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2-METHYLNICOTINALDEHYDE

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Company Name: Hefei Lbao Physical & Chemical Science Co.,Ltd
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Products Intro: Product Name:2-Methylnicotinaldehyde
CAS:60032-57-7
Purity:98% Package:1kg;
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Products Intro: Product Name:2-Methylnicotinaldehyde
CAS:60032-57-7
Purity:98%(Min,HPLC) Package:100g;1kg;5kg,10kg,25kg,50kg
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Products Intro: Product Name:2-Methylnicotinaldehyde
CAS:60032-57-7
Purity:97+% Package:1g;10g;100g;;1kg Remarks:Z-12573
Company Name: CONIER CHEM AND PHARMA LIMITED
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Products Intro: Product Name:2-METHYLPYRIDINE-3-CARBALDEHYDE
CAS:60032-57-7
Purity:99% Package:1kg
Company Name: career henan chemical co
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Products Intro: Product Name:2-METHYLNICOTINALDEHYDE
CAS:60032-57-7
Purity:98%min Package:1KG;5.5USD

2-METHYLNICOTINALDEHYDE manufacturers

  • 2-METHYLNICOTINALDEHYDE
  • 2-METHYLNICOTINALDEHYDE pictures
  • $1.10 / 1g
  • 2025-11-18
  • CAS:60032-57-7
  • Min. Order: 1g
  • Purity: 99.00%
  • Supply Ability: 100 Tons min
  • 2-METHYLNICOTINALDEHYDE
  • 2-METHYLNICOTINALDEHYDE pictures
  • $5.50 / 1KG
  • 2020-01-13
  • CAS:60032-57-7
  • Min. Order: 1KG
  • Purity: 98%min
  • Supply Ability: 1kg-100kg
2-METHYLNICOTINALDEHYDE Basic information
Uses
Product Name:2-METHYLNICOTINALDEHYDE
Synonyms:2-Methylpyridine-3-carboxaldehyde;2-Methylpyridine-3-carbox...;3-Pyridinecarboxaldehyde, 2-Methyl-;2-Methyl-3-Pyridinecarboxaldehyde;2-METHYLNICOTINALDEHYDE;2-Methylpyridine-3-carbaldehyde;2-METHYLNICOTINALDEHYDE ISO 9001:2015 REACH
CAS:60032-57-7
MF:C7H7NO
MW:121.14
EINECS:
Product Categories:Pyridines
Mol File:60032-57-7.mol
2-METHYLNICOTINALDEHYDE Structure
2-METHYLNICOTINALDEHYDE Chemical Properties
Melting point 242 °C (decomp)
Boiling point 94 °C(Press: 12 Torr)
density 1.106 g/mL at 25 °C
refractive index n20/D1.549
Fp 93℃
storage temp. 2-8°C, stored under nitrogen
pka4.15±0.10(Predicted)
form liquid
color Pale yellow
InChI1S/C7H7NO/c1-6-7(5-9)3-2-4-8-6/h2-5H,1H3
InChIKeyJHRPHASLIZOEBJ-UHFFFAOYSA-N
SMILESCc1ncccc1C=O
Safety Information
Hazard Codes Xn
Risk Statements 22-37/38-41
Safety Statements 26-39
WGK Germany 3
HS Code 2933399990
Storage Class10 - Combustible liquids
Hazard ClassificationsAcute Tox. 4 Oral
Eye Dam. 1
Skin Irrit. 2
STOT SE 3
MSDS Information
2-METHYLNICOTINALDEHYDE Usage And Synthesis
Uses2-Methylnicotinaldehyde is a useful research chemical.
Synthesis
(2-METHYL-PYRIDIN-3-YL)-METHANOL

56826-61-0

2-METHYLNICOTINALDEHYDE

60032-57-7

General procedure for the synthesis of 2-methylpyridine-3-carbaldehyde from 2-methylpyridine-3-methanol: A mixture of 3-hydroxymethyl-2-methylpyridine (9.0 g, 73.1 mmol) and manganese(IV) dioxide (28.1 g, 322 mmol) in dichloromethane (100 mL) was heated and refluxed for 48 hours. Upon completion of the reaction, the insoluble material was removed by diatomaceous earth filtration and the filter cake was washed with a solvent mixture of methanol/dichloromethane. Subsequently, the solvent in the filtrate was removed by rotary evaporator to give 2-methylpyridine-3-carboxaldehyde (7.5 g, 85% yield) as an oily product. Its nuclear magnetic resonance hydrogen spectrum (NMR) data were as follows: δ 2.78 (s, 3H), 7.43 (dd, 1H), 8.15 (dd, 1H), 8.66 (dd, 1H).

References[1] Patent: WO2006/106307, 2006, A1. Location in patent: Page/Page column 91
[2] Patent: WO2006/100461, 2006, A1. Location in patent: Page/Page column 83
[3] Chemical and Pharmaceutical Bulletin, 1994, vol. 42, # 9, p. 1841 - 1849
[4] Patent: WO2013/19682, 2013, A1. Location in patent: Page/Page column 101
[5] Patent: WO2013/19626, 2013, A1. Location in patent: Page/Page column 27
2-METHYLNICOTINALDEHYDE Preparation Products And Raw materials
Raw materialsN,N-Dimethylformamide-->(2-METHYL-PYRIDIN-3-YL)-METHANOL-->3-Bromo-2-methylpyridine-->Manganese dioxide-->Dichloromethane
Tag:2-METHYLNICOTINALDEHYDE(60032-57-7) Related Product Information
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