2-Chloro-5-aminophenol

2-Chloro-5-aminophenol Suppliers list

Company Name:	Hebei Chuanghai Biotechnology Co,.LTD
Tel:	+86-13131129325
Email:	sales1@chuanghaibio.com
Products Intro:	Product Name:2-Chloro-5-aminophenol CAS:6358-06-1 Purity:99.9 Package:1KG;9.00;USD

Company Name:	airuikechemical co., ltd.
Tel:	+86-18353166132
Email:	sales02@airuikechemical.com
Products Intro:	Product Name:2-chloro-5-Aminophenol CAS:6358-06-1 Purity:99.99% Package:1g;0.00;USD\|5g;0.00;USD\|25g;0.00;USD

Company Name:	Capot Chemical Co.,Ltd.
Tel:	+86-（0）57185586718; +8613336195806
Email:	sales@capot.com
Products Intro:	Product Name:5-Amino-2-chlorophenol CAS:6358-06-1 Purity:98%(Min,GC) Package:100g;1kg;5kg,10kg,25kg,50kg

Company Name:	Nanjing ChemLin Chemical Industry Co., Ltd.
Tel:	025-83697070
Email:	product@chemlin.com.cn
Products Intro:	CAS:6358-06-1 Purity:99% Package:g-Kg

Company Name:	career henan chemical co
Tel:	+86-0371-86658258 +8613203830695
Email:	sales@coreychem.com
Products Intro:	Product Name:2-Chloro-5-aminophenol CAS:6358-06-1 Purity:98% Package:1KG;1USD

2-Chloro-5-aminophenol manufacturers

2-Chloro-5-aminophenol Basic information

Product Name:	2-Chloro-5-aminophenol
Synonyms:	3-amino-6-chlorophenol;5-amino-2-chloro-pheno;2-CHLORO-5-AMINOPHENOL;5-AMINO-2-CHLOROPHENOL;4-Chloro-3-hydroxyaniline;2-ch1oro-5-aminophenol;5-azanyl-2-chloro-phenol;2-Chloro-5-aminophenol, >=99%
CAS:	6358-06-1
MF:	C6H6ClNO
MW:	143.57
EINECS:
Product Categories:	Amines;blocks
Mol File:	6358-06-1.mol

2-Chloro-5-aminophenol Chemical Properties

Melting point	160 °C
Boiling point	185.5°C (rough estimate)
density	1.2028 (rough estimate)
refractive index	1.5618 (estimate)
storage temp.	under inert gas (nitrogen or Argon) at 2–8 °C
solubility	DMSO, Methanol
pka	8.55±0.10(Predicted)
form	Powder
color	Gray
Sensitive	Light Sensitive
InChIKey	JSCNCRWPXOTDDZ-UHFFFAOYSA-N
CAS DataBase Reference	6358-06-1(CAS DataBase Reference)
EPA Substance Registry System	Phenol, 5-amino-2-chloro- (6358-06-1)

Safety Information

MSDS Information

2-Chloro-5-aminophenol Usage And Synthesis

Chemical Properties	White powder
Uses	5-Amino-2-chlorophenol is used in the synthesis of antimalarial quinolones. Also used in the synthesis of potent anti-HIV agents based upon pyrimidinylphenylamine 1.
Synthesis	619-10-3 6358-06-1 Step 1: 2-Chloro-5-nitrophenol (20.0 g, 115.2 mmol) was dissolved in a solvent mixture of ethanol (150 mL) and water (150 mL). To this solution, iron powder (32.2 g, 576.2 mmol) and ammonium chloride (32.1 g, 599.3 mmol) were added sequentially. The reaction mixture was heated to reflux and kept for 2 hours. After completion of the reaction, it was cooled to room temperature and filtered to remove insoluble material. The filtrate was concentrated to dryness under reduced pressure. The residue was purified by fast column chromatography (eluent: hexane/ethyl acetate = 9:1) to afford 5-amino-2-chlorophenol (15.85 g, 96% yield) as a white solid.
References	[1] Patent: US2003/100580, 2003, A1 [2] Patent: US2010/160388, 2010, A1. Location in patent: Page/Page column 58 [3] Patent: US2010/160389, 2010, A1. Location in patent: Page/Page column 49 [4] Patent: US2011/28502, 2011, A1. Location in patent: Page/Page column 44-45 [5] Patent: US2011/71143, 2011, A1. Location in patent: Page/Page column 36

2-Chloro-5-aminophenol Preparation Products And Raw materials

Raw materials	4-Chloro-3-methoxyaniline-->2-Chloro-5-nitrophenol-->2-CHLORO-5-NITROANISOLE-->2-Methoxy-4-nitroaniline-->2-Amino-5-nitrophenol-->Ethanol-->Iron-->Ammonium chloride-->Water
Preparation Products	5-amino-4-bromo-2-chlorophenol-->4-Chloro-3-ethoxyaniline-->Benzenamine, 4-chloro-3-(1-methylethoxy)--->TERT-BUTYL 4-CHLORO-3-HYDROXYPHENYLCARBAMATE

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