| Identification | More | [Name]
9-AMINOFLUORENE HYDROCHLORIDE | [CAS]
5978-75-6 | [Synonyms]
9-AMINOFLUORENE HCL
9-AMINOFLUORENE HYDROCHLORIDE
9-FLUORENAMINE HYDROCHLORIDE
9H-FLUOREN-9-AMINE, HYDROCHLORIDE
FLUOREN-9-AMINE HCL SALT
TIMTEC-BB SBB003370
9-Aminofluorene hydrochloride,99%
9-FluorenylamineHCl
9-fluorenylamine hydrochloride
9-AMINOFLUORENE HYDROCHLORIDE 99% | [EINECS(EC#)]
227-778-6 | [Molecular Formula]
C13H12ClN | [MDL Number]
MFCD00012536 | [Molecular Weight]
217.69 | [MOL File]
5978-75-6.mol |
| Chemical Properties | Back Directory | [Appearance]
WHITE TO BEIGE CRYSTALLINE POWDER | [Melting point ]
265-270 °C (dec.)(lit.) | [storage temp. ]
Inert atmosphere,Room Temperature | [form ]
powder to crystal | [color ]
White to Light yellow | [Sensitive ]
Hygroscopic | [BRN ]
3915368 | [InChI]
InChI=1S/C13H11N.ClH/c14-13-11-7-3-1-5-9(11)10-6-2-4-8-12(10)13;/h1-8,13H,14H2;1H | [InChIKey]
SYKJOJSYQSVNOM-UHFFFAOYSA-N | [SMILES]
C1(N)C2=C(C=CC=C2)C2=C1C=CC=C2.[H]Cl | [CAS DataBase Reference]
5978-75-6(CAS DataBase Reference) |
| Safety Data | Back Directory | [Risk Statements ]
R36/37/38:Irritating to eyes, respiratory system and skin . | [Safety Statements ]
S24/25:Avoid contact with skin and eyes . | [WGK Germany ]
3
| [RTECS ]
LL5130000 | [PackingGroup ]
III | [HS Code ]
2921490090 |
| Hazard Information | Back Directory | [Chemical Properties]
WHITE TO BEIGE CRYSTALLINE POWDER | [Synthesis]
In the first step, 9-fluorenone oxime (400 mg) was mixed with a solution of concentrated hydrochloric acid (0.86 mL) in ethanol (50 mL), 10% Pd/C catalyst (33 mg) was added, and the hydrogenation reaction was carried out at atmospheric pressure. Upon completion of the reaction, the reaction mixture was filtered to remove the catalyst and the filtrate was concentrated. The concentrated residue was suspended in ethyl acetate and filtered again to give 9-aminofluorene hydrochloride (240 mg) as a white solid. | [References]
[1] Patent: EP2511283, 2012, A1. Location in patent: Page/Page column 92-93
[2] Patent: US2013/45942, 2013, A1. Location in patent: Paragraph 0390
[3] Patent: JP2015/172077, 2015, A. Location in patent: Paragraph 0190 |
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| Company Name: |
Alfa Aesar
|
| Tel: |
400-6106006 |
| Website: |
http://chemicals.thermofisher.cn |
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