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3-Chloro-4-fluoronitrobenzene

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CAS:350-30-1
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3-Chloro-4-fluoronitrobenzene manufacturers

3-Chloro-4-fluoronitrobenzene Basic information
Synthesis
Product Name:3-Chloro-4-fluoronitrobenzene
Synonyms:2-chloro-1-fluoro-4-nitro-benzen;Benzene, 2-chloro-1-fluoro-4-nitro-;Benzene,2-chloro-1-fluoro-4-nitro-;2-CHLORO-1-FLUORO-4-NITROBENZENE;1-CHLORO-2-FLUORO-5-NITROBENZENE;3-CHLORO-4-FLUORONITROBENZENE;4-FLUORO-3-CHLORONITROBENZENE;3-chloro-4-fluorobenzene
CAS:350-30-1
MF:C6H3ClFNO2
MW:175.54
EINECS:206-499-3
Product Categories:Fluorinated benzene series;Nitro Compounds;Nitrogen Compounds;Organic Building Blocks
Mol File:350-30-1.mol
3-Chloro-4-fluoronitrobenzene Structure
3-Chloro-4-fluoronitrobenzene Chemical Properties
Melting point 40-42 °C(lit.)
Boiling point 227-232°C
density 1.61
Fp >230 °F
storage temp. Sealed in dry,Room Temperature
solubility soluble in Methanol
form powder to crystal
color White to Light yellow to Green
BRN 1944997
InChIInChI=1S/C6H3ClFNO2/c7-5-3-4(9(10)11)1-2-6(5)8/h1-3H
InChIKeyDPHCXXYPSYMICK-UHFFFAOYSA-N
SMILESC1(F)=CC=C([N+]([O-])=O)C=C1Cl
CAS DataBase Reference350-30-1(CAS DataBase Reference)
NIST Chemistry Reference3-Chloro-4-fluoronitrobenzene(350-30-1)
EPA Substance Registry System3-Chloro-4-fluoronitrobenzene (350-30-1)
Safety Information
Hazard Codes Xn,Xi
Risk Statements 22-37/38-41-36/37/38-20/21/22
Safety Statements 26-39-36/37/39
RIDADR 2811
WGK Germany 3
RTECS CZ0720000
Hazard Note Irritant
HazardClass 6.1
PackingGroup III
HS Code 29049090
MSDS Information
ProviderLanguage
3-Chloro-4-fluoronitrobenzene English
SigmaAldrich English
ACROS English
ALFA English
3-Chloro-4-fluoronitrobenzene Usage And Synthesis
SynthesisIn certain instances, when both chloro and nitro may act as a leaving group, a surprising selectivity of one over the other is observed, for example chloro-2,5- dinitrobenzene was converted to 4-fluoro-3-chloronitrobenzene.
3-Chloro-4-fluoronitrobenzene
Chemical Propertieswhite to light yellow crystal powder
Uses2-Chloro-1-fluoro-4-nitrobenzene is an intermediate used in synthesis of benzoimidolones on Ameba resin and methyl 6,7,8,9-tetrahydropyrido[1,2-a]indol-10-ylacetate.
Uses2-Chloro-1-fluoro-4-nitrobenzene has been used in synthesis of:
  • benzoimidolones on Ameba resin
  • methyl 6,7,8,9-tetrahydropyrido[1,2-a]indol-10-ylacetate
Synthesis Reference(s)The Journal of Organic Chemistry, 63, p. 8448, 1998 DOI: 10.1021/jo981557o
Synthetic Communications, 21, p. 505, 1991 DOI: 10.1080/00397919108016776
General Description2-Chloro-1-fluoro-4-nitrobenzene undergoes reduction in the presence of Mo(CO)6 and 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) under microwave irradiation to yield a mixture of 3-chloro-4-fluoroaniline and 3-chloro-4-ethoxyaniline.
References[1] Catalysis Today, 2012, vol. 198, # 1, p. 300 - 304
[2] Chemical Communications, 1996, # 3, p. 297 - 298
[3] Chemical Communications, 1996, # 3, p. 297 - 298
[4] Journal of Fluorine Chemistry, 2004, vol. 125, # 5, p. 701 - 704
[5] Advanced Synthesis and Catalysis, 2008, vol. 350, # 17, p. 2677 - 2682
Tag:3-Chloro-4-fluoronitrobenzene(350-30-1) Related Product Information
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