N-(3-Bromophenyl)methansulfonamide
- CAS No.
- 83922-51-4
- Chemical Name:
- N-(3-Bromophenyl)methansulfonamide
- Synonyms
- N-(3-Bromophenyl)methansulfonamide;3-BROMO PHENYL METHANE SULPHONAMIDE;3-(methylsulfonyl)amino-1-bromo-benzene
- CBNumber:
- CB22130976
- Molecular Formula:
- C7H8BrNO2S
- Molecular Weight:
- 250.11
- MDL Number:
- MFCD01213915
- MOL File:
- 83922-51-4.mol
- MSDS File:
- SDS
- TDS File:
- TDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) | ![]() GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319 |
| Precautionary statements | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 |
| HS Code | 2935909099 |
N-(3-Bromophenyl)methansulfonamide price More Price(35)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Biosynth | IDA92251 | N-(3-Bromophenyl)methanesulfonamide | 83922-51-4 | 10g | $472 | 2026-06-04 | Buy |
| Activate Scientific | AS43968 | N-(3-Bromophenyl)methanesulfonamide 98% | 83922-51-4 | 1g | $49 | 2026-06-04 | Buy |
| Activate Scientific | AS43968 | N-(3-Bromophenyl)methanesulfonamide 98% | 83922-51-4 | 5g | $199 | 2026-06-04 | Buy |
| Activate Scientific | AS43968 | N-(3-Bromophenyl)methanesulfonamide 98% | 83922-51-4 | 25g | $472 | 2026-06-04 | Buy |
| Apolloscientific | OR322586 | N-(3-Bromophenyl)methanesulfonamide 95% | 83922-51-4 | 1g | $83 | 2026-06-04 | Buy |
N-(3-Bromophenyl)methansulfonamide Chemical Properties, Uses, Production
Synthesis
124-63-0
591-19-5
83922-51-4
Step i: To a stirred solution of anhydrous dichloromethane (200 ml) of m-bromoaniline (6 g, 34.87 mmol) was sequentially added pyridine (4.13 mg, 52.31 mmol) and methanesulfonyl chloride (5.194 g, 45.34 mmol) at 10 °C. The reaction mixture was stirred at room temperature for 15 h. The progress of the reaction was monitored by thin layer chromatography (TLC, the unfolding agent was a hexane solution of 35% ethyl acetate). After completion of the reaction, the reaction mixture was diluted with dichloromethane (50 ml) and washed with 1N hydrochloric acid (25 ml). The organic layer was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give N-(3-bromophenyl)methane sulfonamide 8.45 g in 96.3% yield. The product was structurally confirmed by 1H NMR (DMSO-d6, 300 MHz) and mass spectrometry (MS: m/z = 251.8 [M + 1]).
References
[1] Patent: WO2014/6554, 2014, A1. Location in patent: Page/Page column 28
[2] Synthetic Communications, 2004, vol. 34, # 20, p. 3807 - 3819
[3] Patent: WO2017/18803, 2017, A1. Location in patent: Paragraph 791; 792; 793
[4] Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1982, vol. 38, # 7, p. 791 - 796
[5] Heterocycles, 2001, vol. 54, # 1, p. 105 - 108
N-(3-Bromophenyl)methansulfonamide Preparation Products And Raw materials
Raw materials
Preparation Products
N-(3-Bromophenyl)methansulfonamide Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Beijing Ouhe Technology Co., Ltd | 13552068683 13522913783 | 2355560935@qq.com | China | 11777 | 60 |
| Amatek Scientific Co. Ltd. | 0512-56316828 4008675858 | sales@amateksci.com | China | 9848 | 55 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Beijing FYF Chemicals Co., Ltd | 010-57903446 15869909019 | 168931144@qq.com | China | 2876 | 58 |
| Cool Pharm, Ltd | 021-60455363 18019463053 | sales@coolpharm.com | China | 8455 | 58 |
| Watson Biotechnology Co.,Ltd | 027-59207879 1972026995 18140587686 | sales@3600chem.com | China | 4175 | 55 |
| Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd | 18210788515; 18210788515 | zhuzixin999@163.c0m | China | 4999 | 55 |
| Yantai ShengKailun Chemical Technology Co., Ltd. | 13356901049 | 3119594100@qq.com | China | 7964 | 55 |
| Aikon International Limited | 025-58859352 19370895928 | sales01@aikonchem.com | China | 15078 | 58 |
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