2-bromo-6-methoxy-aniline
- CAS No.
- 5473-01-8
- Chemical Name:
- 2-bromo-6-methoxy-aniline
- Synonyms
- Nsc29554;2-Amino-3-bromoanisole;2-Bromo-6-methoxyaniline97%;2-Bromo-6-methoxyaniline 97%;2-BroMo-6-Methoxy-phenylaMine;BenzenaMine, 2-broMo-6-Methoxy-;2-Amino-3-bromoanisole, 6-Bromo-o-anisidine
- CBNumber:
- CB41480038
- Molecular Formula:
- C7H8BrNO
- Molecular Weight:
- 202.05
- MDL Number:
- MFCD08741448
- MOL File:
- 5473-01-8.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H302-H312-H319-H332-H335 |
| Precautionary statements | P261-P271-P280 |
| HS Code | 2922290090 |
2-bromo-6-methoxy-aniline price More Price(57)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| ChemScene | CS-0033843 | 2-Bromo-6-methoxyaniline ≥98% | 5473-01-8 | 100mg | $5 | 2026-06-04 | Buy |
| ChemScene | CS-0033843 | 2-Bromo-6-methoxyaniline ≥98% | 5473-01-8 | 250mg | $11 | 2026-06-04 | Buy |
| ChemScene | CS-0033843 | 2-Bromo-6-methoxyaniline ≥98% | 5473-01-8 | 1g | $15 | 2026-06-04 | Buy |
| ChemScene | CS-0033843 | 2-Bromo-6-methoxyaniline ≥98% | 5473-01-8 | 5g | $44 | 2026-06-04 | Buy |
| ChemScene | CS-0033843 | 2-Bromo-6-methoxyaniline ≥98% | 5473-01-8 | 10g | $75 | 2026-06-04 | Buy |
2-bromo-6-methoxy-aniline Chemical Properties, Uses, Production
Synthesis
90-04-0
5473-01-8
Step A: Synthesis of 6-bromo-2-anisidine. A solution of bromine (1.22 mL, 23.7 mmol) in acetic acid (10 mL) was slowly added dropwise to a cooled solution of o-methoxyaniline (2.7 mL, 23.7 mmol) in hexadecanecarboxylic acid (20 mL) for a controlled time period of 10 minutes at 10°C. The reaction mixture was then stirred for 10 minutes. After the dropwise addition was completed, the reaction mixture was continued to be stirred for 10 min. Upon completion of the reaction, the solvent was removed by rotary evaporation and the residue was dissolved in ethyl acetate. The solution was sequentially washed with saturated sodium bicarbonate solution and dried with anhydrous magnesium sulfate. After drying, the desiccant was removed by filtration and the filtrate was concentrated by rotary evaporation. The crude product was purified by fast column chromatography on silica gel, the eluent being a hexane solution of 45% dichloromethane, resulting in 3.44 g of 2-bromo-6-methoxyaniline in 72% yield.
References
[1] Patent: US6291511, 2001, B1
2-bromo-6-methoxy-aniline Preparation Products And Raw materials
2-bromo-6-methoxy-aniline Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| J & K SCIENTIFIC LTD. | 18210857532 18210857532 | jkinfo@jkchemical.com | China | 96815 | 76 |
| Hangzhou Sage Chemical Co., Ltd. | +86057186818502 13588463833 | info@sagechem.com | China | 10265 | 58 |
| Jiangsu Aikon Biopharmaceutical R&D co.,Ltd. | 025-66113011 13913916777 | cfzhang@aikonchem.com | China | 19902 | 55 |
| Shanghai Jian Chao Chemical Technology Co., Ltd. | 150-2103-5486 18017383231 | 983544897@qq.com | China | 9335 | 55 |
| SuZhou ShiYa Biopharmaceuticals, Inc. | 86(512)5235 8471 17715136450 | sales@shiyabiopharm.com | China | 4167 | 58 |
| Shanghai Raise Chemical Technology Co.,Ltd | +86-021-50935922 | China | 7854 | 55 | |
| CEG Chemical Science&Technology Co., Ltd. | Mobile:13665161512 | China | 1784 | 58 | |
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| Xinyanhe Pharmatech Co.,Ltd | 0519-85252752 15366845260 | taihuaren@vip.163.com | China | 1032 | 58 |
| Mashilabs (Shanghai) Co.,Ltd. | 19916721580 | mafarm@126.com | China | 4534 | 58 |
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