4-硝基苄基羟胺盐酸盐
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- CAS号:
- 2086-26-2
- 英文名:
- O-(4-NITROBENZYL)HYDROXYLAMINE HYDROCHLORIDE
- 英文别名:
- PNBA;TIMTEC-BB SBB003507;4-nitrobenzyloxyamine;O-(4-Nitrobenzyl)hydroxylamineHCl;P-NITROBENZYLOXYAMINE HYDROCHLORIDE;4-NITROBENZYLOXYAMINE HYDROCHLORIDE;4-Nitrobenzylhydroxylamine hydrochloride;O-(4-NITROBENZYL)-HYDROXYLAMMONIUM CHLORIDE;O-(4-NITROBENZYL)HYDROXYLAMINE HYDROCHLORIDE;O-(4-Nitrobenzyl)hydroxylammoniumhydrochlorid
- 中文名:
- 4-硝基苄基羟胺盐酸盐
- 中文别名:
- 对硝基苄氧胺盐酸盐;4-硝基苄基羟胺盐酸盐;O-(4-硝基苄基)羟胺;O-(4-硝基苄基)羟胺盐酸盐;O-(4-硝基苯基)羟胺盐酸盐;O-(4-硝基苄基)羟胺盐酸盐,98%;O-(4-硝基苄基)羟胺盐酸盐, 衍生化试剂;O-4-硝基苄基羟胺盐酸盐 [HPLC标记用];O-4-硝基苄基羟胺盐酸盐 [HPLC标记用];O-(4-硝基苄基)羟胺盐酸盐[用于高效液相色谱标记]
- CBNumber:
- CB5431153
- 分子式:
- C7H9ClN2O3
- 分子量:
- 204.61
- MOL File:
- 2086-26-2.mol
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4-硝基苄基羟胺盐酸盐性质、用途与生产工艺
以2-((4-硝基苄基)氧基)异吲哚啉-1,3-二酮为原料合成4-硝基苄基羟胺盐酸盐的一般步骤：将化合物18（2.00 g，6.71 mmol）悬浮于EtOH（10 mL）中，磁力搅拌下缓慢加入浓盐酸水溶液（20 mL）。将反应混合物加热回流3小时。反应完成后，稍冷却，加入H2O（30 mL），随后用CHCl3（20 mL×1）洗涤。分离水相，减压浓缩，得到4-硝基苄基羟胺盐酸盐19（1.37 g，定量收率），为乳白色固体，熔点179.1-205.9℃（文献值217℃）。1H NMR（300 MHz，DMSO-d6）δ11.37（br s，2H），8.26（d，J=8.6 Hz，2H），7.68（d，J=8.6 Hz，2H），5.22（s，2H）。
参考文献：
[1] Patent: WO2008/124878, 2008, A1. Location in patent: Page/Page column 42
[2] Patent: US2014/378399, 2014, A1. Location in patent: Paragraph 0122
[3] MedChemComm, 2013, vol. 4, # 8, p. 1156 - 1165
[4] European Journal of Medicinal Chemistry, 2016, vol. 108, p. 564 - 576
[5] Arkivoc, 2018, vol. 2018, # 4, p. 139 - 148
用途
衍生化试剂
4-硝基苄基羟胺盐酸盐
上下游产品信息
上游原料
下游产品
| 更新日期 | 产品编号 | 产品名称 | CAS编号 | 包装 | 价格 |
|---|
| 2025/05/22 | L05861 | O-(4-硝基苄基)羟胺盐酸盐, 98%
O-(4-Nitrobenzyl)hydroxylamine hydrochloride, 98% | 2086-26-2 | 1g | 418元 |
| 2025/05/22 | L05861 | O-(4-硝基苄基)羟胺盐酸盐, 98%
O-(4-Nitrobenzyl)hydroxylamine hydrochloride, 98% | 2086-26-2 | 5g | 1510元 |
4-硝基苄基羟胺盐酸盐
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4-硝基苄基羟胺盐酸盐国内生产厂家
2086-26-2, 4-硝基苄基羟胺盐酸盐 相关搜索:
- UV Detection (HPLC Labeling Reagents)
- Hydroxylamines (O-Substituted)
- Hydroxylamines
- HPLC Labeling Reagents
- Carbonyl Group Labeling Reagents for HPLC
- Analytical Chemistry
- Pharmaceuticals
- Intermediates & Fine Chemicals
- Aromatics
- Amines
- 高端化学
- 有机中间体
- 苯类
- 合成
- Nitrogen Compounds
- Hydroxylamines
- HPLC Labeling Reagents
- UV Detection (HPLC Labeling Reagents)
- Carbonyl Group Labeling Reagents for HPLC
- Hydroxylamines (O-Substituted)
- Building Blocks
- Organic Building Blocks
- O2NC6H4CH2ONH2HCl
- C7H8N2O3HCl
- O-4-硝基苄基羟胺盐酸盐 [HPLC标记用]
- O-4-硝基苄基羟胺盐酸盐 [HPLC标记用]
- O-4-硝基苄基羟胺盐酸盐[用于高效液相色谱标记](易制爆,甄准不供应)
- O-(4-硝基苄基)羟胺盐酸盐, 衍生化试剂
- O-(4-硝基苯基)羟胺盐酸盐
- 4-硝基苄基羟胺盐酸盐
- O-(4-硝基苄基)羟胺盐酸盐
- O-(4-硝基苄基)羟胺盐酸盐[用于高效液相色谱标记]
- O-(4-硝基苄基)羟胺盐酸盐,98%
- O-(4-硝基苄基)羟胺
- O-4-硝基苄基羟胺盐酸盐(>99.0%(HPLC),用于高效液相色谱标记)
- 对硝基苄氧胺盐酸盐
- 2086-26-2
- 4-Nitrobenzylhydroxylamine hydrochloride
- O-(4-Nitrobenzyl)hydroxylamine hydrochloride
- Hydroxylamine,O-[(4-nitrophenyl)methyl]-, hydrochloride (1:1)
- O-4-Nitrobenzylhydroxylamine Hydrochloride [for HPLC Labeling]>
- O-(4-Nitrobenzyl)hydroxylammoniumhydrochlorid
- O-(4-NITROBENZYL)- HYDROXYLAMINE HYDROCHLORIDE 98%
- O-(4-Nitrobenzyl)hydroxylamine hydrochloride, 98%, derivatization grade
- O-[(4-nitrophenyl)methyl]hydroxylamine chloride
- 4-NITROBENZYLOXYAMINE HYDROCHLORIDE
- 1-[(AMMONIOOXY)METHYL]-4-NITROBENZENE CHLORIDE
- 1-[(AMINOOXY)METHYL]-4-NITROBENZENE HYDROCHLORIDE
- o-[(4-nitrophenyl)methyl]-hydroxylaminmonohydrochloride
- o-(p-nitrophenylmethyl)-hydroxylaminmonohydrochloride
- 4-nitrobenzyloxyamine
- O-(4-Nitrobenzyl)-hydroxylammonium chloride for synthesis
- O-(4-Nitrobenzyl)hydroxylamine hydrochloride≥ 99%(Titration)
- O-[(4-nitrophenyl)Methyl]hydroxylaMine Hydrochloride
- O-(p-Nitrobenzyl)hydroxylaMine Monohydrochloride
- O-(4-Nitrobenzyl)hydroxylamine hydrochloride >=98.5% (AT)
- O-(4-Nitrobenzyl)hydroxylamine hydrochloride,98%
- O-(4-Nitrobenzyl)hydroxylamineHCl