ChemicalBook--->CAS DataBase List--->39562-22-6

39562-22-6

39562-22-6 Structure

39562-22-6 Structure
IdentificationMore
[Name]

2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
[CAS]

39562-22-6
[Synonyms]

2-METHOXYETHYL 2-(3-NITROBENZYLIDENE)ACETOACETATE
2-methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate
methoxyethyl 3-nitrobenzylidenacetoacetate
SALOR-INT L133884-1EA
2-Methoxyethyl-2-(3-nitrobenzyliden)acetoacetate
METHOXYRTHYL-3-NITROBENZYLIDENACETOACETATE
3-NITROBENZYLIDENEACETOACETATE-2-METHOXYETHYLESTER
(Z)-2-METHOXYETHYL 2-BENZYLIDENE-3-OXOBUTANOATE
2-[(3-Nitrophenyl)methylene]-3-oxobutanoic acid 2-methoxyethyl ester
2-Acetyl-3-(3-nitrophenyl)acrylic acid 2-methoxyethyl ester
[EINECS(EC#)]

254-511-0
[Molecular Formula]

C14H15NO6
[MDL Number]

MFCD00521048
[Molecular Weight]

293.27
[MOL File]

39562-22-6.mol
Chemical PropertiesBack Directory
[Melting point ]

72-74°C
[Boiling point ]

433.4±40.0 °C(Predicted)
[density ]

1.266±0.06 g/cm3(Predicted)
[storage temp. ]

Sealed in dry,2-8°C
[solubility ]

DMSO, Methanol
[form ]

Solid
[color ]

Off-White to Pale Yellow
[CAS DataBase Reference]

39562-22-6(CAS DataBase Reference)
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)Environment (GHS09)
GHS07,GHS09
[Signal word ]

Warning
[Hazard statements ]

H317-H410
[Precautionary statements ]

P261-P272-P280-P302+P352-P333+P313-P321-P363-P501-P273-P391-P501
[REACH Registrations]

Active
[HazardClass ]

IRRITANT
Hazard InformationBack Directory
[Hazard]

Low toxicity by ingestion and inhalation. A moderate eye irritant.
[Chemical Properties]

Off-White to Pale Yellow Solid
[Uses]

Cilnidipine intermediate.
[Synthesis]

200 kg of methoxyethyl acetoacetate and 185.1 kg of 3-nitrobenzaldehyde were suspended in 800 l of isopropanol. Then 5.65 kg of p-anisic acid and 5.05 kg of an ethanol solution of 33% dimethylamine were added and heated at about 35°C for about 30 minutes
Spectrum DetailBack Directory
[Spectrum Detail]

2-Methoxyethyl 2-[(3-nitrophenyl)methylene]acetoacetate(39562-22-6)1HNMR
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