3-BROMO-2-METHOXYBENZALDEHYDE
- CAS No.
- 88275-87-0
- Chemical Name:
- 3-BROMO-2-METHOXYBENZALDEHYDE
- Synonyms
- 3-BROMO-2-METHOXYBENZALDEHYDE;Benzaldehyde, 3-bromo-2-methoxy-
- CBNumber:
- CB41092589
- Molecular Formula:
- C8H7BrO2
- Molecular Weight:
- 215.04
- MDL Number:
- MFCD09834811
- MOL File:
- 88275-87-0.mol
- MSDS File:
- SDS
| Product description | Number | Pack Size | Price |
| 3-Bromo-2-methoxybenzaldehyde 95% | AS30568 | 1g | $35 |
| 3-Bromo-2-methoxybenzaldehyde 95% | AS30568 | 5g | $121 |
| 3-Bromo-2-methoxybenzaldehyde 95% | AS30568 | 25g | $478 |
| 3-Bromo-2-methoxybenzaldehyde 95% | AS30568 | 100g | $1724 |
| 3-Bromo-2-methoxybenzaldehyde 95% | OR400651 | 1g | $88 |
| More product size | |||
| Boiling point | 282.3±20.0 °C(Predicted) |
|---|---|
| Density | 1.522±0.06 g/cm3(Predicted) |
| storage temp. | Inert atmosphere,2-8°C |
| form | solid |
| Appearance | Light brown to white Solid |
| InChI | 1S/C8H7BrO2/c1-11-8-6(5-10)3-2-4-7(8)9/h2-5H,1H3 |
| InChIKey | SZDPZQAPHXPVCN-UHFFFAOYSA-N |
| SMILES | COC1=C(C=CC=C1C=O)Br |
| UNSPSC Code | 12352200 |
| NACRES | NA.21 |
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302+H312+H332-H315-H319-H335 |
| Precautionary statements | P260-P280-P301+P312 |
| WGK Germany | WGK 3 |
| HS Code | 2913000090 |
| Storage Class | 11 - Combustible Solids |
| Hazard Classifications | Acute Tox. 4 Oral |
3-BROMO-2-METHOXYBENZALDEHYDE price More Price(41)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Activate Scientific | AS30568 | 3-Bromo-2-methoxybenzaldehyde 95% | 88275-87-0 | 1g | $35 | 2026-06-04 | Buy |
| Activate Scientific | AS30568 | 3-Bromo-2-methoxybenzaldehyde 95% | 88275-87-0 | 5g | $121 | 2026-06-04 | Buy |
| Activate Scientific | AS30568 | 3-Bromo-2-methoxybenzaldehyde 95% | 88275-87-0 | 25g | $478 | 2026-06-04 | Buy |
| Activate Scientific | AS30568 | 3-Bromo-2-methoxybenzaldehyde 95% | 88275-87-0 | 100g | $1724 | 2026-06-04 | Buy |
| Apolloscientific | OR400651 | 3-Bromo-2-methoxybenzaldehyde 95% | 88275-87-0 | 1g | $88 | 2026-06-04 | Buy |
3-BROMO-2-METHOXYBENZALDEHYDE Chemical Properties,Uses,Production
Synthesis
1829-34-1
74-88-4
88275-87-0
GENERAL STEPS: 3-Bromo-2-hydroxybenzaldehyde (5.0 g, 24.87 mmol) was dissolved in acetone (200 mL) and iodomethane (5.3 g, 37.34 mmol) and potassium carbonate (5.2 g, 37.63 mmol) were added sequentially. The reaction mixture was heated to 60 °C and stirred for 2 hours. After completion of the reaction, the mixture was cooled to room temperature and filtered to remove insoluble solids. The filtrate was concentrated to dryness by rotary evaporation and the resulting residue was redissolved in ethyl acetate. The organic phase was washed with saturated aqueous sodium bicarbonate and subsequently dried over anhydrous magnesium sulfate. After filtration to remove the desiccant, the filtrate was concentrated to give the crude product. The crude product was purified by silica gel column chromatography using 50% ethyl acetate in hexane solution as eluent. The eluate containing the target product was collected and concentrated to give 3-bromo-2-methoxybenzaldehyde (2.0 g, 93% yield) as a colorless slurry. Mass spectrometry analysis showed m/z 215.0 ([M+H]+); the high performance liquid chromatography retention time (HPLC rt) was 13.8 min [a].
References
[1] Patent: WO2013/10904, 2013, A1. Location in patent: Page/Page column 65
[2] Journal of Medicinal Chemistry, 2002, vol. 45, # 17, p. 3573 - 3575
[3] Patent: WO2011/33265, 2011, A1. Location in patent: Page/Page column 93-94
[4] Patent: WO2009/76602, 2009, A1. Location in patent: Page/Page column 161-162
[5] Synthesis (Germany), 2018, vol. 50, # 13, p. 2516 - 2522
3-BROMO-2-METHOXYBENZALDEHYDE Preparation Products And Raw materials
Raw materials
Preparation Products
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Fuxin Pharmaceutical | +86-021-021-50872116 | contact@fuxinpharm.com | China | 9976 | 58 |
| Career Henan Chemica Co | +86-0371-86658258 +86-13203830695 | laboratory@coreychem.com | China | 30203 | 58 |
| Win-Win chemical CO., Limited | +86-0086-577-64498589 +86-15355981851 | sales@win-winchemical.com | China | 14301 | 58 |
| SHAANXI LIGHTE OPTOELECTRONICS MATERIAL CO., LTD | +86-17691239725 +86-15529797525 | lijiasheng@ltom.com | China | 185 | 58 |
| Dayang Chem (Hangzhou) Co.,Ltd. | +86-0571-88938639 17705817739 | info@dycnchem.com | China | 52693 | 58 |
| HANGZHOU LEAP CHEM CO., LTD. | +86-571-87711850 +86-15355479329 | market18@leapchem.com | China | 43303 | 58 |
| Shanghai Acmec Biochemical Technology Co., Ltd. | +86-18621343501 | product@acmec-e.com | China | 33301 | 58 |
| Aladdin Scientific | tp@aladdinsci.com | United States | 50108 | 58 | |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Energy Chemical | 021-021-58432009 400-005-6266 | sales8178@energy-chemical.com | China | 44848 | 61 |
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