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N,N'-Ethylenebis(stearamide)

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CAS:110-30-5
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CAS:110-30-5
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CAS:110-30-5
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CAS:110-30-5
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N,N'-Ethylenebis(stearamide) manufacturers

N,N'-Ethylenebis(stearamide) Basic information
Product Name:N,N'-Ethylenebis(stearamide)
Synonyms:N,N'-ETHYLENEBISSTEARAMIDE;N,N'-ETHYLENEBISOCTADECANAMIDE;1,2-bis(octadecanamido)ethane;abrilwax10ds;Glyco(R) Asphalt Modifier beads;Acrawax(R) C atomized;N, N` Distearoylethyelendiamine;Acrawax(R) C beads
CAS:110-30-5
MF:C38H76N2O2
MW:593.02
EINECS:203-755-6
Product Categories:Intermediates & Fine Chemicals;Isotope Labeled Compounds;Neurochemicals;Pharmaceuticals;Engineering Polymers;Polymer Science;Waxes and Oils
Mol File:110-30-5.mol
N,N'-Ethylenebis(stearamide) Structure
N,N'-Ethylenebis(stearamide) Chemical Properties
Melting point 144-146 °C(lit.)
Boiling point 646.41°C (rough estimate)
density 1 g/cm3 (20℃)
bulk density210kg/m3
vapor pressure 0.000023 Pa (20 °C)
refractive index 1.4670 (estimate)
Fp 280℃
storage temp. 2-8°C
solubility ketones, alcohols and aromatic solvents at their boiling points: soluble
form beads
pka15.53±0.46(Predicted)
AppearanceWhite to off-white Solid
Water Solubility 0ng/L at 25℃
Cosmetics Ingredients FunctionsVISCOSITY CONTROLLING
InChIKeyRKISUIUJZGSLEV-UHFFFAOYSA-N
LogP13.98 at 25℃
CAS DataBase Reference110-30-5(CAS DataBase Reference)
EPA Substance Registry SystemN,N'-Ethylenebis(stearamide) (110-30-5)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
WGK Germany 1
TSCA TSCA listed
HS Code 29242990
Hazardous Substances Data110-30-5(Hazardous Substances Data)
ToxicityLD50 orally in Rabbit: > 20000 mg/kg
MSDS Information
ProviderLanguage
N,N'-Ethylenebis(stearamide) English
SigmaAldrich English
N,N'-Ethylenebis(stearamide) Usage And Synthesis
Chemical PropertiesOily Liquid
UsesN,N'-Ethylenebis(stearamide) is a bis-amide polymer additive that lowers the temperature at which the asphalt softens. It is used as processing aid for resins and polymers and as defoaming agent. It is traditionally used as lubricant and binder for cold compaction of powdered metal parts.
UsesGlyco Asphalt Modifier is a bis-amide polymer additive that lowers the temperature at which the asphalt softens.
UsesAcrawax(R) C is used as processing aid for resins and polymers and as defoaming agent. Acrawax(R) C atomized is traditionally used as lubricant and binder for cold compaction of powdered metal parts.
UsesAcrawax(R) C is used as a processing aid for resins and polymers and as a defoaming agent. Acrawax(R) C beaded is an effective lubricant, processing aid, slip additive and pigment dispersant aid for most polymers.
UsesGlycowax(R) 765 is an ethylenebisstearamide, specifically developed to afford low, consistent viscosities and superior cost performance in paper pulp defoamer applications. Useful as defoamer for paper making and textile processing . Product Data Sheet
General DescriptionN,N′-Ethylenebis(stearamide) (EBS) is a synthetic wax that has fatty amide groups that can interact with the surface of a variety of nanoparticles. It can be used for a wide range of applications such as lubricants, activators and dispersing agents that reduce the friction in the system and increase the rate of processing.
Synthesis
Ethylenediamine

107-15-3

Stearic acid

57-11-4

N,N'-Ethylenebis(stearamide)

110-30-5

General procedure: stearic acid with 0.28% of a complex antioxidant (mass ratio of antioxidant 1076, antioxidant DLTDP to antioxidant T501 is 0.20: 0.36: 1) was added to a reactor and stirred for 10 minutes under N2 atmosphere. Subsequently, the mixture was slowly heated to 100 °C until the stearic acid was completely melted. Next, a composite catalyst consisting of 0.20% by weight of the total weight of ethylenediamine and stearic acid (the mass ratio of p-toluenesulfonic acid/SAPO-34-loaded solid acid catalyst to phosphoric acid/SiO2-Al2O3-loaded solid acid catalyst was 1:3.5) was added. The reaction was kept at a constant temperature for 2 hours. After that, the temperature was slowly increased to 180 °C, and the constant temperature reaction was continued for 4 h for dehydration reaction, and the water produced during the reaction was carried out by N2. After completion of the reaction, the heating was stopped and the material was discharged after cooling to 160°C. The molar ratio of stearic acid to ethylenediamine was 1: 0.58. The yield of N,N'-ethylene bis-stearamide was obtained by the above steps.

Toxics Screening LevelThe initial threshold screening level (ITSL) for N,N'-ethylene bis-octadecanamide is 0.1 μg/m3 (annual averaging time).
References[1] Patent: CN105777568, 2016, A. Location in patent: Paragraph 0024; 0025
[2] Industrial and Engineering Chemistry, 1948, vol. 40, p. 1365
[3] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1976, p. 386 - 389
[4] Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983, p. 2197 - 2200
[5] Patent: CN105348128, 2016, A. Location in patent: Paragraph 0015
N,N'-Ethylenebis(stearamide) Preparation Products And Raw materials
Raw materialsEthylenediamine-->Stearic acid
Preparation Productsdefoaming agent OTD
Tag:N,N'-Ethylenebis(stearamide)(110-30-5) Related Product Information
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