| Company Name: |
J & K SCIENTIFIC LTD.
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| Tel: |
18210857532; 18210857532 |
| Email: |
jkinfo@jkchemical.com |
| Products Intro: |
Product Name:1-Boc-amino-butyl-3-amine
CAS:878799-20-3
Package:1g
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| Company Name: |
Chemsky（shanghai）International Co.,Ltd.
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| Tel: |
021-50135380 |
| Email: |
shchemsky@sina.com |
| Products Intro: |
Product Name:1-Boc-aMinobutyl-3-aMine
CAS:878799-20-3
Purity:98%+ Package:2490RMB/100MG; 5000RMB/250MG; 1800RMB/25MG; 7970RMB/1G
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| Company Name: |
Shanghai Sheepchem Co., Ltd.
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| Tel: |
+86 (21) 6715-7650 |
| Email: |
sheepchem@163.com |
| Products Intro: |
Product Name:1-Boc-aMino-butyl-3-aMine
CAS:878799-20-3
Purity:96% Package:50g;500g;1kg;5kg Remarks:For R&D Only
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| | 1-BOC-AMINO-BUTYL-3-AMINE Basic information |
| Product Name: | 1-BOC-AMINO-BUTYL-3-AMINE | | Synonyms: | 1-BOC-AMINO-BUTYL-3-AMINE;Carbamic acid, N-(3-aminobutyl)-, 1,1-dimethylethyl ester;tert-Butyl (3-aMinobutyl)carbaMate;1-N-Boc-butane-1,3-diamine | | CAS: | 878799-20-3 | | MF: | C9H20N2O2 | | MW: | 188.27 | | EINECS: | | | Product Categories: | | | Mol File: | 878799-20-3.mol |  |
| | 1-BOC-AMINO-BUTYL-3-AMINE Chemical Properties |
| Boiling point | 282.6±23.0 °C(Predicted) | | density | 0.972±0.06 g/cm3(Predicted) | | storage temp. | Keep in dark place,Inert atmosphere,Store in freezer, under -20°C | | pka | 12.77±0.46(Predicted) |
| | 1-BOC-AMINO-BUTYL-3-AMINE Usage And Synthesis |
| Synthesis | Under nitrogen protection, 1,3-dimethylethyl phenylmethyl-1,3-butanediyl biscarbamate (0.19 g, 0.59 mmol) was dissolved in 5 mL of ethanol and 30 mg of 10% palladium/carbon catalyst was added. The reaction mixture was placed under hydrogen atmosphere (1 atm) and stirred at room temperature for 5 hours. After completion of the reaction, the catalyst was removed by filtration and the filtrate was concentrated to give 0.10 g of tert-butyl (3-aminobutyl)carbamate in 90% yield. | | References | [1] Patent: WO2006/29210, 2006, A2. Location in patent: Page/Page column 125 |
| | 1-BOC-AMINO-BUTYL-3-AMINE Preparation Products And Raw materials |
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