| | 95-47-6 Basic information More.. |
| Product Name: | o-Xylene | | Synonyms: | 1,2-Xylene standard in Methanol;1，2-Xylene;1,2-DIMETHYLBENZENE;o-Xylene, 99%, Extra Dry, AcroSeal;AKOS BBS-00004266;XYLENES;XYLOL;O-XYLENE FOR SYNTHESIS | | CAS: | 95-47-6 | | MF: | C8H10 | | MW: | 106.17 | | EINECS: | 202-422-2 | | Mol File: | 95-47-6.mol |  |
Use
o-Xylene (4.4Kg) is sulfonated by stirring for 4hours with 2.5L of conc H2SO4 at 95o. After cooling, and separating the unsulfonated material, the product is diluted with 3L of water and neutralised with 40% NaOH. On cooling, sodium o-xylene sulfonate separates and is recrystallised from half its weight of water. [A further crop of crystals is obtained by concentrating the mother liquor to one-third of its volume.] The salt is dissolved in the minimum amount of cold water, then mixed with the same amount of cold water, and with the same volume of conc H2SO4 and heated to 110o. o-Xylene is regenerated and steam distils. The distillate is saturated with NaCl, the organic layer is separated, dried and redistilled. [Beilstein 5 H 362, 5 I 179, 5 II 281, 5 III 807, 5 IV 917.]
- o-Xylene
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- US $19.90 / kg
- 2025-06-24
- CAS:95-47-6
- Min. Order: 1kg
- Purity: 99%
- Supply Ability: 10 mt
- o-Xylene
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- US $9.00 / KG
- 2025-05-26
- CAS:95-47-6
- Min. Order: 1KG
- Purity: 99.9
- Supply Ability: 1 ton
- o-xylene
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- US $20.00-10.00 / kg
- 2024-05-11
- CAS:95-47-6
- Min. Order: 1kg
- Purity: 98%
- Supply Ability: 20
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95-47-6
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