2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone

2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone Basic information
Product Name:2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone
Synonyms:2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone;Ethanone, 2,2-dichloro-2-fluoro-1-(4-methoxyphenyl)-
CAS:16629-88-2
MF:C9H7Cl2FO2
MW:237.06
EINECS:
Product Categories:
Mol File:16629-88-2.mol
2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone Structure
2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone Chemical Properties
Boiling point 110-112 °C(Press: 2 Torr)
density 1.368±0.06 g/cm3(Predicted)
Safety Information
MSDS Information
2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone Usage And Synthesis
PreparationTo acetonitrile was added periodic acid and this mixture was stirred at r.t. for 15 min. Dichlorofluoromethyl 4-methoxyphenyl alcohol was added followed by addition of pyridinium chlorochromate in acetonitrile, then the reaction mixture was stirred at 0°, for 10 min and at r.t. for 2.5 h (62%). Also obtained by reaction of sodium fluorodichloroacetate with p-anisole mag-nesium bromide in ethyl ether.
2,2-Dichloro-2-fluoro-1-(4-methoxyphenyl)ethanone Preparation Products And Raw materials
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