole (8.00 g, 58.8 mmol) was dissolved in chloroform (160 mL) and stirred under ice bath cooling. 60% nitric acid (20 mL) was slowly added dropwise to the reaction system, and after dropping, stirring was continued for 30 minutes at room temperature. After completion of the reaction, the reaction mixture was diluted with dichloromethane, washed sequentially with water and saturated sodium bicarbonate solution, and dried over anhydrous potassium carbonate. The desiccant was removed by filtration and the filtrate was concentrated under reduced pressure to give a light yellow solid 5-methyl-6-nitrobenzo[d][1,3]dioxole (9.58 g, 90% yield).1H-NMR (300 MHz, CDCl3) δ: 2.55 (s, 3H), 6.08 (s, 2H), 6.70 (s, 1H), 7.50 (s, 1H).

References

[1] Patent: US2012/196824, 2012, A1
[2] Patent: US2003/87842, 2003, A1
[3] Patent: US2004/77554, 2004, A1
[4] Yakugaku Zasshi, 1933, vol. 53, p. 73,83, 118; dtsch. Ref. S. 11, 22
[5] Chem. Zentralbl., 1933, vol. 104, # I, p. 3201,3203

5-Methyl-6-nitrobenzo[d][1,3]dioxole Preparation Products And Raw materials

Raw materials

5-Methyl-1,3-benzodioxole Chloroform Nitric acid

Preparation Products

5-Methyl-6-nitrobenzo[d][1,3]dioxole Suppliers

Global Suppliers ( 22)
Supplier Tel Email Country ProdList Advantage
Cool Pharm, Ltd 021-60455363 18019463053 sales@coolpharm.com China 8455 58
Amadis Chemical Company Limited 571-89925085 sales@amadischem.com China 131885 58
Aikon International Limited 025-66061636 19370895928 qqyang@aikonchem.com China 15810 58
Shanghai ZiHao Pharmaceutical Co., Ltd. 021-13482410-12 13482410112; 362383684@qq.com China 751 58
Amel Pharmatech Corporation 027-888-4366503 13986279625 sales@amelpharmatech.com China 4826 58
Shanghai TenSus Biotechnology Co., Ltd. 021-50895067 18616507272;13681616114;15020344067 tensus@163.com China 8029 58
Fuxin Pharmaceutical +86-021-021-50872116 contact@fuxinpharm.com China 9976 58
Zhende Chemical Technology (Shanghai) Co., Ltd. 15601952568 sales4@myuchem.com China 2997 58
Zhengzhou convergence chemical co., LTD 037155153829 18003835034 3897192574@qq.com China 9982 58
Shanghai Haohong Pharmaceutical Co., Ltd. 400-8210725 4008210725 malulu@leyan.com China 39796 58
Supplier Advantage
Cool Pharm, Ltd 58
Amadis Chemical Company Limited 58
Aikon International Limited 58
Shanghai ZiHao Pharmaceutical Co., Ltd. 58
Amel Pharmatech Corporation 58
Shanghai TenSus Biotechnology Co., Ltd. 58
Fuxin Pharmaceutical 58
Zhende Chemical Technology (Shanghai) Co., Ltd. 58
Zhengzhou convergence chemical co., LTD 58
Shanghai Haohong Pharmaceutical Co., Ltd. 58

5-Methyl-6-nitrobenzo[d][1,3]dioxole Spectrum

5-Methyl-6-nitrobenzo[d][1,3]dioxole(32996-27-3)1HNMR

32996-27-3 (5-Methyl-6-nitrobenzo[d][1,3]dioxole) Related Search:

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5-Methyl-6-nitrobenzo[d][1,3]dioxole 1,3-Benzodioxole, 5-methyl-6-nitro- 32996-27-3