Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat

D-Lysergic Acid Methyl Ester Struktur
4579-64-0
CAS-Nr.
4579-64-0
Bezeichnung:
Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat
Englisch Name:
D-Lysergic Acid Methyl Ester
Synonyma:
Methyl Ergoline Acid;methyl lysergate;D-Lysergic Acid Methyl Ester;NSC 157966;Lysergic acid methyl;Methyl Lysergic Acid;Methyl Ergoline Acid, 10 mM in DMSO;methyl 9,10-didehydro-6-methylergoline-8;D-Lysergic acid N,N-diethylamide tartrate;methyl 9,10-didehydro-6-methylergoline-8β-carboxylate
CBNumber:
CB0386447
Summenformel:
C17H18N2O2
Molgewicht:
282.34
MOL-Datei:
4579-64-0.mol

Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat Eigenschaften

Schmelzpunkt:
164-166 °C(Solv: benzene (71-43-2))
Siedepunkt:
469.0±45.0 °C(Predicted)
Dichte
1.30±0.1 g/cm3(Predicted)
storage temp. 
-20°C Freezer
Löslichkeit
Chloroform (Slightly), DMSO (Slightly), Methanol (Slightly)
Aggregatzustand
Solid
pka
17.25±0.40(Predicted)
Farbe
Pale Grey to Black
InChI
InChI=1/C17H18N2O2/c1-19-9-11(17(20)21-2)6-13-12-4-3-5-14-16(12)10(8-18-14)7-15(13)19/h3-6,8,11,15,18H,7,9H2,1-2H3/t11?,15-/s3
InChIKey
RNHDWLRHUJZABX-RXHCFGRJNA-N
SMILES
C12C3C=CC=C4NC=C(C[C@@]1([H])N(C)CC(C(OC)=O)C=2)C=34 |&1:10,r|

Sicherheit

Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat Chemische Eigenschaften,Einsatz,Produktion Methoden

Beschreibung

Lysergic acid methyl ester is an analogue of lysergic acid diethylamide (LSD). It is a member of the tryptamine family and is extremely uncommon. It acts on the 5-HT receptors in the brain, as do most tryptamines.

Verwenden

D-Lysergic Acid Methyl Ester is used in preparation of Serotonin agonists.It is an impurity of Lysergic Acid (L488000). Lysergic Acid and Iso-lysergic Acid are the main cleavage products formed on alkaline hydrolysis of the alkaloids which are characteristic of ergot. Potent hallucinogen; non-selective serotonin receptor agonist.

synthetische

synthesis of lysergic acid methyl ester: A suspension is prepared from 5.0 g of isolysergic acid amide in 80 ml of anhydrous methanol; the mixture is cooled to about -50°C and, under agitation, 40 ml of a 13N solution of hydrogen chloride in anhydrous methanol is added thereto. The clear solution is allowed to warm up to room temperature and further stirred overnight. The primary amount of the thus-formed ester hydrochloride is thus crystallized. By cooling in an ice bath and adding ethyl acetate, the crystallization is completed, and the precipitate is vacuum-filtered. Yield: 5.2 g (84% of theory) of lysergic acid methyl ester, hydrochloride.

Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat Upstream-Materialien And Downstream Produkte

Upstream-Materialien

Downstream Produkte


Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat Anbieter Lieferant Produzent Hersteller Vertrieb Händler.

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4579-64-0(Methyl-9,10-didehydro-6-methylergolin-8β-carboxylat)Verwandte Suche:


  • Methyl Ergoline Acid
  • 9,10-DIDEHYDRO-6-METHYL-ERGOLINE-8-CARBOXYLIC ACID METHYL ESTER
  • methyl 9,10-didehydro-6-methylergoline-8beta-carboxylate
  • Lysergic acid methyl
  • D-Lysergic Acid Methyl Ester
  • Methyl Lysergic Acid
  • methyl 9,10-didehydro-6-methylergoline-8
  • methyl 9,10-didehydro-6-methylergoline-8β-carboxylate
  • methyl lysergate
  • Methyl (6aR,9R)-7-methyl-4,6,6a,7,8,9-hexahydroindolo[4,3-fg]quinoline-9-carboxylate
  • NSC 157966
  • Ergoline-8-carboxylic acid, 9,10-didehydro-6-methyl-, methyl ester, (8β)-
  • D-Lysergic acid N,N-diethylamide tartrate
  • methyl (7R)-6-methyl-6,11-diazatetracyclo[7.6.1.0?2,a?·.0?1?2,?1a??]hexadeca-1(16),2,9,12,14-pentaene-4-carboxylate
  • Methyl Ergoline Acid, 10 mM in DMSO
  • 4579-64-0
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