- 6-Cyanoindole
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- $10.00 / 1KG
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2026-03-20
- CAS:15861-36-6
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: 10 mt
- 6-Cyanoindole
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- $100.00 / 1kg
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2023-08-08
- CAS:15861-36-6
- Min. Order: 1kg
- Purity: 99%
- Supply Ability: 1000tons
- 6-Cyanoindole
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- $0.00 / 1KG
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2022-02-09
- CAS:15861-36-6
- Min. Order: 1KG
- Purity: 98.8%
- Supply Ability: 100 tons
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| | 6-Cyanoindole Basic information |
| | 6-Cyanoindole Chemical Properties |
| Melting point | 130-132°C | | Boiling point | 350.0±15.0 °C(Predicted) | | density | 1.24±0.1 g/cm3(Predicted) | | storage temp. | Keep in dark place,Inert atmosphere,Room temperature | | solubility | Dichloromethane, Methanol | | form | Solid | | pka | 15.17±0.30(Predicted) | | color | Off-White Crystalline | | Sensitive | Air & Light Sensitive | | BRN | 116502 | | InChI | InChI=1S/C9H6N2/c10-6-7-1-2-8-3-4-11-9(8)5-7/h1-5,11H | | InChIKey | SZSZDBFJCQKTRG-UHFFFAOYSA-N | | SMILES | N1C2=C(C=CC(C#N)=C2)C=C1 | | CAS DataBase Reference | 15861-36-6(CAS DataBase Reference) |
| Provider | Language |
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ALFA
| English |
| | 6-Cyanoindole Usage And Synthesis |
| Chemical Properties | Off-White Crystalline Solid | | Uses | 6-Cyanoindole (cas# 15861-36-6) is a compound useful in organic synthesis. | | Synthesis | To a stirred solution of 4-methyl-3-nitrobenzonitrile (16.58 g, 102.3 mmol) in 55 mL of N,N-dimethylformamide (DMF) was added N,N-dimethylacetamide (15.24 g, 128.1 mmol). The reaction mixture turned dark red and was subsequently stirred at 110 °C for 3 hours. After completion of the reaction, the solvent was removed under reduced pressure and the residue was dissolved in a mixture of 300 mL of ethanol and 300 mL of acetic acid. The reaction mixture was heated to 60 °C and iron powder (33 g, 594 mmol) was added in batches. The reaction mixture was refluxed for 2 h. After the reaction was completed, it was filtered through a Hyflo pad. Ether was added to the filtrate and the acidic layer was extracted with ether (1×). The ether layers were combined and concentrated in vacuum. The residue was purified by silica gel column chromatography using dichloromethane as eluent to give 7.02 g (48% yield) of 6-cyanoindaha solid. | | References | [1] Patent: US2006/122189, 2006, A1. Location in patent: Page/Page column 20 |
| | 6-Cyanoindole Preparation Products And Raw materials |
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