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831203-13-5

831203-13-5 Structure

831203-13-5 Structure
IdentificationMore
[Name]

5-Bromo-2-chloro-3-fluoropyridine
[CAS]

831203-13-5
[Synonyms]

5-BROMO-2-CHLORO-3-FLUOROPYRIDINE
[Molecular Formula]

C5H2BrClFN
[MDL Number]

MFCD03411574
[Molecular Weight]

210.43
[MOL File]

831203-13-5.mol
Questions And AnswerBack Directory
[Synthesis]

The suspension of 5-bromo-3-fluoro-2-hydroxypyridine (10.0 g) in phosphoric acid chloride (50 mL) was heated at 150 °C for 4 hours. The mixture was poured onto ice, and the pH of the resulting mixture was adjusted to 10 by adding potassium carbonate. The mixture was then extracted with dichloromethane. The organic extract was dried over anhydrous magnesium sulfate, filtered, and then concentrated under vacuum to obtain the target product.

Synthesis of 831203-13-5

Figure 2: Synthetic route of 5-Bromo-2-chloro-3-fluoropyridine

Chemical PropertiesBack Directory
[Melting point ]

50-52℃
[Boiling point ]

195.3±35.0 °C(Predicted)
[density ]

1.829±0.06 g/cm3(Predicted)
[storage temp. ]

Inert atmosphere,2-8°C
[form ]

Solid
[pka]

-2.44±0.10(Predicted)
[color ]

White
[CAS DataBase Reference]

831203-13-5(CAS DataBase Reference)
Safety DataBack Directory
[Symbol(GHS) ]

Exclamation Mark (GHS07)
GHS07
[Signal word ]

Warning
[Hazard statements ]

H315-H319-H335
[Precautionary statements ]

P261-P280a-P304+P340-P305+P351+P338-P405-P501a
[Hazard Codes ]

Xi
[Risk Statements ]

22-37/38-41
[Safety Statements ]

26-39
[HazardClass ]

IRRITANT
[HS Code ]

2933399990
Hazard InformationBack Directory
[Uses]

5-Bromo-2-chloro-3-fluoropyridine is an important organic chemical with a high reactivity that can be used in chemoselective amination reactions. It is also used as a pharmaceutical intermediate.
Spectrum DetailBack Directory
[Spectrum Detail]

5-Bromo-2-chloro-3-fluoropyridine(831203-13-5)1HNMR
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