2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole

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Company Name:	Springchem New Material Technology Co.,Limited
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Company Name:	Chembon Pharmaceutical Co., Ltd.
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Products Intro:	Product Name:2-(4-BroMo-phenyl)-1-phenyl-1H-benzoiMidazole CAS:2620-76-0 Purity:>98% Package:25g, 50g, 100g, 1kg

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2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole manufacturers

2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole Basic information

Product Name:	2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole
Synonyms:	2-(4-BROMO-PHENYL)-1-PHENYL-1H-BENZOIMIDAZOLE;2-(4-broMophenyl)-1-phenyl-1H-1,3-benzodiazole;2-(4-BroMophenyl)-1-phenylbenziMidazole;BIBA-A;1H-Benzimidazole,2-(4-bromophenyl)-1-phenyl-;2-(4-broMophenyl)-1-phenyl-1H-benzo[d]iMidazole;2-(4-BroMophenyl)-1-phenylbenzoiMidazole, 97%;2-(4-Bromophenyl)-1-phenylbenzimidazole >
CAS:	2620-76-0
MF:	C19H13BrN2
MW:	349.22
EINECS:	1533716-785-6
Product Categories:	OLED materials,pharm chemical,electronic;OLED
Mol File:	2620-76-0.mol

2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole Chemical Properties

Melting point	162-166℃
Boiling point	503.5±52.0 °C(Predicted)
density	1.38±0.1 g/cm3(Predicted)
storage temp.	Inert atmosphere,Room Temperature
form	Powder
pka	3.75±0.10(Predicted)
color	Off-white
λmax	297nm(CH3CN)(lit.)
InChI	InChI=1S/C19H13BrN2/c20-15-12-10-14(11-13-15)19-21-17-8-4-5-9-18(17)22(19)16-6-2-1-3-7-16/h1-13H
InChIKey	DXRLALXPCIOIDK-UHFFFAOYSA-N
SMILES	C1(C2=CC=C(Br)C=C2)N(C2=CC=CC=C2)C2=CC=CC=C2N=1
CAS DataBase Reference	2620-76-0

Safety Information

HS Code

2934999090

MSDS Information

2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole Usage And Synthesis

Uses	2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole is a useful research chemical.
Chemical Properties	White to yellow Crystal
Synthesis	359427-13-7 2620-76-0 General procedure for the synthesis of 1-phenyl-2-(4-bromophenyl)-1H-benzimidazole from the compound (CAS:359427-13-7): Example 1.3.2; 9; Synthesis of 2-(4-bromophenyl)-1-phenyl-1H-benzo[d]imidazole (9): amide 1 (9.6 g, 26 mmol) was suspended in anhydrous 1,4-dioxane (100 mL), and phosphorus oxychloride (POCl3) (9.2 mL, 100 mmol) was slowly added. Subsequently, the reaction mixture was heated at 100 °C overnight. After completion of the reaction, it was cooled to room temperature and the mixture was slowly poured into ice (200 g) under stirring. The precipitate was collected by filtration and recrystallized in dichloromethane (DCM)/hexane solvent mixture to give a light gray solid product (compound 9) (8.2 g, 90% yield).
References	[1] Advanced Functional Materials, 2010, vol. 20, # 3, p. 399 - 408 [2] Journal of Materials Chemistry, 2012, vol. 22, # 43, p. 23005 - 23011 [3] Journal of Materials Chemistry C, 2013, vol. 1, # 11, p. 2217 - 2223 [4] Patent: WO2011/8560, 2011, A1. Location in patent: Page/Page column 30 [5] Patent: WO2011/34967, 2011, A1. Location in patent: Page/Page column 22

2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole Preparation Products And Raw materials

Raw materials	4-Bromobenzoyl chloride-->4-Bromobenzaldehyde-->N-(2-Aminophenyl)-4-bromo-N-phenylbenzamide-->4-Bromo-N-(2-(phenylamino)phenyl)benzamide-->2-Aminodiphenylamine-->p-Toluenesulfonic acid-->1,4-Dioxane-->trichlorophosphate
Preparation Products	9-Phenyl-3-[4-(1-phenyl-1H-benzimidazol-2-yl)phenyl]-9H-carbazole

Tag:2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole(2620-76-0) Related Product Information

2-(4-bromophenyl)-4,6-diphenyl-1,3,5-triazine 2-(3'-BroMo-biphenyl-3-yl)-4,6-diphenyl-[1,3,5]triazine 2-(3-bromophenyl)-1-phenyl-1H-benzimidazole Phenylhydrazine Triphenylphosphine 2-Phenylbenzimidazole Benzimidazole (FORMYLMETHYLENE)TRIPHENYLPHOSPHORANE PHENYL VALERATE Triphenylmethyl Chloride 2-Phenylphenol Phenylacetone 1,2-Diphenyl-1H-benzimidazole 2-(4-BROMOPHENYL)BENZIMIDAZOLE 2-(4-BROMO-PHENYL)-1H-IMIDAZOLE 2-(4-Bromophenyl)-1-phenyl-1H-benzoimidazole Alkyl benzimidazole benzimidazolone

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