4-aminonaphthalene-1,6-disulfonic acid

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4-aminonaphthalene-1,6-disulfonic acid Basic information
Product Name:4-aminonaphthalene-1,6-disulfonic acid
Synonyms:1-naphthylamine-4,7-disulfonic acid;4-aminonaphthalene-1,6-disulfonic acid;4-azanylnaphthalene-1,6-disulfonic acid;4-aminonaphthalene-1,6-disulphonic acid;4-Amino-1,6-naphthalenedisulfonic acid;Dahl's acid III;1,6-Naphthalenedisulfonic acid, 4-amino-
CAS:85-75-6
MF:C10H9NO6S2
MW:303.31
EINECS:201-630-0
Product Categories:
Mol File:85-75-6.mol
4-aminonaphthalene-1,6-disulfonic acid Structure
4-aminonaphthalene-1,6-disulfonic acid Chemical Properties
Boiling point 205.8°C (rough estimate)
density 1.6329 (rough estimate)
refractive index 1.7330 (estimate)
EPA Substance Registry System1,6-Naphthalenedisulfonic acid, 4-amino- (85-75-6)
Safety Information
RIDADR 1759
TSCA TSCA listed
HazardClass 8
PackingGroup III
MSDS Information
4-aminonaphthalene-1,6-disulfonic acid Usage And Synthesis
Description1-Aminonaphthalene-4,7-disulfonic acid [85-75-6]. (4-aminonaphthalene-1,6-disulfonic acid), Dahl’s acid III, C10H9NO6S2, Mr 303.3, and its sodium salt are readily soluble in water, but the calcium and barium salts are only sparingly soluble. Conversion to 1-hydroxynaphthalene-4,7-disulfonic acid is achieved by reverse-Bucherer reaction or diazotization and hydrolysis. Sulfonation (35 % oleum, 90℃) yields 1-aminonaphthalene-2,4,7-trisulfonic acid.
Production MethodsAlthough separation of 4-aminonaphthalene-1,6-disulfonic acid from the mixture obtained by sulfonation of naphthionic acid is not practicable on a large scale, the 1,4,7-isomer can be obtained directly in high yield by sulfonation of 1-aminonaphthalene-7-sulfonic acid with oleum.
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