Carbonic acid dihexyl ester manufacturers
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| | Carbonic acid dihexyl ester Basic information |
| Product Name: | Carbonic acid dihexyl ester | | Synonyms: | Dabigatran Impurity 90;Dabigatran Etexilate Impurity 94;Dihexyl carbonate? (Dabigatran Impurity);Dihexyl carbonat;Carbonic acid dihexyl ester;carbonacidihexyl ester | | CAS: | 7523-15-1 | | MF: | C13H26O3 | | MW: | 230.34 | | EINECS: | | | Product Categories: | | | Mol File: | 7523-15-1.mol |  |
| | Carbonic acid dihexyl ester Chemical Properties |
| Boiling point | 265-267 °C | | density | 0.910±0.06 g/cm3(Predicted) | | storage temp. | Sealed in dry,Room Temperature | | Appearance | Colorless to light yellow Liquid |
| | Carbonic acid dihexyl ester Usage And Synthesis |
| Synthesis | A syringe tube connected to a glass bulb filter (G2, manufactured by Vidrex Co., Ltd., Japan) was inserted into a two-necked flask equipped with a condenser and a stirrer was placed. 0.75 g of liquid containing the organometallic compound and 41 g of hexanol were added to the flask. Subsequently, high-purity carbon dioxide gas was passed into the flask through the injection tube at a flow rate of 100 mL/min. The flask was heated in an oil bath at 130° C. while continuously stirring and passing carbon dioxide gas to promote the formation of dihexyl carbonate. After 288 hours of reaction, the yield of dihexyl carbonate reached 40%. | | References | [1] Journal of Catalysis, 2014, vol. 318, p. 95 - 107
[2] Patent: EP1460056, 2004, A1. Location in patent: Page 32
[3] Journal of the Chemical Society - Perkin Transactions 1, 1999, # 15, p. 2205 - 2208
[4] Patent: EP1460056, 2004, A1. Location in patent: Page 29
[5] Patent: EP1460056, 2004, A1. Location in patent: Page 29-30 |
| | Carbonic acid dihexyl ester Preparation Products And Raw materials |
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