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4-morpholinocyclohexanone

4-morpholinocyclohexanone Structure
4-morpholinocyclohexanone structure
CAS No.
139025-93-7
Chemical Name:
4-morpholinocyclohexanone
Synonyms
4-morpholinocyclohexanone;4-Morpholinocyclohexan-1-one;4-(4-Morpholinyl)-cyclohexanone;4-(Morpholin-4-yl)cyclohexanone;Cyclohexanone, 4-(4-morpholinyl)-;4-(Morpholin-4-yl)cyclohexan-1-one
CBNumber:
CB52499692
Molecular Formula:
C10H17NO2
Molecular Weight:
183.25
MDL Number:
MFCD17013167
MOL File:
139025-93-7.mol
Last updated:2025-07-24 18:13:44
Product description Number Pack Size Price
4-(Morpholin-4-yl)cyclohexanone M723710 100mg $150
4-Morpholinocyclohexanone 95+% 074771 250mg $445
4-(Morpholin-4-yl)cyclohexanone 47785 100mg $650
4-Morpholinocyclohexanone 95+% 074771 1g $958
4-morpholinocyclohexanone W3041 100mg $104
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4-morpholinocyclohexanone Properties

storage temp. 2-8°C
solubility Chloroform (Slightly), DMSO (Slightly), Ethyl Acetate (Slightly), Methanol (Slightly)
form Oil
color Dark Yellow to Dark Brown

SAFETY

Risk and Safety Statements

HS Code  2934999090

4-morpholinocyclohexanone price More Price(16)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TRC M723710 4-(Morpholin-4-yl)cyclohexanone 139025-93-7 100mg $150 2021-12-16 Buy
Matrix Scientific 074771 4-Morpholinocyclohexanone 95+% 139025-93-7 250mg $445 2021-12-16 Buy
Medical Isotopes, Inc. 47785 4-(Morpholin-4-yl)cyclohexanone 139025-93-7 100mg $650 2021-12-16 Buy
Matrix Scientific 074771 4-Morpholinocyclohexanone 95+% 139025-93-7 1g $958 2021-12-16 Buy
AK Scientific W3041 4-morpholinocyclohexanone 139025-93-7 100mg $104 2021-12-16 Buy
Product number Packaging Price Buy
M723710 100mg $150 Buy
074771 250mg $445 Buy
47785 100mg $650 Buy
074771 1g $958 Buy
W3041 100mg $104 Buy

4-morpholinocyclohexanone Chemical Properties,Uses,Production

Uses

4-(Morpholin-4-yl)cyclohexanone is a useful synthetic intermediate. It was used to synthesize diastereomeric 3,6-diaminobicyclo[3.1.0]hexane derivatives.

Synthesis

4-(1,4-dioxaspiro[4.5]decan-8-yl)morpholine

127562-53-2

4-morpholinocyclohexanone

139025-93-7

The general procedure for the synthesis of 4-morpholin-4-ylcyclohexanone (VII-a) from the compound (CAS:127562-53-2) was as follows: to a solution of compound (4.50 g, 19.8 mmol) in tetrahydrofuran (THF, 100 mL) was added an aqueous 7N hydrochloric acid solution (40 mL). The reaction mixture was stirred at room temperature for 17 hours. Upon completion of the reaction, the mixture was poured into saturated aqueous sodium bicarbonate (NaHCO3) solution (475 mL) to quench the reaction. Subsequently, the reaction mixture was sequentially extracted with ethyl acetate (1 time) and dichloromethane (CH2Cl2, 3 times). The organic phases were combined, dried over anhydrous magnesium sulfate (MgSO4) and concentrated under reduced pressure. The resulting oil was purified by Kugelrohr distillation to afford the target product 4-morpholin-4-ylcyclohexanone (VII-a) (3.17 g, 87% yield) as a clear oil. The structure of the product was confirmed by 1H NMR (400 MHz, CDCl3), δ 1.80-1.94 (m, 2H), 1.80-2.10 (m, 2H), 2.30 (m, 1H), 2.45-2.65 (m, 8H), and 3.74 (t, J=4.7 Hz, 4H).

References

[1] Patent: WO2008/95943, 2008, A1. Location in patent: Page/Page column 175-176
[2] Patent: WO2008/95944, 2008, A1. Location in patent: Page/Page column 236; 238
[3] Patent: WO2010/15803, 2010, A1. Location in patent: Page/Page column 34-35
[4] Patent: WO2018/137593, 2018, A1. Location in patent: Page/Page column 105
[5] Synthesis, 1991, # 12, p. 1142 - 1147

4-morpholinocyclohexanone Preparation Products And Raw materials

Raw materials

4-(1,4-dioxaspiro[4.5]decan-8-yl)morpholine Tetrahydrofuran Sodium bicarbonate Water Hydrochloric acid

Preparation Products

4-[4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)-3-CYCLOHEXEN-1-YL]-MORPHOLINE

4-morpholinocyclohexanone Suppliers

Global( 50)Suppliers
Supplier Tel Email Country ProdList Advantage
Capot Chemical Co.,Ltd. 		+86-（0）57185586718; +8613336195806 sales@capot.com China 29735 60
ATK CHEMICAL COMPANY LIMITED 		+undefined-21-51877795 ivan@atkchemical.com China 33024 60
Alchem Pharmtech,Inc. 		8485655694 sales@alchempharmtech.com United States 63687 58
career henan chemical co 		+86-0371-86658258 +8613203830695 factory@coreychem.com China 29798 58
Zhejiang J&C Biological Technology Co.,Limited 		+1-2135480471 sales@sarms4muscle.com China 10473 58
Nextpeptide Inc 		+86-0571-81612335 +8613336028439 sales@nextpeptide.com China 19908 58
Labnetwork lnc. 		+86-27-50766799 +8618062016861 contact@labnetwork.com China 19987 58
HANGZHOU LEAP CHEM CO., LTD. 		+86-571-87711850 market18@leapchem.com China 43339 58
Amadis Chemical Company Limited 		571-89925085 sales@amadischem.com China 131957 58
ROSEWA HOLDING GROUP CO.,LIMITED 		+86-023-62871537 sales@rosewachem.com China 2803 58
Supplier Advantage
Capot Chemical Co.,Ltd. 		60
ATK CHEMICAL COMPANY LIMITED 		60
Alchem Pharmtech,Inc. 		58
career henan chemical co 		58
Zhejiang J&C Biological Technology Co.,Limited 		58
Nextpeptide Inc 		58
Labnetwork lnc. 		58
HANGZHOU LEAP CHEM CO., LTD. 		58
Amadis Chemical Company Limited 		58
ROSEWA HOLDING GROUP CO.,LIMITED 		58

View Lastest Price from 4-morpholinocyclohexanone manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
4-morpholinocyclohexanone pictures 2019-12-27 4-morpholinocyclohexanone
139025-93-7
 US $6.60 / KG 1KG 97%-99% 1kg-1000kg Career Henan Chemical Co

4-morpholinocyclohexanone Spectrum

4-morpholinocyclohexanone(139025-93-7)1HNMR
4-morpholinocyclohexanone 4-(Morpholin-4-yl)cyclohexan-1-one 4-(Morpholin-4-yl)cyclohexanone 4-Morpholinocyclohexan-1-one 4-(4-Morpholinyl)-cyclohexanone Cyclohexanone, 4-(4-morpholinyl)- 139025-93-7 39025-93-7