5-bromo-2-nitro-N-phenyl-aniline
- CAS No.
- 6311-47-3
- Chemical Name:
- 5-bromo-2-nitro-N-phenyl-aniline
- Synonyms
- 5-bromo-2-nitro-N-phenyl-aniline;N-(5-bromo-2-nitrophenyl)benzenamine;BenzenaMine, 5-broMo-2-nitro-N-phenyl-
- CBNumber:
- CB61258369
- Molecular Formula:
- C12H9BrN2O2
- Molecular Weight:
- 293.12
- MDL Number:
- MFCD22056128
- MOL File:
- 6311-47-3.mol
- MSDS File:
- SDS
SAFETY
Risk and Safety Statements
| Symbol(GHS) |  GHS07 |
|---|---|
| Signal word | Warning |
| Hazard statements | H315-H319-H335 |
| Precautionary statements | P264-P280-P302+P352-P321-P332+P313-P362-P305+P351+P338-P337+P313-P261-P271-P304+P340-P312-P403+P233-P405-P501 |
5-bromo-2-nitro-N-phenyl-aniline price More Price(20)
| Manufacturer | Product number | Product description | CAS number | Packaging | Price | Updated | Buy |
|---|---|---|---|---|---|---|---|
| Matrix Scientific | 132111 | 5-Bromo-2-nitro-N-phenylaniline | 6311-47-3 | 100.00g | $1764 | 2026-05-18 | Buy |
| Matrix Scientific | 132111 | 5-Bromo-2-nitro-N-phenylaniline | 6311-47-3 | 250.00g | $3240 | 2026-05-18 | Buy |
| A1 Biochem Labs | A1-05606 | N-phenyl-5-bromo-2-nitrobenzenamine 0.95 | 6311-47-3 | 5g | $700 | 2026-06-05 | Buy |
| aablocks | AA00EIWI | 5-Bromo-2-Nitro-N-Phenylaniline 98% | 6311-47-3 | 250mg | $32 | 2026-05-28 | Buy |
| ACHEMBLOCK | 10639 | 5-Bromo-2-nitro-N-phenylaniline 95% | 6311-47-3 | 1G | $165 | 2026-05-27 | Buy |
5-bromo-2-nitro-N-phenyl-aniline Chemical Properties, Uses, Production
Synthesis
321-23-3
62-53-3
6311-47-3
General procedure for the synthesis of 5-bromo-2-nitro-N-phenyl-aniline from 2-fluoro-4-bromonitrobenzene and aniline: 4-bromo-2-fluoronitrobenzene (5.6 g, 20.9 mmol) and aniline (2.5 g, 72.2 mmol) were dissolved in 50 mL of anhydrous N-methylpyrrolidone (NMP). The reaction mixture was heated to 110 °C and the reaction was stirred overnight. After completion of the reaction, it was cooled to room temperature and the solvent was removed by distillation under reduced pressure. The crude product was purified by silica gel column chromatography with the eluent cyclohexane/ethyl acetate (9:1, v/v) to give an orange solid product in 92% yield (5.7 g). The 1H-NMR (400 MHz, CD2Cl2) data of the product were as follows: δ= 9.48 (s, 1H), 8.06 (d, 1H), 7.46 (t, 2H), 7.30 (t, 4H), 6.89 (d, 1H).
References
[1] Patent: WO2015/14944, 2015, A1. Location in patent: Page/Page column 115; 116
[2] Patent: WO2015/150203, 2015, A1. Location in patent: Page/Page column 85
[3] Patent: WO2014/100695, 2014, A1. Location in patent: Paragraph 00349
[4] Patent: US2015/30588, 2015, A1. Location in patent: Page/Page column 71
[5] Patent: US9295673, 2016, B2. Location in patent: Page/Page column 351; 352
5-bromo-2-nitro-N-phenyl-aniline Preparation Products And Raw materials
5-bromo-2-nitro-N-phenyl-aniline Suppliers
| Supplier | Tel | Country | ProdList | Advantage | |
|---|---|---|---|---|---|
| Nanbu County Chengxin Technology Co., Ltd. | 0838-5675166 15883665058 | nbcxkj@126.com | China | 956 | 55 |
| Hangzhou Sage Chemical Co., Ltd. | +86057186818502 13588463833 | info@sagechem.com | China | 10265 | 58 |
| Shanghai Keepontech Co.,Ltd | 021-54849683 13601642561 | sales@keepontech.com | China | 998 | 59 |
| Shanghai Yolne Chemical Co., Ltd. | 021-62960152 | 934678158@qq.com | China | 9886 | 55 |
| Mashilabs (Shanghai) Co.,Ltd. | 19916721580 | mafarm@126.com | China | 4534 | 58 |
| Shanghai HuanChuan Industry Co.,Ltd. | 021-61478794 | sales@hcshhai.com | China | 9781 | 50 |
| Zhengzhou Guancheng Laboratory equipment Sales | 0371-88888888 qq272369594;2159423853qq | 2723695949@qq.com | China | 4990 | 50 |
| Chengdu jingzhihuacheng Chemical Technology Co., Ltd. | 028-028-37664989 15900794981 | jingzhichem@163.com | China | 536 | 55 |
| Amadis Chemical Company Limited | 571-89925085 | sales@amadischem.com | China | 131885 | 58 |
| Aikon International Limited | 025-66061636 19370895928 | qqyang@aikonchem.com | China | 15810 | 58 |
