4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine

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Company Name:	Shanghai Boc Chemical Co., Ltd.
Tel:	021-34975602; +8618721111801
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Products Intro:	Product Name:4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine CAS:123148-78-7 Purity:0.98 Package:50KG；5KG;1KG

Company Name:	Capot Chemical Co.,Ltd.
Tel:	+86-（0）57185586718; +8613336195806
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Products Intro:	Product Name:4-chloro-5-iodo-7H-pyrrolo[2,3-d]pyrimidine CAS:123148-78-7 Purity:98%(Min.) Package:1G;1KG;100KG

Company Name:	Hi-Tech Chemistry Corp
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Products Intro:	Product Name:4-chloro-5-iodo-7H-pyrrolo[2,3-d]pyrimidine CAS:123148-78-7

Company Name:	Shanghai Time Chemicals CO., Ltd.
Tel:	+86-021-57951555 +8617317452075
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Products Intro:	CAS:123148-78-7

Company Name:	Nanjing ChemLin Chemical Industry Co., Ltd.
Tel:	025-83697070
Email:	product@chemlin.com.cn
Products Intro:	CAS:123148-78-7 Purity:98% Package:g-Kg Remarks:Light yellow powder

4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine manufacturers

4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine Basic information

Product Name:	4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine
Synonyms:	4-Chloro-5-iodo-7H-pyrrolo[2,3-d]pyrimidine;4-CHLORO-5-IODO-7H-PYRROL[2,3]PYRIMIDINE;4-CHLORO-5-IODO-1H-PYRROLO [2,3-D] PYRIMIDINE;4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine;6-Chloro-7-iodo-7-deazapurine;4-Chloro-5-iodo-1H-pyrrol...;JR-13973, 4-Chloro-5-iodo-7H-pyrrolo[2,3-d]pyrimidine, 95%;7H-Pyrrolo[2,3-d]pyriMidine, 4-chloro-5-iodo-
CAS:	123148-78-7
MF:	C6H3ClIN3
MW:	279.47
EINECS:	626-377-7
Product Categories:	Heterocycle-Pyrimidine series
Mol File:	123148-78-7.mol

4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine Chemical Properties

Melting point	179-183 °C
Boiling point	241.0±50.0 °C(Predicted)
density	2.47±0.1 g/cm3(Predicted)
storage temp.	Keep in dark place,Sealed in dry,Room Temperature
form	powder to crystal
pka	9.61±0.20(Predicted)
color	White to Orange to Green
Water Solubility	Insoluble in water.
λmax	305nm(H2O)(lit.)
Sensitive	Light Sensitive
InChI	InChI=1S/C6H3ClIN3/c7-5-4-3(8)1-9-6(4)11-2-10-5/h1-2H,(H,9,10,11)
InChIKey	CBWBJFJMNBPWAL-UHFFFAOYSA-N
SMILES	C1=NC(Cl)=C2C(I)=CNC2=N1

Safety Information

Hazard Codes	Xn
Risk Statements	22-36/37/38-R36/37/38-R22
Safety Statements	26-36/37-S36/37-S26-37
WGK Germany	3
HazardClass	IRRITANT
HS Code	29335990
Storage Class	11 - Combustible Solids
Hazard Classifications	Acute Tox. 4 Oral Eye Irrit. 2 Skin Irrit. 2 STOT SE 3

MSDS Information

4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine Usage And Synthesis

Uses	6-Chloro-7-iodo-7-deazapurine is used as pharmaceutical intermediate.
Definition	4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine, also known as 6-Chloro-7-iodo-7-deazapurine or 4-Chloro-5-iodo-1H-pyrrolo[2,3-d]pyrimidine, is a white solid that can be obtained by iodine reaction of 4-chloro-7h-pyrrole [2,3-d] pyrimidine with NIS.
Synthesis	4-chloro-7h-pyrrole [2,3-d] pyrimidine (8.0 g, 52.32 mmol, 1.0 eq) was dissolved in DMF(40 mL) and NIS(15.7g, 57.55 mmol, 1.1eq) was added at 0℃. After stirring at room temperature overnight, 200 mL of saturated Na2S2O3 solution was added. The mixture was filtered, washed with water three times, and vacuum drying, to obtain 4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine.
References	[1] Patent: US2005/107312, 2005, A1 [2] Patent: US2005/215510, 2005, A1 [3] Patent: US2005/215511, 2005, A1 [4] Patent: WO2012/158795, 2012, A1. Location in patent: Page/Page column 100

4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine Preparation Products And Raw materials

Raw materials	N-Iodosuccinimide-->4-Chloro-7H-pyrrolo[2,3-d]pyrimidine-->Ethanol-->N,N-Dimethylformamide-->Sodium sulfate
Preparation Products	5-iodo-7-Methyl-7H-pyrrolo[2,3-d]pyriMidin-4-aMine-->4-Chloro-7H-pyrrolo[2,3-d]pyrimidine-5-carbonitrile-->PF-06447475-->5-IODOTUBERCIDIN-->4-CHLORO-7-CYCLOPENTYL-5-IODO-7H-PYRROLO[2,3-D]PYRIMIDINE

Tag:4-Chloro-5-iodo-7H-pyrrol[2,3-d]pyrimidine(123148-78-7) Related Product Information

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