(4-Bromo-2-methylphenyl)methanamine hydrochloride
- CAS No.
- 1171381-49-9
- Chemical Name:
- (4-Bromo-2-methylphenyl)methanamine hydrochloride
- Synonyms
- 4-BroMo-2-Methyl benzylaMine HCl;(4-Bromo-2-methylphenyl)methanamine hydrochloride
- CBNumber:
- CB03161968
- Molecular Formula:
- C8H11BrClN
- Molecular Weight:
- 236.53664
- MDL Number:
- MFCD11045167
- MOL File:
- 1171381-49-9.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H315-H319-H335 |
| Precautionary statements | P261-P305+P351+P338 |
| HS Code | 2921490090 |
(4-Bromo-2-methylphenyl)methanamine hydrochloride price
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Apolloscientific | OR3058 | 4-Bromo-2-methylbenzylamine hydrochloride >97% | 1171381-49-9 | 100mg | $21 | 2026-06-04 | Buy |
| Apolloscientific | OR3058 | 4-Bromo-2-methylbenzylamine hydrochloride >97% | 1171381-49-9 | 250mg | $32 | 2026-06-04 | Buy |
| Apolloscientific | OR3058 | 4-Bromo-2-methylbenzylamine hydrochloride >97% | 1171381-49-9 | 1g | $67 | 2026-06-04 | Buy |
| Apolloscientific | OR3058 | 4-Bromo-2-methylbenzylamine hydrochloride >97% | 1171381-49-9 | 5g | $195 | 2026-06-04 | Buy |
| Activate Scientific | AS47048 | (4-Bromo-2-methylphenyl)methanamine hydrochloride 97% | 1171381-49-9 | 1g | $112 | 2026-06-04 | Buy |
(4-Bromo-2-methylphenyl)methanamine hydrochloride Chemical Properties,Uses,Production
Synthesis
67832-11-5
1171381-49-9
The general procedure for the synthesis of (4-bromo-2-methylphenyl)methanamine hydrochloride from 4-bromo-2-methylbenzonitrile was as follows: to a solution of 4-bromo-2-methylbenzenecarbonitrile (3 g, 15 mmol) in tetrahydrofuran (THF, 20 mL) was slowly added borane-tetrahydrofuran complex (BH3-THF, 45 mL, 45 mmol). The reaction mixture was stirred at 0 °C for 1 h. The temperature was gradually increased to 80 °C and the reaction was maintained for 16 hours. After completion of the reaction, the reaction was quenched with methanol (MeOH). After concentration under reduced pressure to remove the solvent, the residue was treated with saturated hydrogen chloride/ethyl acetate (HCl/EtOAc) solution with stirring and subsequently filtered. The resulting solid was washed with ether (20 mL x 3) and finally dried under vacuum to afford the target product (4-bromo-2-methylphenyl)methylamine hydrochloride (3.2 g, yield: 90%) as a white solid. Electrospray ionization mass spectrometry (ESI-MS) showed molecular ion peak (M + H)+: 200.1.
References
[1] Patent: WO2016/201280, 2016, A1. Location in patent: Paragraph 0655; 0656
(4-Bromo-2-methylphenyl)methanamine hydrochloride Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Adamas Reagent, Ltd. | 400-6009262 15618770481 | yhx@titansci.com | China | 14098 | 59 |
| Tianjin Derchemist Science & Technology Co., Ltd. | 22-58627059 13920586291 | zdcomcon@126.com | China | 4094 | 50 |
| Nanjing Norris-Pharm Technology Co., Ltd | 13901585132 | sales@norris-pharm.com | China | 8869 | 55 |
| Shanghai YuanYe Biotechnology Co., Ltd. | 15026964105 | 2881489226@qq.com | China | 89667 | 60 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Aikon International Limited | 025-58859352 15955137747 | sales01@aikonchem.com | China | 16021 | 58 |
| Suzhou Xiya Pharmaceutical Co., Ltd. | 0512-87819718 18912655635 | 2587879032@qq.com | China | 1279 | 58 |
| Nanjing Pope Bio-tech R&D Co., Ltd | 025-87138562 18951783565 | sales@popebiotech.com | China | 414 | 58 |
| Shanghai Jizhi Biochemical Technology Co. Ltd. | 021-4009004166/18616739031 18616739031 | 3007523370@qq.com | China | 40000 | 58 |
| Shanghai Thunder Biological Technology Co., Ltd. | 18621609968 | 1162686636@qq.com | China | 1028 | 58 |
