| Identification | Back Directory | [Name]
(1,5-DIMETHYL-1H-PYRAZOL-3-YL)METHYLAMINE | [CAS]
423768-52-9 | [Synonyms]
AKOS B014394
AKOS PAO-0907
BUTTPARK 147\11-05
ART-CHEM-BB B016042
ART-CHEM-BB B014394
3-(AMinoMethyl)-1,5-diMethylpyrazole
(1,5-Dimethylpyrazol-3-yl)methanamine
3-(Aminomethyl)-1,5-dimethyl-1H-pyrazole
1H-Pyrazole-3-methanamine, 1,5-dimethyl-
(1,5-DiMethyl-1H-pyrazol-3-yl)MethanaMine
(1,5-DIMETHYL-1H-PYRAZOL-3-YL)METHYLAMINE
1H-Pyrazole-3-methanamine,1,5-dimethyl-(9CI)
3-(Aminomethyl)-1,5-dimethyl-1H-pyrazole 95+%
(1,5-Dimethyl-1H-pyrazol-3-yl)methylamine ,97% | [Molecular Formula]
C6H11N3 | [MDL Number]
MFCD03422531 | [MOL File]
423768-52-9.mol | [Molecular Weight]
125.17 |
| Chemical Properties | Back Directory | [Boiling point ]
94 °C | [density ]
1.12±0.1 g/cm3(Predicted) | [storage temp. ]
under inert gas (nitrogen or Argon) at 2–8 °C | [form ]
liquid | [pka]
8.26±0.29(Predicted) | [color ]
Colourless to light yellow | [InChI]
1S/C6H11N3/c1-5-3-6(4-7)8-9(5)2/h3H,4,7H2,1-2H3 | [InChIKey]
JGYXJOBBROGMLL-UHFFFAOYSA-N | [SMILES]
Cc1cc(CN)nn1C |
| Hazard Information | Back Directory | [Synthesis]
1,5-Dimethyl-1H-pyrazole-3-carboxamide was used as starting material and dissolved in 70 mL of tetrahydrofuran (THF) at 0 °C. Subsequently, lithium aluminum hydride (LiAlH4, 4.1 g, 107.89 mmol) was added in batches. The reaction mixture was heated to reflux for 1 hour. Upon completion of the reaction, solid impurities were removed by filtration and the filtrate was concentrated to afford (1,5-dimethyl-1H-pyrazol-3-yl)methanamine in the form of a yellow oil in a yield of 3 g and 67%. | [References]
[1] Patent: WO2009/139834, 2009, A1. Location in patent: Page/Page column 129 |
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