9-Bromo-10-phenylanthracene
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- CAS-Nr.
- 23674-20-6
- Englisch Name:
- 9-Bromo-10-phenylanthracene
- Synonyma:
- 9-Bromo-10-phenyl;Afatinib/Afatinib;9-Bromo-10-phenylant;9-bromo-10-phenylindole;9-Bromo-1-phenylanthracene;10-phenyl-9-BroMoanthracene;9-Bromo-10-phenylanthracene;10-broMo-9-phenylanthracene;9-bromo-10-phenylanthrancene;Anthracene, 9-Bromo-10-phenyl
- CBNumber:
- CB61089413
- Summenformel:
- C20H13Br
- Molgewicht:
- 333.22
- MOL-Datei:
- 23674-20-6.mol
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9-Bromo-10-phenylanthracene Eigenschaften
- Schmelzpunkt:
- 154-155 °C
- Siedepunkt:
- 449.7±14.0 °C(Predicted)
- Dichte
- 1.393
- storage temp.
- Sealed in dry,Room Temperature
- Löslichkeit
- Chloroform, Methanol (Slightly)
- Aggregatzustand
- Powder
- Farbe
- Pale yellow
- Wasserlöslichkeit
- Insoluble in water. Soluble in hot toluene, dimethylformamide.
- InChI
- InChI=1S/C20H13Br/c21-20-17-12-6-4-10-15(17)19(14-8-2-1-3-9-14)16-11-5-7-13-18(16)20/h1-13H
- InChIKey
- WHGGVVHVBFMGSG-UHFFFAOYSA-N
- SMILES
- C1=C2C(C(C3=CC=CC=C3)=C3C(=C2Br)C=CC=C3)=CC=C1
Sicherheit
- Risiko- und Sicherheitserklärung
- Gefahreninformationscode (GHS)
| S-Sätze: |
24/25 |
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| HS Code |
29039990 |
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| Bildanzeige (GHS) |
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| Alarmwort |
Warnung
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| Gefahrenhinweise |
| Code |
Gefahrenhinweise |
Gefahrenklasse |
Abteilung |
Alarmwort |
Symbol |
P-Code |
| H302 |
Gesundheitsschädlich bei Verschlucken. |
Akute Toxizität oral |
Kategorie 4 |
Warnung |
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P264, P270, P301+P312, P330, P501 |
| H315 |
Verursacht Hautreizungen. |
Hautreizung |
Kategorie 2 |
Warnung |
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P264, P280, P302+P352, P321,P332+P313, P362 |
| H317 |
Kann allergische Hautreaktionen verursachen. |
Sensibilisierung der Haut |
Kategorie 1A |
Warnung |
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P261, P272, P280, P302+P352,P333+P313, P321, P363, P501 |
| H319 |
Verursacht schwere Augenreizung. |
Schwere Augenreizung |
Kategorie 2 |
Warnung |
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P264, P280, P305+P351+P338,P337+P313P |
| H335 |
Kann die Atemwege reizen. |
Spezifische Zielorgan-Toxizität (einmalige Exposition) |
Kategorie 3 (Atemwegsreizung) |
Warnung |
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| Sicherheit |
| P261 |
Einatmen von Staub vermeiden. |
| P304+P340 |
BEI EINATMEN: Die Person an die frische Luft bringen und für ungehinderte Atmung sorgen. |
| P305+P351+P338 |
BEI KONTAKT MIT DEN AUGEN: Einige Minuten lang behutsam mit Wasser spülen. Eventuell vorhandene Kontaktlinsen nach Möglichkeit entfernen. Weiter spülen. |
| P405 |
Unter Verschluss aufbewahren. |
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9-Bromo-10-phenylanthracene Chemische Eigenschaften,Einsatz,Produktion Methoden
Beschreibung
9-Bromo-10-phenylanthracene is a yellow-white solid powder that is commonly used as an organic synthesis intermediate.It is not soluble in water but can dissolve in dimethyl sulfoxide, N,N-dimethylformamide, and other polar solvents. It is also soluble in hot non-polar solvents due to its low polarity.
Chemische Eigenschaften
Pale yellow powder
Verwenden
It is used as an OLED material.
synthetische
9-Phenylanthracene (2.5g, 9.83mmol) and NBS (2.1g, 11.8mmol) were dissolved in 80mL CHCl3. Then the mixture was heated to 60°C for 2h under N2. After cooled to room temperature, 20 mL water was added. And the mixture was extracted with CH2Cl2. The organic extracts were dried over anhydrous MgSO4 and concentrated by rotary evaporation.The crude product was recrystallized from methanol to get a green-yellow powder (2g, 61.2%). 1H NMR (500 MHz, CDCl3) δ 8.67 – 8.61 (m, 2H), 7.71 – 7.65 (m, 2H), 7.64 – 7.56 (m, 5H), 7.45 – 7.37 (m, 4H). EI-MS (m/z): Calculated for C20H13Br: 333.22. Found [M+]: 332.30.
Synthesis of 9-bromo-10-phenylanthracene
9-Bromo-10-phenylanthracene Upstream-Materialien And Downstream Produkte
Upstream-Materialien
Downstream Produkte
9-Bromo-10-phenylanthracene Anbieter Lieferant Produzent Hersteller Vertrieb Händler.
Global( 273)Lieferanten
23674-20-6()Verwandte Suche:
- Anthracene, 9-Bromo-10-phenyl
- 9-Bromo-10-phenylanthracene
- 10-phenyl-9-BroMoanthracene
- 9-Bromo-10-phenylant
- 10-broMo-9-phenylanthracene
- 9-bromo-10-phenylindole
- 9-bromo-10-phenylanthrancene
- 9-Bromo-10-phenyl
- 9-Bromo-10-phenylanthracene >
- 9-Bromo-10-phenylanthracene,98%
- 9-Bromo-10-phenylanthracene ISO 9001：2015 REACH
- 9-Bromo-1-phenylanthracene
- Afatinib/Afatinib
- 23674-20-6
- C20H13Br
- organic chemicals and derivatives/others
- OLED
