9-Iodophenanthrene
- CAS No.
- 17024-12-3
- Chemical Name:
- 9-Iodophenanthrene
- Synonyms
- 9-IODOPHENANTHREN;9-Iodophenanthrene;9-Phenanthryl iodide;Phenanthrene, 9-iodo-;9-Iodophenanthrene 97%;2,5-bis(4-ethoxyanilino)-3,6-dimethoxycyclohexa-2,5-diene-1,4-dione
- CBNumber:
- CB3760198
- Molecular Formula:
- C14H9I
- Molecular Weight:
- 304.13
- MDL Number:
- MFCD00192230
- MOL File:
- 17024-12-3.mol
- MSDS File:
- SDS
| Melting point | 91-93 °C (lit.) |
|---|---|
| Boiling point | 411.0±14.0 °C(Predicted) |
| Density | 1.692±0.06 g/cm3(Predicted) |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| Appearance | Light yellow to yellow Solid |
| Stability | Stable, but light sensitive - store in the dark. Incompatible with strong oxidizing agents. |
| InChI | InChI=1S/C14H9I/c15-14-9-10-5-1-2-6-11(10)12-7-3-4-8-13(12)14/h1-9H |
| InChIKey | CBFIPOTVFMLMFQ-UHFFFAOYSA-N |
| SMILES | C1=C2C(C3C(C(I)=C2)=CC=CC=3)=CC=C1 |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 |
| target organs | Respiratory system |
| PPE | dust mask type N95 (US), Eyeshields, Gloves |
| Hazard Codes | Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 26-36 |
| WGK Germany | 3 |
| Storage Class | 11 - Combustible Solids |
| Hazard Classifications | Eye Irrit. 2 Skin Irrit. 2 STOT SE 3 |
9-Iodophenanthrene price More Price(28)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 389358 | 9-Iodophenanthrene 97% | 17024-12-3 | 1g | $85.7 | 2026-04-30 | Buy |
| Usbiological | 280756 | 9-Iodophenanthrene Asreported | 17024-12-3 | 5g | $2088 | 2026-06-03 | Buy |
| Usbiological | 280756 | 9-Iodophenanthrene Asreported | 17024-12-3 | 10g | $3212 | 2026-06-03 | Buy |
| Activate Scientific | AS113894 | 9-Iodophenanthrene 98% | 17024-12-3 | 1g | $38 | 2026-06-04 | Buy |
| Activate Scientific | AS113894 | 9-Iodophenanthrene 98% | 17024-12-3 | 5g | $129 | 2026-06-04 | Buy |
9-Iodophenanthrene Chemical Properties, Uses, Production
Chemical Properties
solid
Synthesis
573-17-1
17024-12-3
General procedure for the synthesis of 9-iodophenanthrene from 9-bromophenanthrene: General method: aryl bromide (10 mmol) was dissolved in anhydrous THF (30 mL) and cooled to -78 °C at room temperature. Slowly add n-butyllithium (1.6 M, dissolved in hexane; 7.5 mL; 12 mmol) dropwise. After 15 min of reaction, a solution of anhydrous THF (10 mL) with iodine (I2, 3.81 g; 15 mmol) was added, followed by gradual warming of the reaction mixture to room temperature and stirring overnight. After completion of the reaction, the mixture was concentrated under vacuum. Water (H2O) was added to the residue and extracted with dichloromethane (DCM, 3 times). The organic phases were combined and washed sequentially with saturated sodium thiosulfate (Na2S2O5) solution and water. The organic phase was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure, and the resulting crude product was purified by column chromatography.
References
[1] Synlett, 2013, vol. 24, # 20, p. 2730 - 2734
[2] Synthesis, 1986, # 1, p. 121 - 122
[3] Journal of Organic Chemistry, 2009, vol. 74, # 12, p. 4650 - 4653
[4] Tetrahedron Letters, 1999, vol. 40, # 36, p. 6671 - 6672
[5] Beilstein Journal of Organic Chemistry, 2011, vol. 7, p. 1499 - 1503
9-Iodophenanthrene Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Shanghai Fengtian Biotechnology Co., Ltd | 021-17514032201 17514032201 | 17514032201@163.com | China | 75 | 58 |
| Beijing HwrkChemical Technology Co., Ltd | 89508211 18501085097 | sales.bj@hwrkchemical.com | China | 9407 | 55 |
| Energy Chemical | 400-0056266 | sales8178@energy-chemical.com | China | 44850 | 61 |
| Shanghai Hanhong Scientific Co.,Ltd. | 021-54306202 13764082696 | info@hanhongsci.com | China | 42917 | 64 |
| Syntechem Co.,Ltd | info@syntechem.com | China | 12973 | 57 | |
| Hunan Hui Bai Shi Biotechnology Co., Ltd. | 0731-85526065 13308475853 | ivy@hnhbsj.com | China | 7236 | 62 |
| Shanghai Topbiochem Technology Co., Ltd | 021-58170097 | info@topbiochem.com | China | 9510 | 58 |
| Shanghai Run-Biotech Co., Ltd. | 021-57171705 13817537615 | sales@run-biotech.com | China | 2282 | 58 |
| Bide Pharmatech Ltd. | 400-164-7117 18317119277 | product02@bidepharm.com | China | 40000 | 60 |
| Sigma-Aldrich | 021-61415566 800-8193336 | orderCN@merckgroup.com | China | 51389 | 80 |
View Latest Price from 9-Iodophenanthrene manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2026-09-02 | Phenanthrene, 9-iodo-
17024-12-3
|
$5.00 | 1KG | 99% | Henan Fengda Chemical Co., Ltd |
-
- Phenanthrene, 9-iodo-
17024-12-3
- $5.00
- 99%
- Henan Fengda Chemical Co., Ltd
