ChemicalBook >> CAS DataBase List >>N-(3-Bromophenyl)methansulfonamide

N-(3-Bromophenyl)methansulfonamide

CAS No.
83922-51-4
Chemical Name:
N-(3-Bromophenyl)methansulfonamide
Synonyms
N-(3-Bromophenyl)methansulfonamide;3-BROMO PHENYL METHANE SULPHONAMIDE;3-(methylsulfonyl)amino-1-bromo-benzene
CBNumber:
CB22130976
Molecular Formula:
C7H8BrNO2S
Molecular Weight:
250.11
MDL Number:
MFCD01213915
MOL File:
83922-51-4.mol
MSDS File:
SDS
TDS File:
TDS
Last updated:2026-05-28 00:00:51

N-(3-Bromophenyl)methansulfonamide Properties

Boiling point 330.7±44.0 °C(Predicted)
Density 1.711±0.06 g/cm3(Predicted)
storage temp. Sealed in dry,Room Temperature
pka 7.47±0.10(Predicted)
Appearance White to gray Solid

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313
HS Code  2935909099

N-(3-Bromophenyl)methansulfonamide price More Price(35)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Biosynth IDA92251 N-(3-Bromophenyl)methanesulfonamide 83922-51-4 10g $472 2026-06-04 Buy
Activate Scientific AS43968 N-(3-Bromophenyl)methanesulfonamide 98% 83922-51-4 1g $49 2026-06-04 Buy
Activate Scientific AS43968 N-(3-Bromophenyl)methanesulfonamide 98% 83922-51-4 5g $199 2026-06-04 Buy
Activate Scientific AS43968 N-(3-Bromophenyl)methanesulfonamide 98% 83922-51-4 25g $472 2026-06-04 Buy
Apolloscientific OR322586 N-(3-Bromophenyl)methanesulfonamide 95% 83922-51-4 1g $83 2026-06-04 Buy
Product number Packaging Price Buy
IDA92251 10g $472 Buy
AS43968 1g $49 Buy
AS43968 5g $199 Buy
AS43968 25g $472 Buy
OR322586 1g $83 Buy

N-(3-Bromophenyl)methansulfonamide Chemical Properties, Uses, Production

Synthesis

Methanesulfonyl chloride

124-63-0

3-Bromoaniline

591-19-5

N-(3-Bromophenyl)methansulfonamide

83922-51-4

Step i: To a stirred solution of anhydrous dichloromethane (200 ml) of m-bromoaniline (6 g, 34.87 mmol) was sequentially added pyridine (4.13 mg, 52.31 mmol) and methanesulfonyl chloride (5.194 g, 45.34 mmol) at 10 °C. The reaction mixture was stirred at room temperature for 15 h. The progress of the reaction was monitored by thin layer chromatography (TLC, the unfolding agent was a hexane solution of 35% ethyl acetate). After completion of the reaction, the reaction mixture was diluted with dichloromethane (50 ml) and washed with 1N hydrochloric acid (25 ml). The organic layer was dried with anhydrous sodium sulfate and concentrated under reduced pressure to give N-(3-bromophenyl)methane sulfonamide 8.45 g in 96.3% yield. The product was structurally confirmed by 1H NMR (DMSO-d6, 300 MHz) and mass spectrometry (MS: m/z = 251.8 [M + 1]).

References

[1] Patent: WO2014/6554, 2014, A1. Location in patent: Page/Page column 28
[2] Synthetic Communications, 2004, vol. 34, # 20, p. 3807 - 3819
[3] Patent: WO2017/18803, 2017, A1. Location in patent: Paragraph 791; 792; 793
[4] Spectrochimica Acta, Part A: Molecular and Biomolecular Spectroscopy, 1982, vol. 38, # 7, p. 791 - 796
[5] Heterocycles, 2001, vol. 54, # 1, p. 105 - 108

N-(3-Bromophenyl)methansulfonamide Preparation Products And Raw materials

N-(3-Bromophenyl)methansulfonamide Suppliers

Global Suppliers ( 54)
Supplier Tel Email Country ProdList Advantage
J & K SCIENTIFIC LTD. 18210857532 18210857532 jkinfo@jkchemical.com China 96815 76
Beijing Ouhe Technology Co., Ltd 13552068683 13522913783 2355560935@qq.com China 11777 60
Amatek Scientific Co. Ltd. 0512-56316828 4008675858 sales@amateksci.com China 9848 55
Bide Pharmatech Ltd. 400-164-7117 18317119277 product02@bidepharm.com China 40000 60
Beijing FYF Chemicals Co., Ltd 010-57903446 15869909019 168931144@qq.com China 2876 58
Cool Pharm, Ltd 021-60455363 18019463053 sales@coolpharm.com China 8455 58
Watson Biotechnology Co.,Ltd 027-59207879 1972026995 18140587686 sales@3600chem.com China 4175 55
Zhengzhou kangnuochenrui Chemical Technology Co.,Ltd 18210788515; 18210788515 zhuzixin999@163.c0m China 4999 55
Yantai ShengKailun Chemical Technology Co., Ltd. 13356901049 3119594100@qq.com China 7964 55
Aikon International Limited 025-58859352 19370895928 sales01@aikonchem.com China 15078 58

N-(3-Bromophenyl)methansulfonamide Spectrum

N-(3-Bromophenyl)methansulfonamide 3-(methylsulfonyl)amino-1-bromo-benzene 3-BROMO PHENYL METHANE SULPHONAMIDE 83922-51-4 Aryl Building Blocks