4-(HYDROXYMETHYL)CYCLOHEXANONE

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Products Intro: Product Name:4-(Hydroxymethyl)cyclohexanone
CAS:38580-68-6
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Products Intro: Product Name:4-(Hydroxymethyl)cyclohexanone
CAS:38580-68-6
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Products Intro: Product Name:4-(Hydroxymethyl)cyclohexanone
CAS:38580-68-6
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4-(HYDROXYMETHYL)CYCLOHEXANONE Basic information
Product Name:4-(HYDROXYMETHYL)CYCLOHEXANONE
Synonyms:4-(HYDROXYMETHYL)CYCLOHEXANONE;4-(Hydroxymethyl)cyclohexan-1-one;101951;4-(Hydroxymethyl)cyclohexan-1-one 97%;(4-Oxocyclohex-1-yl)methanol, 1-(Hydroxymethyl)-4-oxocyclohexane;4-(HydroxyMethly)cyclohexanone;4-Methylolcyclohexan-1-one;Cyclohexanone, 4-(hydroxyMethyl)-
CAS:38580-68-6
MF:C7H12O2
MW:128.17
EINECS:
Product Categories:Ring Systems;Hydroxymethyl's
Mol File:38580-68-6.mol
4-(HYDROXYMETHYL)CYCLOHEXANONE Structure
4-(HYDROXYMETHYL)CYCLOHEXANONE Chemical Properties
Boiling point 239.8±13.0 °C(Predicted)
density 1.054±0.06 g/cm3(Predicted)
storage temp. Inert atmosphere,Store in freezer, under -20°C
form solid
pka14.85±0.10(Predicted)
InChIInChI=1S/C7H12O2/c8-5-6-1-3-7(9)4-2-6/h6,8H,1-5H2
InChIKeyKHMBXNKCMNGLKG-UHFFFAOYSA-N
SMILESC1(=O)CCC(CO)CC1
Safety Information
Hazard Codes Xi
Risk Statements 37/38-41
Safety Statements 26-39
HS Code 2914500090
MSDS Information
4-(HYDROXYMETHYL)CYCLOHEXANONE Usage And Synthesis
Uses4-(Hydroxymethyl)cyclohexanone is a reagent used for the preparation of indazoles and benzisoxazoles containing cyclohexylazetidine moieties which are CCR2 antagonists with good hERG selectivity.
Synthesis Reference(s)Tetrahedron Letters, 19, p. 2771, 1978 DOI: 10.1016/S0040-4039(01)94858-0
Synthesis
1,10-Undecanediol

10596-05-1

4-(Hydroxymethyl)cyclohexanol (cis- and trans- mixture)

33893-85-5

2-UNDECANOL

1653-30-1

4-(HYDROXYMETHYL)CYCLOHEXANONE

38580-68-6

Example 5: Ce(IV)/PFCP (50 mg, 0.027 mmol) and NaBrO3 (200 mg) were dispersed and dissolved in acetic acid. Subsequently, 1,10-undecanediol (1.0 mmol) and 4-hydroxymethylcyclohexanol (1.0 mmol) were added, respectively. The reaction mixture was heated at 55°C for 3 hours. Upon completion of the reaction, the products were purified by column chromatography to afford 10-undecan-1-ol (154 mg, 82% yield) and 4-hydroxymethylcyclohexanone (93 mg, 73% yield).

References[1] Patent: US4617153, 1986, A
Tag:4-(HYDROXYMETHYL)CYCLOHEXANONE(38580-68-6) Related Product Information
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