3-(Aminomethyl)-1-methylpiperidine
- CAS No.
- 14613-37-7
- Chemical Name:
- 3-(Aminomethyl)-1-methylpiperidine
- Synonyms
- (1-METHYLPIPERIDIN-3-YL)METHANAMINE;CHEMBRDG-BB 4103006;1-Methyl-3-(aminomethyl)p...;3-AMINOMETHYL-1-METHYLPIPERIDINE;1-Methyl-3-piperidinemethanamine;(1-METHYLPIPERID-3-YL)METHYLAMINE;(1-methyl-3-piperidyl)methanamine;3-PIPERIDINEMETHANAMINE, 1-METHYL-;N-Methyl-3-(aMinoMethyl)piperidine;N-Methyl-3-(aMinoMethyl)-piperidin
- CBNumber:
- CB3687503
- Molecular Formula:
- C7H16N2
- Molecular Weight:
- 128.22
- MDL Number:
- MFCD06738902
- MOL File:
- 14613-37-7.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 3-(Aminomethyl)-1-methylpiperidine | A613905 | 25mg | $45 |
| 3-(Aminomethyl)-1-methylpiperidine | A613905 | 250mg | $145 |
| 3-(Aminomethyl)-1-methylpiperidine | 3H32-1-M3 | 1g | $225 |
| 3-(Aminomethyl)-1-methyl-piperidine | FA51097 | 500mg | $360 |
| 3-(Aminomethyl)-1-methyl-piperidine | FA51097 | 1g | $435 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |   GHS05,GHS07 |
|---|---|
| Signal word | Danger |
| Hazard statements | H302+H312+H332-H318 |
| Precautionary statements | P260-P280-P308+P313 |
| Hazard Codes | Xi,Xn |
| Risk Statements | 22 |
| HazardClass | IRRITANT |
| HS Code | 2933399990 |
3-(Aminomethyl)-1-methylpiperidine price More Price(32)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| TRC | A613905 | 3-(Aminomethyl)-1-methylpiperidine | 14613-37-7 | 25mg | $45 | 2021-12-16 | Buy |
| TRC | A613905 | 3-(Aminomethyl)-1-methylpiperidine | 14613-37-7 | 250mg | $145 | 2021-12-16 | Buy |
| SynQuest Laboratories | 3H32-1-M3 | 3-(Aminomethyl)-1-methylpiperidine | 14613-37-7 | 1g | $225 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FA51097 | 3-(Aminomethyl)-1-methyl-piperidine | 14613-37-7 | 500mg | $360 | 2021-12-16 | Buy |
| Biosynth Carbosynth | FA51097 | 3-(Aminomethyl)-1-methyl-piperidine | 14613-37-7 | 1g | $435 | 2021-12-16 | Buy |
3-(Aminomethyl)-1-methylpiperidine Chemical Properties,Uses,Production
Synthesis
![Imidodicarbonic acid, 2-[(1-methyl-3-piperidinyl)methyl]-, 1,3-bis(1,1-dimethylethyl) ester](/CAS/20240320/GIF/672324-98-0.gif)
672324-98-0
14613-37-7
3-(Di-tert-butoxymethylamino)-1-methylpiperidine (500 mg, 1.52 mmol) was used as raw material and dissolved in a 1,4-dioxane solution (19.75 mL) of methanol (7.5 mL) and 10% (v/v) concentrated sulfuric acid. The reaction mixture was stirred at 25°C for 0.5 hours. Methanol (300 mL) was then added and BioRad AG1-X8 resin (OH type) was added until the pH reached 10. The resin was removed by filtration and the resin was washed with methanol (2 x 200 mL). The eluates were combined and evaporated to dryness, and the residue was purified by silica gel column chromatography (30 × 2.5 cm) to afford 3-(aminomethyl)-1-methylpiperidine (69.2 mg, 35%) using 10% concentrated ammonium hydroxide in methanol solution-dichloromethane as eluent. The product characterization data were as follows: FABMS: m/z 129.1 (MH+); HRFABMS: m/z 129.1392 (MH+), calculated value C7H17N2: m/z 129.1392; 1H NMR (CDCl3) δ 0.90 (2H, m, CH2), 1.65 (2H, m, CH2), 1.72 (1H, m. CH), 1.79 (1H, m, CH2), 1.91 (1H, m, CH2), 2.30 (3H, s, NCH3), 2.64 (2H, m, CH2), 2.82 (1H, m, CH2NH2), 2.92 (1H, m, CH2NH2); 13C NMR (CDCl3) δ CH3: 46.7; CH2: 25.2, 28.0, 46.0, 36.4, 60.3; CH: 39.9.
References
[1] Patent: WO2004/22561, 2004, A1. Location in patent: Page 109
3-(Aminomethyl)-1-methylpiperidine Preparation Products And Raw materials
Raw materials
Preparation Products
3-(Aminomethyl)-1-methylpiperidine Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Alchem Pharmtech,Inc. | 8485655694 | sales@alchempharmtech.com | United States | 63687 | 58 |
| Wuhan Chemwish Technology Co., Ltd | 027-67849912 | sales@chemwish.com | CHINA | 10821 | 58 |
| CONIER CHEM AND PHARMA LIMITED | +8618523575427 | sales@conier.com | China | 49977 | 58 |
| career henan chemical co | +86-0371-86658258 +8613203830695 | factory@coreychem.com | China | 29795 | 58 |
| Guangzhou Yuheng Pharmaceutical Technology Co., Ltd | +8613580539051 | joe@yuhengpharm.com | CHINA | 21142 | 58 |
| Hefei TNJ Chemical Industry Co.,Ltd. | +86-0551-65418671 +8618949823763 | sales@tnjchem.com | China | 34563 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 +8617705817739 | info@dycnchem.com | China | 52846 | 58 |
| GIHI CHEMICALS CO.,LIMITED | +86-571-86217390; +8618058761490 | info@gihichemicals.com | China | 49958 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 | market18@leapchem.com | China | 43333 | 58 |
| Young Lively PharminBlock Co.,Ltd | +undefined18600731423 | jason_gao@yl-pharminblock.com | China | 1944 | 58 |
View Lastest Price from 3-(Aminomethyl)-1-methylpiperidine manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2019-12-23 | 3-(Aminomethyl)-1-methylpiperidine
14613-37-7
|
US $1.00 / KG | 1KG | 99% | Customized | Career Henan Chemical Co |
-
- 3-(Aminomethyl)-1-methylpiperidine
14613-37-7
- US $1.00 / KG
- 99%
- Career Henan Chemical Co
