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2-Chloro-6-methyl-N-phenylbenzamide

2-Chloro-6-methyl-N-phenylbenzamide Structure
2-Chloro-6-methyl-N-phenylbenzamide structure
CAS No.
1386861-46-6
Chemical Name:
2-Chloro-6-methyl-N-phenylbenzamide
Synonyms
EOS-60720;Duvelisib RC1;2-Chloro-6-methyl-N-phenylbenzamide;Benzamide, 2-chloro-6-methyl-N-phenyl-;Dosulepin Impurity 5 (Dosulepin EP Impurity E);2-chloro-6-methyl-N-phenylbenzamide - [AC77793]
CBNumber:
CB93033280
Molecular Formula:
C14H12ClNO
Molecular Weight:
245.7
MDL Number:
MFCD25459278
MOL File:
1386861-46-6.mol
MSDS File:
SDS
Last updated:2025-07-24 18:13:50
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2-Chloro-6-methyl-N-phenylbenzamide Properties

Boiling point 317.8±35.0 °C(Predicted)
Density 1.250±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Store in freezer, under -20°C
pka 12.85±0.70(Predicted)
Appearance White to off-white Solid
InChI InChI=1S/C14H12ClNO/c1-10-6-5-9-12(15)13(10)14(17)16-11-7-3-2-4-8-11/h2-9H,1H3,(H,16,17)
InChIKey CPCKYTVKZDZSBA-UHFFFAOYSA-N
SMILES C(NC1=CC=CC=C1)(=O)C1=C(C)C=CC=C1Cl

2-Chloro-6-methyl-N-phenylbenzamide price More Price(16)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Synthonix AC77793 2-chloro-6-methyl-N-phenylbenzamide 95% 1386861-46-6 100mg $19 2026-05-06 Buy
Synthonix AC77793 2-chloro-6-methyl-N-phenylbenzamide 95% 1386861-46-6 500mg $29 2026-05-06 Buy
aablocks AA0018XA 2-Chloro-6-methyl-N-phenylbenzamide 98% 1386861-46-6 1g $11 2026-05-28 Buy
aablocks AA0018XA 2-Chloro-6-methyl-N-phenylbenzamide 98% 1386861-46-6 5g $32 2026-05-28 Buy
aablocks AA0018XA 2-Chloro-6-methyl-N-phenylbenzamide 98% 1386861-46-6 25g $104 2026-05-28 Buy
Product number Packaging Price Buy
AC77793 100mg $19 Buy
AC77793 500mg $29 Buy
AA0018XA 1g $11 Buy
AA0018XA 5g $32 Buy
AA0018XA 25g $104 Buy

2-Chloro-6-methyl-N-phenylbenzamide Chemical Properties, Uses, Production

Synthesis

Benzoyl chloride, 2-chloro-6-methyl- (9CI)

89894-44-0

Aniline

62-53-3

2-Chloro-6-methyl-N-phenylbenzamide

1386861-46-6

To a 250 mL round bottom flask was added 5.8 mL (63.76 mmol, 1.05 eq.) of a 150 mL solution of aniline in anhydrous dichloromethane, and 14.8 mL (106.26 mmol, 1.75 eq.) of triethylamine was slowly added at 0 °C and stirred for 30 min. Subsequently, 11.479 g (60.72 mmol, 1.0 eq.) of 2-chloro-6-methylbenzoyl chloride was added slowly dropwise, maintaining the reaction temperature at 0 °C and stirring the reaction for over 3 hours. Upon completion of the reaction, the mixture was washed sequentially with 1N HCl, water and aqueous sodium bicarbonate each. The organic layer was dried over anhydrous sodium sulfate and purified by recrystallization to give 13 g (52.91 mmol, 87% yield) of 2-chloro-6-methyl-N-phenylbenzamide as a white solid.

References

[1] Patent: KR2017/74381, 2017, A. Location in patent: Paragraph 0191; 0192; 0195; 0196
[2] Patent: KR2017/74380, 2017, A. Location in patent: Paragraph 0224; 0225; 0228; 0229
[3] Patent: WO2017/188720, 2017, A2. Location in patent: Paragraph 220
[4] Patent: US2018/105527, 2018, A1. Location in patent: Paragraph 0508-0510
[5] Patent: US2012/184568, 2012, A1. Location in patent: Page/Page column 79

2-Chloro-6-methyl-N-phenylbenzamide Preparation Products And Raw materials

Raw materials

Benzoyl chloride, 2-chloro-6-methyl- (9CI) Aniline Dichloromethane Triethylamine

Preparation Products

2-Chloro-6-methyl-N-phenylbenzamide Suppliers

Global Suppliers ( 55)
Supplier Tel Email Country ProdList Advantage
Suzhou Sino Rare Chemical Co., Ltd. 512-62857507 sales@sinorarechem.com China 1864 58
Energy Chemical 400-0056266 sales8178@energy-chemical.com China 44850 61
Haoyuan Chemexpress Co., Ltd. 021-58950125 info@chemexpress.com China 7545 61
Shanghai YuanQi Biotechnology Co., Ltd. +86-2332782371 +86-18120098618 sales@adobechem.com China 1250 50
AN PharmaTech Co Ltd 86(21)68097365 sales@anpharma.net China 4875 55
Shanghai Synchem Pharma Co., ltd 21-619849051-1 18521059765 synchempharma@aliyun.com China 4988 55
Chongqing Acemol Technology Co.,Ltd 023-86822659 18611316925 sales@acemol.com China 991 55
Artis Biotech Co. Ltd. 18108108965 18108108965 sales@artisbio.com China 2503 58
Shanghai Changyan Chem & Tech Co., Ltd. 021-20242659 18930833303 sales@changyanchem.cn China 4998 55
ShangHai Biochempartner Co.,Ltd 177-54423994 17754423994 2853530910@QQ.com China 8000 62
Supplier Advantage
Suzhou Sino Rare Chemical Co., Ltd. 58
Energy Chemical 61
Haoyuan Chemexpress Co., Ltd. 61
Shanghai YuanQi Biotechnology Co., Ltd. 50
AN PharmaTech Co Ltd 55
Shanghai Synchem Pharma Co., ltd 55
Chongqing Acemol Technology Co.,Ltd 55
Artis Biotech Co. Ltd. 58
Shanghai Changyan Chem & Tech Co., Ltd. 55
ShangHai Biochempartner Co.,Ltd 62

View Latest Price from 2-Chloro-6-methyl-N-phenylbenzamide manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
2-Chloro-6-methyl-N-phenylbenzamide pictures 2020-01-08 2-Chloro-6-methyl-N-phenylbenzamide
1386861-46-6
 $2.00 1g 98%MIN Career Henan Chemical Co

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2-Chloro-6-methyl-N-phenylbenzamide EOS-60720 Benzamide, 2-chloro-6-methyl-N-phenyl- Duvelisib RC1 Dosulepin Impurity 5 (Dosulepin EP Impurity E) 2-chloro-6-methyl-N-phenylbenzamide - [AC77793] 1386861-46-6