9-IODOPHENANTHRENE
- CAS No.
- 17024-12-3
- Chemical Name:
- 9-IODOPHENANTHRENE
- Synonyms
- 9-IODOPHENANTHRENE;9-Phenanthryl iodide;Phenanthrene, 9-iodo-;9-Iodophenanthrene 97%;2,5-bis(4-ethoxyanilino)-3,6-dimethoxycyclohexa-2,5-diene-1,4-dione
- CBNumber:
- CB3760198
- Molecular Formula:
- C14H9I
- Molecular Weight:
- 304.13
- MDL Number:
- MFCD00192230
- MOL File:
- 17024-12-3.mol
- MSDS File:
- SDS
| Melting point | 91-93 °C (lit.) |
|---|---|
| Boiling point | 411.0±14.0 °C(Predicted) |
| Density | 1.692±0.06 g/cm3(Predicted) |
| storage temp. | Keep in dark place,Sealed in dry,Room Temperature |
| Appearance | Light yellow to yellow Solid |
| Stability | Stable, but light sensitive - store in the dark. Incompatible with strong oxidizing agents. |
| InChI | InChI=1S/C14H9I/c15-14-9-10-5-1-2-6-11(10)12-7-3-4-8-13(12)14/h1-9H |
| InChIKey | CBFIPOTVFMLMFQ-UHFFFAOYSA-N |
| SMILES | C1=C2C(C3C(C(I)=C2)=CC=CC=3)=CC=C1 |
| UNSPSC Code | 12352100 |
| NACRES | NA.22 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P261-P264-P271-P280-P302+P352-P305+P351+P338 |
| Hazard Codes | Xi |
| Risk Statements | 36/37/38 |
| Safety Statements | 26-36 |
| WGK Germany | 3 |
9-IODOPHENANTHRENE price More Price(16)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Sigma-Aldrich | 389358 | 9-Iodophenanthrene 97% | 17024-12-3 | 1g | $74.7 | 2025-07-31 | Buy |
| Usbiological | 280756 | 9-Iodophenanthrene | 17024-12-3 | 5g | $2088 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0067235 | 9-IODOPHENANTHRENE 95.00% | 17024-12-3 | 50G | $2679.6 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0067235 | 9-IODOPHENANTHRENE 95.00% | 17024-12-3 | 100G | $2899.05 | 2021-12-16 | Buy |
| American Custom Chemicals Corporation | HCH0067235 | 9-IODOPHENANTHRENE 95.00% | 17024-12-3 | 25G | $1270.5 | 2021-12-16 | Buy |
9-IODOPHENANTHRENE Chemical Properties,Uses,Production
Chemical Properties
solid
Synthesis
573-17-1
17024-12-3
General procedure for the synthesis of 9-iodophenanthrene from 9-bromophenanthrene: General method: aryl bromide (10 mmol) was dissolved in anhydrous THF (30 mL) and cooled to -78 °C at room temperature. Slowly add n-butyllithium (1.6 M, dissolved in hexane; 7.5 mL; 12 mmol) dropwise. After 15 min of reaction, a solution of anhydrous THF (10 mL) with iodine (I2, 3.81 g; 15 mmol) was added, followed by gradual warming of the reaction mixture to room temperature and stirring overnight. After completion of the reaction, the mixture was concentrated under vacuum. Water (H2O) was added to the residue and extracted with dichloromethane (DCM, 3 times). The organic phases were combined and washed sequentially with saturated sodium thiosulfate (Na2S2O5) solution and water. The organic phase was dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure, and the resulting crude product was purified by column chromatography.
References
[1] Synlett, 2013, vol. 24, # 20, p. 2730 - 2734
[2] Synthesis, 1986, # 1, p. 121 - 122
[3] Journal of Organic Chemistry, 2009, vol. 74, # 12, p. 4650 - 4653
[4] Tetrahedron Letters, 1999, vol. 40, # 36, p. 6671 - 6672
[5] Beilstein Journal of Organic Chemistry, 2011, vol. 7, p. 1499 - 1503
9-IODOPHENANTHRENE Preparation Products And Raw materials
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Henan Fengda Chemical Co., Ltd | +86-371-86557731 +86-13613820652 | info@fdachem.com | China | 20191 | 58 |
| ATK CHEMICAL COMPANY LIMITED | +undefined-21-51877795 | ivan@atkchemical.com | China | 33024 | 60 |
| Jilin Chinese Academy of Sciences - Yanshen Technology Co., Ltd. | 0431-80514535 13634302652 | Extension@chemextension.com | CHINA | 967 | 58 |
| Wuhan Chemwonders Technology Inc. | 027-85778276 | info@chemwonders.com | CHINA | 176 | 58 |
| Shanghai Daeyeon Chemicals Co., Ltd | 021-64478606 +8615900664856 | daeyeon001@vip.163.com | China | 2062 | 58 |
| Labnetwork lnc. | +86-27-50766799 +8618062016861 | contact@labnetwork.com | China | 19987 | 58 |
| Hangzhou Benoy Chemical Co., Ltd | +8617342059697 | sales@benoychem.com | China | 315 | 58 |
| SUZHOU SENFEIDA CHEMICAL CO.,LTD | +86-0512-83500002 +8618662433356 | 3899766280@qq.com | China | 26362 | 58 |
| Jilin Chinese Academy of Sciences-yanshen Technology | +undefined18143011203 | info@chemextension.com | China | 42056 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 57505 | 58 |
View Lastest Price from 9-IODOPHENANTHRENE manufacturers
| Image | Update time | Product | Price | Min. Order | Purity | Supply Ability | Manufacturer | |
|---|---|---|---|---|---|---|---|---|
 |
2024-01-14 | Phenanthrene, 9-iodo-
17024-12-3
|
US $5.00-0.50 / KG | 1KG | 99% | g-kg-tons, free sample is available | Henan Fengda Chemical Co., Ltd |
-
- Phenanthrene, 9-iodo-
17024-12-3
- US $5.00-0.50 / KG
- 99%
- Henan Fengda Chemical Co., Ltd
