ChemicalBook >> CAS DataBase List >>1,3-DIBROMO-5-IODOBENZENE

1,3-DIBROMO-5-IODOBENZENE

CAS No.
19752-57-9
Chemical Name:
1,3-DIBROMO-5-IODOBENZENE
Synonyms
SKL670;3,5-DIBROMOIODOBENZENE;3-DIBROMO-5-IODOBENZENE;3,5-Dibromophenyl iodide;1-Iodo-3,5-dibromobenzene;1,3-DIBROMO-5-IODOBENZENE;1,3-Dibromo-5-iodiobenzene;Benzene,1,3-dibromo-5-iodo-;1,3-Dibromo-5-iodobenzene>1,3-DIBROMO-5-IODOBENZENE 25G
CBNumber:
CB5752502
Molecular Formula:
C6H3Br2I
Molecular Weight:
361.8
MDL Number:
MFCD07778996
MOL File:
19752-57-9.mol
MSDS File:
SDS
Last updated:2026-06-25 18:04:04
Product description Number Pack Size Price
1,3-Dibromo-5-iodobenzene D4691 1G $34
1,3-Dibromo-5-iodobenzene D4691 5G $125
1,3-Dibromo-5-iodobenzene 95% OR931667 1g $21
1,3-Dibromo-5-iodobenzene 95% OR931667 5g $73
1,3-Dibromo-5-iodobenzene 98% AS39814 5g $24
More product size

1,3-DIBROMO-5-IODOBENZENE Properties

Melting point 124.4-124.7℃
Boiling point 302.7±32.0 °C(Predicted)
Density 2.514±0.06 g/cm3 (20 ºC 760 Torr)
storage temp. Keep in dark place,Sealed in dry,Room Temperature
form powder to crystal
color Light yellow to Brown
InChI InChI=1S/C6H3Br2I/c7-4-1-5(8)3-6(9)2-4/h1-3H
InChIKey KARUMYWDGQTPFL-UHFFFAOYSA-N
SMILES C1(Br)=CC(I)=CC(Br)=C1

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319
Precautionary statements  P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313
HS Code  2903998090

1,3-DIBROMO-5-IODOBENZENE price More Price(47)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
TCI Chemical D4691 1,3-Dibromo-5-iodobenzene 19752-57-9 1G $34 2026-04-30 Buy
TCI Chemical D4691 1,3-Dibromo-5-iodobenzene 19752-57-9 5G $125 2026-04-30 Buy
Apolloscientific OR931667 1,3-Dibromo-5-iodobenzene 95% 19752-57-9 1g $21 2026-06-04 Buy
Apolloscientific OR931667 1,3-Dibromo-5-iodobenzene 95% 19752-57-9 5g $73 2026-06-04 Buy
Activate Scientific AS39814 1,3-Dibromo-5-iodobenzene 98% 19752-57-9 5g $24 2026-06-04 Buy
Product number Packaging Price Buy
D4691 1G $34 Buy
D4691 5G $125 Buy
OR931667 1g $21 Buy
OR931667 5g $73 Buy
AS39814 5g $24 Buy

1,3-DIBROMO-5-IODOBENZENE Chemical Properties,Uses,Production

Uses

1,3-Dibromo-5-iodobenzene is an important organic intermediate widely used in the fields of dyes, pigments, pharmaceuticals and pesticides.

Chemical Properties

Reddish brown powder

Synthesis

2,6-dibromo-4-iodoaniline

10527-69-2

1,3-DIBROMO-5-IODOBENZENE

19752-57-9

The general procedure for the synthesis of 1,3-dibromo-5-iodobenzene from 2,6-dibromo-4-iodoaniline is as follows: 1. Preparation of 3,5-dibromoiodobenzene: 188.4 g of 2,6-dibromo-4-iodoaniline and 600 g of hypophosphorous acid were added to the reaction vessel at room temperature and stirred well. Subsequently, a solution formed by dissolving 34.5 g of sodium nitrite in 60 ml of water was added dropwise. The reaction is violently exothermic and the reaction temperature needs to be controlled at 20-25°C by means of a water bath. After the dropwise addition was completed, the reaction was continued for about 3 hours until a large white solid precipitate was observed. The reaction was continued at this temperature for 1 hour. The progress of the reaction was monitored by HPLC and stopped when the raw material 2,6-dibromo-4-iodoaniline completely disappeared. The crude product was collected by filtration. 2. Purification of the crude product: the crude product was dispersed in three 1000 ml flasks, 700 ml of anhydrous ethanol was added to each flask, and the product was heated to reflux (ca. 80 °C) to completely dissolve the product. Subsequently, it was cooled to 20-25 °C, the crystals were collected by filtration and dried under reduced pressure at 60 °C to obtain white needle-like crystals of 136 g. The purity of the product, 3,5-dibromo-2-iodobenzene, was 99.72% by HPLC analysis and the reaction yield was 75.2%.

References

[1] Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1913, vol. <5> 22 I, p. 823
[2] Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1914, vol. <5> 23 I, p. 283 Anm.
[3] Journal of the American Chemical Society, 2002, vol. 124, # 29, p. 8661 - 8666
[4] Journal of Organic Chemistry, 2015, vol. 80, # 2, p. 882 - 896
[5] Patent: CN105523884, 2016, A. Location in patent: Paragraph 0014; 0016; 0017

10527-69-2
19752-57-9
Synthesis of 1,3-DIBROMO-5-IODOBENZENE from 2,6-dibromo-4-iodoaniline
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View Lastest Price from 1,3-DIBROMO-5-IODOBENZENE manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
1,3-DIBROMO-5-IODOBENZENE pictures 2026-08-03 1,3-DIBROMO-5-IODOBENZENE
19752-57-9
1KG 98% 2000 Shenzhen Nexcon Pharmatechs Ltd.
1,3-DIBROMO-5-IODOBENZENE pictures 2026-06-30 1,3-DIBROMO-5-IODOBENZENE
19752-57-9
1kg 98% 1000kg Shaanxi Dideu New Materials Co. Ltd
1,3-DIBROMO-5-IODOBENZENE pictures 2025-06-27 1,3-DIBROMO-5-IODOBENZENE
19752-57-9
$10.00-30.00 50KG 99% 500000kg Hebei Chuanghai Biotechnology Co., Ltd

1,3-DIBROMO-5-IODOBENZENE Spectrum

Benzene,1,3-dibromo-5-iodo- 1,3-DIBROMO-5-IODOBENZENE 25G 1,3-DIBROMO-5-IODOBENZENE 3,5-DIBROMOIODOBENZENE 1-Iodo-3,5-dibromobenzene 3,5-Dibromophenyl iodide 1,3-Dibromo-5-iodobenzene> 1,3-DIBROMO-5-IODOBENZENE ISO 9001:2015 REACH 3-DIBROMO-5-IODOBENZENE SKL670 1,3-Dibromo-5-iodobenzene 98% 1,3-Dibromo-5-iodiobenzene 19752-57-9 C6H3Br2I organic chemicals and derivatives/others OLED