(4-AMINO-3-METHOXYPHENYL)METHANOL

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CAS:148459-54-5
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(4-AMINO-3-METHOXYPHENYL)METHANOL manufacturers

(4-AMINO-3-METHOXYPHENYL)METHANOL Basic information
Product Name:(4-AMINO-3-METHOXYPHENYL)METHANOL
Synonyms:(4-AMINO-3-METHOXYPHENYL)METHANOL;[4-Amino-3-(methyloxy)phenyl]methanol;BenzeneMethanol,4-aMino-3-Methoxy-;4-Amino-3-methoxy-benzenemethanol;4-Amino-3-methoxybenzyl Alcohol
CAS:148459-54-5
MF:C8H11NO2
MW:153.18
EINECS:
Product Categories:
Mol File:148459-54-5.mol
(4-AMINO-3-METHOXYPHENYL)METHANOL Structure
(4-AMINO-3-METHOXYPHENYL)METHANOL Chemical Properties
Boiling point 312℃
density 1.182
Fp 142℃
storage temp. Keep in dark place,Inert atmosphere,Room temperature
AppearanceLight brown to yellow Liquid
InChIInChI=1S/C8H11NO2/c1-11-8-4-6(5-10)2-3-7(8)9/h2-4,10H,5,9H2,1H3
InChIKeyRVYSKGNWKIIUIF-UHFFFAOYSA-N
SMILESC1(CO)=CC=C(N)C(OC)=C1
Safety Information
HS Code 2922500090
MSDS Information
(4-AMINO-3-METHOXYPHENYL)METHANOL Usage And Synthesis
Uses(4-Amino-3-methoxyphenyl)methanol is a key intermediate in cyclotriveratrylene chemistry.
Synthesis
3-METHOXY-4-NITROBENZYL ALCOHOL

80866-88-2

(4-AMINO-3-METHOXYPHENYL)METHANOL

148459-54-5

3-Methoxy-4-nitrobenzyl alcohol (5 g, 27 mmol) was used as starting material, which was dissolved in methanol (250 mL) and subsequently transferred to a reaction flask containing 10% Pd-C catalyst (5 mol%). The reaction mixture was stirred and reacted overnight under hydrogen atmosphere. Upon completion of the reaction, the catalyst was removed by filtration through a diatomaceous earth plug and the filtrate was concentrated. The crude product was purified by silica gel column chromatography using EtOAc/hexane as eluent to give the final 4-amino-3-methoxybenzyl alcohol as a colorless oil (0.5 g, 15% yield).

References[1] Bulletin de la Societe Chimique de France, 1993, vol. 130, # 1, p. 93 - 95
[2] Patent: WO2005/97752, 2005, A1. Location in patent: Page/Page column 124-125
[3] Tetrahedron, 2004, vol. 60, # 19, p. 4295 - 4302
[4] Patent: US5994368, 1999, A
[5] Patent: US6008229, 1999, A
(4-AMINO-3-METHOXYPHENYL)METHANOL Preparation Products And Raw materials
Raw materials3-METHOXY-4-NITROBENZYL ALCOHOL-->Hydrogen-->Methanol
Tag:(4-AMINO-3-METHOXYPHENYL)METHANOL(148459-54-5) Related Product Information
Methyl 4-amino-3-methoxybenzoate 4-Amino-3-methoxybenzoic acid 3-Methoxy-4-nitrobenzoic acid Benoxinate Hydrochloride 3-METHOXY-4-NITROBENZYL ALCOHOL Oxybuprocaine 4-Amino-3-(trifluoromethoxy)benzoic acid Methyl 3-methoxy-4-nitrobenzoate NITR 5/AM ETHYL 2-(4-AMINO-3-METHOXYPHENYL)-3,3,3-TRIFLUORO-2-HYDROXYPROPANOATE 3-BUTOXY-4-NITROBENZOIC ACID 1-[2-AMINO-5-(1-HYDROXY-1-(2-NITRO-4,5-METHYLENEDIOXYPHENYL))METHYL)PHENOXY]-2-(2'-AMINO-5'-METHYLPHENOXY)CYCLOPENTANE-N,N,N',N'-TETRAACETIC ACID, 4NA 5-(METHOXYCARBONYL)-2-NITROPHENYL 2-THIOPHENECARBOXYLATE nitr 5 NITR 5 TETRASODIUM SALT AURORA KA-6179 AURORA 1315 nitr 2

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