3-Isobutylaniline manufacturers
- 3-Isobutylaniline
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- $6.60
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2019-12-31
- CAS:131826-11-4
- Min. Order: 1KG
- Purity: 97%-99%
- Supply Ability: 1kg-1000kg
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| | 3-Isobutylaniline Basic information |
| Product Name: | 3-Isobutylaniline | | Synonyms: | 3-Isobutylaniline;Benzenamine, 3-(2-methylpropyl)-;3-(2-Methylpropyl)aniline;3-(2-methylpropyl)-Benzenamine | | CAS: | 131826-11-4 | | MF: | C10H15N | | MW: | 149.23 | | EINECS: | | | Product Categories: | | | Mol File: | 131826-11-4.mol |  |
| | 3-Isobutylaniline Chemical Properties |
| Boiling point | 245.7±9.0 °C(Predicted) | | density | 0.944±0.06 g/cm3(Predicted) | | storage temp. | under inert gas (nitrogen or Argon) at 2–8 °C | | pka | 4.60±0.10(Predicted) |
| | 3-Isobutylaniline Usage And Synthesis |
| Uses | 3-Isobutylaniline (cas# 131826-11-4) is a useful research chemical. It is used in the development of novel carboxanilide acaricide, pyflubumide that exhibits excellent acaricidal activity against Tetranychus and Panonychus species. | | Synthesis | The general procedure for the synthesis of 3-isobutylaniline from the compound (CAS: 6026-73-9) was as follows: in a 50 mL round bottom flask, 0.976 g of the oil obtained in Example 11, 1.60 g (15.0 mmol) of sodium hypophosphite monohydrate, 0.27 g (2.5 mmol) of sodium carbonate, and 115 mg of palladium(0)/carbon catalyst ( 5% loading, 50% water content). Subsequently, 2.5 mL of n-butyl acetate and 2.5 mL of water were added and the mixture was reacted under reflux conditions for 3 hours. Upon completion of the reaction, the mixture was processed as in Example 12 and the organic layer was quantitatively analyzed by HPLC internal standard method to yield 0.698 g of 3-isobutyryl aniline (1) (Analytical Condition A). The yield was 93% based on 1-bromo-3-nitrobenzene. | | References | [1] Patent: JP2017/14131, 2017, A. Location in patent: Paragraph 0049
[2] Patent: US5212320, 1993, A |
| | 3-Isobutylaniline Preparation Products And Raw materials |
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