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5-broMo-4-Methyl-1H-benzo[d]iMidazole Basic information |
| Product Name: | 952511-48-7
5-broMo-4-Methyl-1H-benzo[d]iMidazole | | Synonyms: | 952511-48-7
5-broMo-4-Methyl-1H-benzo[d]iMidazole;5-broMo-4-Methyl-1H-benzo[d]iMidazole;6-bromo-7-methyl-1H-benzo[d]imidazole;5-Bromo-4-methyl-1H-benzimidazole 97%;5-Bromo-4-methyl-1H-benzimidazole;1H-Benzimidazole, 6-bromo-7-methyl-;5-Bromo-4-methylbenzimidazole | | CAS: | 952511-48-7 | | MF: | C8H7BrN2 | | MW: | 211.06 | | EINECS: | | | Product Categories: | | | Mol File: | 952511-48-7.mol | ![952511-48-7
5-broMo-4-Methyl-1H-benzo[d]iMidazole Structure](CAS/GIF/952511-48-7.gif) |
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5-broMo-4-Methyl-1H-benzo[d]iMidazole Chemical Properties |
| Boiling point | 418.3±25.0 °C(Predicted) | | density | 1.654±0.06 g/cm3(Predicted) | | storage temp. | Sealed in dry,Room Temperature | | pka | 11.60±0.30(Predicted) | | Appearance | Yellow to brown Solid |
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5-broMo-4-Methyl-1H-benzo[d]iMidazole Usage And Synthesis |
| Synthesis | 3. A mixture of 4-bromo-3-methylbenzene-1,2-diamine (28 g, 140 mmol), formic acid (240 mL), and 37% hydrochloric acid (400 mL) was heated to 60 °C and held for 12 h. The reaction was completed by filtration. Upon completion of the reaction, the mixture was cooled in an ice-water bath and the pH was slowly adjusted to 8-9 with 28% ammonia. the resulting solid was collected by filtration, washed with water, and dried in air to afford 5-bromo-4-methyl-1H-benzo[d]imidazole (25 g, 98% yield) as a yellow solid. Mass spectrum (ESI) m/z = 213 [M + 1]+. | | References | [1] Patent: WO2013/26914, 2013, A1. Location in patent: Page/Page column 143
[2] Patent: US2010/222345, 2010, A1. Location in patent: Page/Page column 87 |
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5-broMo-4-Methyl-1H-benzo[d]iMidazole Preparation Products And Raw materials |
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