DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II)

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CAS:52611-08-2
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CAS:52611-08-2
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CAS:52611-08-2
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CAS:52611-08-2
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Products Intro: Product Name:Dichlorobis(methyldiphenylphosphine)palladium(II)
CAS:52611-08-2
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DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II) Basic information
Product Name:DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II)
Synonyms:Nsc148042;Dichlorobis[methylene-bis(diphenylphosphine)]dipalladium(II);Bis(methyldiphenylphosphine)palladium(II) Dichloride (cis- and trans- mixture);Bis(methyldiphenylphosphin;BIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II) DICHLORIDE;DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II);Bis(methyldiphenylphosphine)palladium(II) Dichloride >;Palladium,dichlorobis(methyldiphenylphosphine)-
CAS:52611-08-2
MF:C26H26Cl2P2Pd
MW:577.76
EINECS:
Product Categories:Catalysis and Inorganic Chemistry;Homogeneous Pd Catalysts;Palladium;Synthetic Organic Chemistry;Transition Metal Compounds;Catalysts for Organic Synthesis;Classes of Metal Compounds;Homogeneous Catalysts;Metal Complexes;Pd (Palladium) Compounds
Mol File:52611-08-2.mol
DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II) Structure
DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II) Chemical Properties
Melting point >120*C (dec.)
storage temp. under inert gas (nitrogen or Argon) at 2-8°C
solubility Chloroform (Slightly, Heated), DMSO (Slightly, Heated), Methanol (Slightly, Heat
form Solid
color Light Yellow to Yellow
InChI1S/2C13H13P.2ClH.Pd/c2*1-14(12-8-4-2-5-9-12)13-10-6-3-7-11-13;;;/h2*2-11H,1H3;2*1H;/q;;;;+2/p-2
InChIKeyGTSFBKGHQLDFHU-UHFFFAOYSA-L
SMILESCl[Pd]Cl.CP(c1ccccc1)c2ccccc2.CP(c3ccccc3)c4ccccc4
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-36
WGK Germany 3
HS Code 2931.90.6000
Storage Class11 - Combustible Solids
Hazard ClassificationsEye Irrit. 2
Skin Irrit. 2
STOT SE 3
MSDS Information
ProviderLanguage
SigmaAldrich English
DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II) Usage And Synthesis
UsesCatalyst for:
  • Ullmann reactions (homocoupling reactions)
  • Cross coupling reaction of tributyltin hydride with aryl iodides
  • Double silylation, double carbonylation and cyclocarbonylation reactions
ApplicationDichlorobis(methyldiphenylphosphine)palladium(II) is a catalyst for the dicarbonylation of aryl halides with amines.
PreparationDichlorobis(methyldiphenylphosphine)palladium(II) is prepared by treating commercially available K2PdCl2 (in DMF) with methyldiphenylphosphine (in CH2Cl2), or  from K2PdCl2 (in H2O) and methyldiphenylphosphine (in CH2Cl2) using Bu4NCl (in CH2Cl2) as a phase-transfer catalyst.
reaction suitabilitycore: palladium
reaction type: Buchwald-Hartwig Cross Coupling Reaction
reaction type: Cross Couplings
reaction type: Heck Reaction
reaction type: Hiyama Coupling
reaction type: Negishi Coupling
reaction type: Sonogashira Coupling
reaction type: Stille Coupling
reaction type: Suzuki-Miyaura Coupling
reagent type: catalyst
DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II) Preparation Products And Raw materials
Tag:DICHLOROBIS(METHYLDIPHENYLPHOSPHINE)PALLADIUM(II)(52611-08-2) Related Product Information
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