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DEUTERIUM CHLORIDE

DEUTERIUM CHLORIDE Suppliers list
Company Name: Peric Technology Co.,Ltd
Tel: +86-0310-7183483 +8615030098277
Email: jiake718@aliyun.com
Products Intro: Product Name:DEUTERIUM CHLORIDE
Purity:99.0%D,Purity≥98.0% Package:25G;100G;500G;1KG;5KG;25KG;123KG;
Company Name: career henan chemical co
Tel: +86-0371-86658258 +8613203830695
Email: sales@coreychem.com
Products Intro: Product Name:DEUTERIUM CHLORIDE
CAS:7698-05-7
Purity:99% Package:1kg;2USD
Company Name: CONIER CHEM AND PHARMA LIMITED
Tel: +8618523575427
Email: sales@conier.com
Products Intro: Product Name:DEUTERIUM CHLORIDE
CAS:7698-05-7
Purity:99% Package:1kg
Company Name: Richest Group Ltd
Tel: 18017061086
Email: oled@richest-group.com
Products Intro: Product Name:Deuteriumchloridesolution
CAS:7698-05-7
Purity:99%min Package:100g/bottle;500g/bottle;1kg/bottle;10kg/drum;50kg/drum;100kg/drum;380T/drum;
Company Name: Shanghai UCHEM Inc.
Tel: +862156762820 +86-13564624040
Email: sales@myuchem.com
Products Intro: Product Name:Deuterium chloride
CAS:7698-05-7
Purity:0.98 Package:25kg;1kg

DEUTERIUM CHLORIDE manufacturers

  • DEUTERIUM CHLORIDE
  • DEUTERIUM CHLORIDE pictures
  • $15.00 / 1KG
  • 2021-08-11
  • CAS:7698-05-7
  • Min. Order: 1KG
  • Purity: 99%+ HPLC
  • Supply Ability: Monthly supply of 1 ton
  • DEUTERIUM CHLORIDE
  • DEUTERIUM CHLORIDE pictures
  • $2.00 / 1kg
  • 2019-07-06
  • CAS:7698-05-7
  • Min. Order: 1 kg
  • Purity: 99%
  • Supply Ability: ask
DEUTERIUM CHLORIDE Basic information
Product Name:DEUTERIUM CHLORIDE
Synonyms:Deuterium chloride,for NMR,20 wt. % solutionin D2O, 99+ atom % D;Deuterium chloride,for NMR,20 wt. % solutionin D2O, 100.0 atom % D;Deuterium chloride,for NMR,1M solution in D2O, 99.8 atom% D;Deuterium chloride, 20% w/w in D2O, 99.5% (Isotopic);DEUTERIUM CHLORIDE, 99 ATOM % D;Hydrochloric acid-D 20 %;DEUTERIUM CHLORIDE, 1.0M SOLUTION IN DIETHYL ETHER;DEUTERIUM CHLORIDE, 35 WT. % SOLUTION IN D2O, 99 ATOM % D
CAS:7698-05-7
MF:ClD
MW:37.47
EINECS:231-715-8
Product Categories:
Mol File:7698-05-7.mol
DEUTERIUM CHLORIDE Structure
DEUTERIUM CHLORIDE Chemical Properties
Melting point −114 °C(lit.)
Boiling point −85 °C(lit.)
density 1.2
vapor density 1.3 (vs air)
vapor pressure 613 psi ( 21.1 °C)
refractive index n20/D 1.355
Fp −40 °F
solubility soluble in H2O
form Liquid
color Colorless to pale yellow
Water Solubility Fully miscible in water.
Sensitive Moisture Sensitive
Major Applicationpharmaceutical
InChIInChI=1S/ClH/h1H/i/hD
InChIKeyVEXZGXHMUGYJMC-DYCDLGHISA-N
SMILESCl[2H]
CAS DataBase Reference7698-05-7(CAS DataBase Reference)
CAS Number Unlabeled7647-01-0
Safety Information
Hazard Codes T,C,Xn,F,Xi,F+
Risk Statements 34-37-68-66-36/37/38-19-11-23-23/25-12-67-22-35
Safety Statements 26-36/37/39-45-46-36/37-16-23-9
RIDADR UN 2924 3/PG 1
WGK Germany 3
10
HazardClass 8
PackingGroup II
HS Code 28459000
Storage Class8A - Combustible corrosive hazardous materials
Hazard ClassificationsEye Dam. 1
Met. Corr. 1
Skin Corr. 1B
STOT SE 3
MSDS Information
ProviderLanguage
SigmaAldrich English
ACROS English
ALFA English
DEUTERIUM CHLORIDE Usage And Synthesis
Chemical Propertiesclear colorless solution
UsesDeuterium chloride solution has been used to study:
  • The kinetics of chitosan reacetylation using acetic anhydride and acetic acid.
  • Regioselective terminal group activation of chitosan by thioacetylation.
  • The complex formation between cyclodextrin and captopril in aqueous solution using NMR spectroscopy.

Synthesis

Step 1: Firstly, argon is passed to the reaction device, phosphorus trichloride is added to the reaction bottle, and then heavy water is added dropwise to form deuterohydrochloric acid solution, when the deuterohydrochloric acid solution in the reaction bottle is saturated, the deuterohydrochloric acid gas is overflowed into the primary heavy water absorption bottle.

Step 2: after saturation of the deuterohydrochloric acid in the first heavy water absorption bottle, the deuterohydrochloric acid gas overflowed into the second heavy water absorption bottle, after saturation of the deuterohydrochloric acid in the second heavy water absorption bottle, the deuterohydrochloric acid gas overflowed into the third heavy water absorption bottle.

Step 3: After the reaction of phosphorus trichloride is completed, ferric chloride is added to the reaction bottle at room temperature. Step 4: Deuterium gas is introduced into the reaction bottle, and the deuterium gas reduces the iron ions contained in the reaction bottle to iron monomers.

The present method provides a deuterated hydrochloric acid production process which effectively removes the phosphorus in the reaction bottle and improves the yield of deuterated hydrochloric acid.

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