4'-NITRO-P-TOLUENESULFONANILIDE(734-25-8) IR1

Product Name4'-NITRO-P-TOLUENESULFONANILIDE

CAS 734-25-8

Molecular FormulaC13H12N2O4S

Molecular Weight292.31

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Mass

MS-IW-3686          
N-(p-nitrophenyl)-p-toluenesulfonamide
C13H12N2O4S         (Mass of molecular ion:    292)

   Source Temperature: 120 °C
   Sample Temperature: 100 °C
   Direct, 75 eV

      28.0       1.2
      30.0       4.4
      38.0       1.2
      39.0       4.6
      41.0       1.9
      51.0       2.1
      52.0       1.8
      53.0       1.0
      62.0       1.2
      63.0       6.5
      64.0       5.2
      65.0      18.1
      66.0       1.1
      77.0       1.7
      79.0       1.0
      89.0       3.5
      90.0       3.1
      91.0     100.0
      92.0       9.7
     107.0       2.4
     108.0       1.2
     138.0       1.3
     139.0       2.6
     155.0      68.0
     156.0       5.9
     157.0       3.6
     180.0       1.0
     292.0      36.3
     293.0       5.8
     294.0       2.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₃ H₁₂ N₂ O₄ S	0.035 g : 0.5 ml DMSO-d₆
N-(p-nitrophenyl)-p-toluenesulfonamide

    Assign.     Shift(ppm)

      A            11.3
      B             8.155
      C             7.791
      D             7.408
      E             7.339
      F             2.350

     Hz     ppm     Int.

   4505.53  11.274     54
   3263.84   8.167    344
   3254.87   8.145    365
   3118.23   7.803    330
   3110.17   7.783    366
   2964.37   7.418    334
   2956.31   7.398    305
   2947.70   7.376     25
   2947.15   7.375     25
   2946.60   7.373     25
   2937.62   7.351    362
   2928.65   7.329    346
    939.46   2.351   1000
    927.74   2.322     22

in DMSO-d6

KBr disc

nujol mull

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