| | 586-96-9 Basic information More.. |
| Product Name: | Nitrosobenzene | | Synonyms: | Nitrosobenzene >=97%;NITROSOBENZENE;benzene,nitroso-;nitroso-benzen;nob;Nitrosobenzol;1-Nitrosobenzene;p-nitrosobenzene | | CAS: | 586-96-9 | | MF: | C6H5NO | | MW: | 107.11 | | EINECS: | 209-591-1 | | Mol File: | 586-96-9.mol |  |
Use
Steam distil nitrosobenzene, then crystallise it from a small volume of EtOH with cooling below 0o, dry it over CaCl2 in a dessicator at atmospheric pressure, and store it under N2 at 0o. Alternatively it can be distilled onto a cold finger cooled with brine at ~-10o in a vacuum at 17mm (water pump), while heating in a water bath at 65-70o [Robertson & Vaughan J Chem Educ 27 605 1950]. [Beilstein 5 IV 702.]
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586-96-9
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