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ChemicalBook > Product Catalog >Organic Chemistry >Amides >Naphthenic amines derivatives >4-Nitrodiphenylamine

4-Nitrodiphenylamine

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CAS:836-30-6
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4-Nitrodiphenylamine Basic information
Product Name:4-Nitrodiphenylamine
Synonyms:4-nitro-n-phenylbenzenamine;4-nitro-N-phenyl-benzenamine;Benzenamine, 4-nitro-N-phenyl-;diphenyl,4-nitro-amin;Diphenylamine, 4-nitro-;N-(4-Nitrophenyl)-N-phenylamine;p-Nitrophenylphenylamine;(4-NITROPHENYL)PHENYLAMINE
CAS:836-30-6
MF:C12H10N2O2
MW:214.22
EINECS:212-646-2
Product Categories:Aromatics Compounds;Aromatics;Amines;C11 to C38;Nitrogen Compounds;Intermediates of Dyes and Pigments
Mol File:836-30-6.mol
4-Nitrodiphenylamine Structure
4-Nitrodiphenylamine Chemical Properties
Melting point 132-135 °C (lit.)
Boiling point 211 °C (30 mmHg)
density 1.2042 (rough estimate)
refractive index 1.6660 (estimate)
Fp 190°C
storage temp. Refrigerator
solubility DMSO (Slightly), Methanol (Slightly)
pka-2.60±0.20(Predicted)
form Solid
color Orange to Brown
Water Solubility INSOLUBLE
BRN 2051910
InChI1S/C12H10N2O2/c15-14(16)12-8-6-11(7-9-12)13-10-4-2-1-3-5-10/h1-9,13H
InChIKeyXXYMSQQCBUKFHE-UHFFFAOYSA-N
SMILES[O-][N+](=O)c1ccc(Nc2ccccc2)cc1
CAS DataBase Reference836-30-6(CAS DataBase Reference)
NIST Chemistry ReferenceN-(4-Nitrophenyl)-N-phenylamine(836-30-6)
EPA Substance Registry System4-Nitrodiphenylamine (836-30-6)
Safety Information
Hazard Codes Xi
Risk Statements 36/37/38
Safety Statements 26-37/39-36
RIDADR 3077
WGK Germany 3
RTECS JJ9600000
Hazard Note Irritant
TSCA TSCA listed
HazardClass 9
PackingGroup III
HS Code 29214400
Storage Class11 - Combustible Solids
Hazard ClassificationsEye Irrit. 2
Skin Irrit. 2
STOT SE 3
Hazardous Substances Data836-30-6(Hazardous Substances Data)
MSDS Information
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4-Nitrodiphenylamine English
SigmaAldrich English
ACROS English
ALFA English
4-Nitrodiphenylamine Usage And Synthesis
Chemical PropertiesOrange Crystalline Solid
Uses4-Nitrodiphenylamine was used to study reduction of nitrated diphenylamine derivatives in sediment water batch enrichments and dense cell suspensions of anaerobic, aromatic-compound-mineralizing pure bacterial cultures.
Synthesis Reference(s)The Journal of Organic Chemistry, 42, p. 1786, 1977 DOI: 10.1021/jo00430a025
General Description4-Nitrodiphenylamine undergoes heterogeneous catalytic transfer hydrogenation to form p-phenylenediamines. 4-Nitrodiphenylamine is used as stabilizer for propellants and explosives.
Purification MethodsCrystallise the amine from EtOH or aqueous EtOH (m 135-136o) and has m 131.5-132o after sublimation in vacuo. [Beilstein 12 H 715, 12 III 1586.]
Toxics Screening LevelThe NOEL from this study was reported as 8.5 mg/m3. The calculation for the ITSL of 1 μg/m3 on an annually averaged basis
4-Nitrodiphenylamine Preparation Products And Raw materials
Raw materials2-Nitrodiphenylamine-->2-(Methylamino)pyridine-->Nitrobenzene
Preparation Products4-Aminodiphenylamine-->Disperse Orange 97-->Amoscanate-->Disperse Orange 97-->N-Isopropyl-N'-phenyl-1,4-phenylenediamine
Tag:4-Nitrodiphenylamine(836-30-6) Related Product Information
Phenothiazine 2-Aminodiphenylamine 2-Methyl-4-nitroaniline 4-Aminodiphenylamine Sodium diphenylamine-4-sulfonate 2,6-Dichloro-4-nitroaniline 5-Nitroanthranilonitrile Diphenylamine 2-BROMO-4-NITROANILINE 2-Chloro-4-nitroaniline 2,4-Dinitrodiphenylamine 4-(2,4-DINITROANILINO)PHENOL HexanitrodiphenylaMine DISPERSE YELLOW 9 ACID YELLOW 65 4-NITROSODIPHENYLAMINE N-Nitrosodiphenylamine Diphenylamine,sulfuric acid solution
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