(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone

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(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone Basic information
Product Name:(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone
Synonyms:Methanone, (3-bromo-5-chlorophenyl)(5-chloro-2-methoxyphenyl)-;(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone
CAS:329944-59-4
MF:C14H9BrCl2O2
MW:360.03
EINECS:
Product Categories:
Mol File:Mol File
(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone Structure
(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone Chemical Properties
Boiling point 479.3±45.0 °C(Predicted)
density 1.554±0.06 g/cm3(Predicted)
Safety Information
MSDS Information
(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone Usage And Synthesis
PreparationA solution of 1,3-dibromo-5-chlorobenzene (1 mmol) in ethyl ether was cooled to 78° and n-butyllithium in hexane (1.1 mmol) was added over 2 min.The reaction mixture was stirred at 78° for an additional 10 min, and then 5-chloro-N,2-dimethoxy-N-methylbenzamide (1 mmol) was added in small portions over 4 min. The reaction mixture was stirred at 78° for 1.25 h and then allowed to warm to r.t. and stirred for 14 h (97%).
(3-Bromo-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone Preparation Products And Raw materials
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