2H-INDOLE-2-THIONE, 5-BROMO-1,3-DIHYDRO- synthesis
- Product Name:2H-INDOLE-2-THIONE, 5-BROMO-1,3-DIHYDRO-
- CAS Number:848649-91-2
- Molecular formula:C8H6BrNS
- Molecular Weight:228.11
20870-78-4
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Yield:848649-91-2 85%
Reaction Conditions:
Stage #1: 5-bromo-2-indolin-2-onewith sodium hydrogencarbonate in tetrahydrofuran at 20;Inert atmosphere;Schlenk technique;
Stage #2: with tetraphosphorus decasulfide in tetrahydrofuran at 20;Inert atmosphere;Schlenk technique;
References:
Gopal, Braj;Singh, Prasoon Raj;Kumar, Madan;Goswami, Avijit [Journal of Organic Chemistry,2023,vol. 88,# 1,p. 132 - 142] Location in patent:supporting information
87-48-9
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