2-Iodo-6-methoxyphenol

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2-Iodo-6-methoxyphenol Basic information
Product Name:2-Iodo-6-methoxyphenol
Synonyms:Phenol, 2-iodo-6-methoxy-;2-Iodo-6-methoxyphenol
CAS:111726-46-6
MF:C7H7IO2
MW:250.04
EINECS:
Product Categories:
Mol File:111726-46-6.mol
2-Iodo-6-methoxyphenol Structure
2-Iodo-6-methoxyphenol Chemical Properties
Boiling point 233.2±20.0 °C(Predicted)
density 1.866±0.06 g/cm3(Predicted)
storage temp. 2-8°C(protect from light)
pka8.52±0.10(Predicted)
Safety Information
MSDS Information
2-Iodo-6-methoxyphenol Usage And Synthesis
DefinitionChEBI: 2-iodo-6-methoxyphenol is a member of phenols and an organoiodine compound.
Synthesis
1-iodo-3-methoxy-2-(methoxymethoxy)benzene

165071-94-3

2-IODO-6-METHOXYPHENOL

111726-46-6

Methyl 3-(2-methoxyphenoxy)propionate (CAS: 165071-94-3, 52 g, 0.18 mol) was dissolved in methanol (400 mL) at 0 °C and 2 M methanolic solution of hydrochloric acid (100 mL) was slowly added. The reaction mixture was stirred at room temperature for 4 h. The solvent was removed by concentration under reduced pressure to afford 2-iodo-6-methoxyphenol (42 g, 95% yield).

References[1] Patent: WO2010/94242, 2010, A1. Location in patent: Example 3.3
[2] Canadian Journal of Chemistry, 1987, vol. 65, p. 2019 - 2023
2-Iodo-6-methoxyphenol Preparation Products And Raw materials
Raw materials1-iodo-3-methoxy-2-(methoxymethoxy)benzene-->Methanol-->Hydrochloric acid
Preparation Products3-(2-Iodo-6-methoxyphenoxy)propan-1-ol
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