| Company Name: |
Tetranov Biopharm
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| Tel: |
13526569071 |
| Email: |
sales@leadmedpharm.com |
| Products Intro: |
Product Name:3-(2-Methoxyphenyl)propanal
CAS:33538-83-9
Purity:95% Package:1g;5g;25g;100g
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3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE manufacturers
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| | 3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE Basic information |
| Product Name: | 3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE | | Synonyms: | 3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE;3-(2-Methoxyphenyl)propanal;Benzenepropanal, 2-Methoxy-;3-(2-Methoxy-phenyl)-propionaldehyde ,98%;3-(2-Methoxyphenyl)propana | | CAS: | 33538-83-9 | | MF: | C10H12O2 | | MW: | 164.2 | | EINECS: | | | Product Categories: | | | Mol File: | 33538-83-9.mol |  |
| | 3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE Chemical Properties |
| Boiling point | 260 °C | | density | 1.025±0.06 g/cm3(Predicted) | | storage temp. | Inert atmosphere,Store in freezer, under -20°C |
| | 3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE Usage And Synthesis |
| Synthesis | The general procedure for the synthesis of 3-(2-methoxyphenyl)propionaldehyde from 2'-methoxycinnamaldehyde was as follows: a suspension of 2'-methoxycinnamaldehyde (1.00 g, 6.17 mmol) with Pd/C (131 mg, 0.20 mmol) in methanol (12 mL) was stirred and reacted for 2 h at room temperature. Upon completion of the reaction, the reaction mixture was filtered through a diatomaceous earth pad and washed with dichloromethane. After combining the filtrates, the solvent was removed by concentration under reduced pressure. The resulting residue was purified by column chromatography (eluent: hexane/ethyl acetate, 3/1, v/v) to afford the target product 3-(2-methoxyphenyl)propionaldehyde. | | References | [1] Bioorganic and Medicinal Chemistry Letters, 2017, vol. 27, # 2, p. 237 - 241
[2] Bioorganic and Medicinal Chemistry Letters, 1997, vol. 7, # 19, p. 2473 - 2476
[3] Chemical Communications, 2014, vol. 50, # 94, p. 14752 - 14755 |
| | 3-(2-METHOXY-PHENYL)-PROPIONALDEHYDE Preparation Products And Raw materials |
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