N-(3-Bromophenyl)methansulfonamide
- CAS No.
- 83922-51-4
- Chemical Name:
- N-(3-Bromophenyl)methansulfonamide
- Synonyms
- N-(3-Bromophenyl)methansulfonamide;3-BROMO PHENYL METHANE SULPHONAMIDE;3-(methylsulfonyl)amino-1-bromo-benzene
- CBNumber:
- CB22130976
- Molecular Formula:
- C7H8BrNO2S
- Molecular Weight:
- 250.11
- MDL Number:
- MFCD01213915
- MOL File:
- 83922-51-4.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| N-(3-Bromophenyl)methanesulfonamide | B698330 | 1g | $75 |
| N-(3-BROMOPHENYL)METHANESULFONAMIDE | BP-21291 | 1g | $106 |
| N-(3-Bromophenyl)methansulfonamide | X5390 | 5g | $192 |
| N-(3-Bromophenyl)methanesulfonamide | 8669-9-57 | 1g | $245 |
| METHANESULFONAMIDE, N-(3-BROMOPHENYL)- 95.00% | HCH0137515 | 1G | $721.57 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) | ![]() GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319 |
| Precautionary statements | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 |
| HS Code | 2935909099 |
N-(3-Bromophenyl)methansulfonamide price More Price(16)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | B698330 | N-(3-Bromophenyl)methanesulfonamide | 83922-51-4 | 1g | $75 | 2021-12-16 | Buy |
| BroadPharm | BP-21291 | N-(3-BROMOPHENYL)METHANESULFONAMIDE | 83922-51-4 | 1g | $106 | 2021-12-16 | Buy |
| AK Scientific | X5390 | N-(3-Bromophenyl)methansulfonamide | 83922-51-4 | 5g | $192 | 2021-12-16 | Buy |
| SynQuest Laboratories | 8669-9-57 | N-(3-Bromophenyl)methanesulfonamide | 83922-51-4 | 1g | $245 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0137515 | METHANESULFONAMIDE, N-(3-BROMOPHENYL)- 95.00% | 83922-51-4 | 1G | $721.57 | 2021-12-16 | Buy |
N-(3-Bromophenyl)methansulfonamide Chemical Properties,Uses,Production
Synthesis
124-63-0
591-19-5
83922-51-4
Step i: To a stirred solution of anhydrous dichloromethane (200 ml) of m-bromoaniline (6 g, 34.87 mmol) was sequentially added pyridine (4.13 mg, 52.31 mmol) and methanesulfonyl chloride (5.194 g, 45.34 mmol) at 10 °C. The reaction mixture was stirred at room temperature for 15 h. The progress of the reaction was monitored by thin layer chromatography (TLC, the unfolding agent was a hexane solution of 35% ethyl acetate). After completion of the reaction, the reaction mixture was diluted with dichloromethane (50 ml) and washed with 1N hydrochloric acid (25 ml). The organic layer was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give N-(3-bromophenyl)methane sulfonamide 8.45 g in 96.3% yield. The product was structurally confirmed by 1H NMR (DMSO-d6, 300 MHz) and mass spectrometry (MS: m/z = 251.8 [M + 1]).
References
[1] Patent: WO2014/6554, 2014, A1. Location in patent: Page/Page column 28
[2] Synthetic Communications, 2004, vol. 34, # 20, p. 3807 - 3819
[3] Patent: WO2017/18803, 2017, A1. Location in patent: Paragraph 791; 792; 793
[4] Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1982, vol. 38, # 7, p. 791 - 796
[5] Heterocycles, 2001, vol. 54, # 1, p. 105 - 108
N-(3-Bromophenyl)methansulfonamide Preparation Products And Raw materials
Raw materials
Preparation Products
N-(3-Bromophenyl)methansulfonamide Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
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| DAYANG CHEM (HANGZHOU) CO.,LTD | +86-88938639 +86-17705817739 | info@dycnchem.com | China | 53802 | 58 |
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| Amatek Scientific Co. Ltd. | 0512-56316828 4008675858 | sales@amateksci.com | China | 9859 | 55 |
| Bide Pharmatech Ltd. | 400-400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
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