- 2,4-Dichlorobenzyl chloride
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- $5.00 / 1KG
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2025-09-25
- CAS:94-99-5
- Min. Order: 1KG
- Purity: 99%
- Supply Ability: g-kg-tons, free sample is available
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| | 2,4-Dichlorobenzyl chloride Basic information |
| Product Name: | 2,4-Dichlorobenzyl chloride | | Synonyms: | 2,4-dichloro-1-(chloromethyl)-benzen;2,4-Dichloro-1-(chloromethyl)benzene;2,4-dichloro-1-chloromethyl-benzene;-2,4-Trichlorotoluene;benzene,2,4-dichloro-1-(chloromethyl)-;Toluene, alpha2,4-trichloro-;toluene,α,2,4-trichloro-;α,2,4-trichlorotoluene | | CAS: | 94-99-5 | | MF: | C7H5Cl3 | | MW: | 195.47 | | EINECS: | 202-381-0 | | Product Categories: | Aromatics;Miscellaneous Reagents;Econazole Nitrate;Aromatic Halides (substituted) | | Mol File: | 94-99-5.mol |  |
| | 2,4-Dichlorobenzyl chloride Chemical Properties |
| Hazard Codes | C,N | | Risk Statements | 34-37-50/53-22 | | Safety Statements | 26-36/37/39-45-61-60 | | RIDADR | UN 3265 8/PG 2 | | WGK Germany | 3 | | F | 19 | | Hazard Note | Corrosive | | TSCA | TSCA listed | | HazardClass | 8 | | PackingGroup | II | | HS Code | 29036990 | | Storage Class | 8A - Combustible corrosive hazardous materials | | Hazard Classifications | Skin Corr. 1B |
| | 2,4-Dichlorobenzyl chloride Usage And Synthesis |
| Chemical Properties | clear colorless to very light yellow oily liquid | | Uses | 2,4-Dichlorobenzyl chloride is a reagent used in the addition of dichlorobenzene. | | Uses | 2,4-Dichlorobenzyl chloride was used as starting reagent for the synthesis of series of novel 1,2,4-triazolium derivatives. | | Synthesis | GENERAL STEPS: 2,4-dichlorobenzyl alcohol (17.7 g, 0.1 mol), dichloromethane (30 mL), and N,N-dimethylformamide (DMF, 1 mL) were added to a 100 mL round-bottomed flask, followed by the slow dropwise addition of phosphorus trichloride (4.68 g, 0.034 mol). The reaction mixture was heated to reflux temperature (60-80°C) and the reaction lasted for 2-3 hours. The progress of the reaction was monitored by thin layer chromatography (TLC) until the complete disappearance of the raw material. After completion of the reaction, 2,4-dichlorobenzyl chloride (17.99 g, 92% yield) was purified by distillation. | | References | [1] Patent: CN106117028, 2016, A. Location in patent: Paragraph 0053; 0054; 0055; 0056 |
| | 2,4-Dichlorobenzyl chloride Preparation Products And Raw materials |
| Raw materials | Chlorine-->AIBN-->2,4-Dichlorotoluene-->ALPHA,ALPHA,2,4-TETRACHLOROTOLUENE-->2,4-Dichlorobenzonitrile-->1,3-Bis(chloromethyl)benzene-->2,4-Dichlorobenzoic acid-->2,4-Dichlorobenzyl alcohol-->Dichloromethane-->Phosphorus trichloride | | Preparation Products | 2,4-Dichlorobenzaldehyde-->ALPHA,ALPHA,2,4-TETRACHLOROTOLUENE-->2,4-Dichlorophenylacetonitrile-->Lonidamine-->5-AMino-1-(2,4-dichlorobenzyl)-1H-indazol-3-ol-->1-((2,4-DICHLOROBENZYL)AMINO)PROPAN-2-OL-->N-(2,4-DICHLOROBENZYL)-2-METHOXYETHANAMINE-->1-(4-Chlorophenyl)-2-(2,4-dichlorophenyl)ethanone |
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