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ChemicalBook >> CAS DataBase List >>N-(4-Chlorophenyl)-2-nitrobenzenamine

N-(4-Chlorophenyl)-2-nitrobenzenamine

N-(4-Chlorophenyl)-2-nitrobenzenamine Structure
N-(4-Chlorophenyl)-2-nitrobenzenamine structure
CAS No.
23008-56-2
Chemical Name:
N-(4-Chlorophenyl)-2-nitrobenzenamine
Synonyms
N-(4-chlorophenyl)-2-nitroaniline;C.I.10336;Disperse Yellow 22;TIMTEC-BB SBB003165;C.I.Disperse Yellow 22;SRA Fast Golden Yellow XII;2-NITRO-4'-CHLORDIPHENYLAMIN;4'-CHLORO-2-NITRODIPHENYLAMINE;4-Chloro-2'-nitrodiphenylamine;2-NITRO-4'-CHLORO DIPHENYLAMINE
CBNumber:
CB0748894
Molecular Formula:
C12H9ClN2O2
Molecular Weight:
248.67
MDL Number:
MFCD02683544
MOL File:
23008-56-2.mol
MSDS File:
SDS
Last updated:2026-09-12 18:48:28
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N-(4-Chlorophenyl)-2-nitrobenzenamine Properties

Melting point 145-148 °C(lit.)
Boiling point 377.2±27.0 °C(Predicted)
Density 1.387±0.06 g/cm3(Predicted)
storage temp. 2-8°C(protect from light)
pka -3.90±0.40(Predicted)
Appearance Brown to dark brown Solid
InChI InChI=1S/C12H9ClN2O2/c13-9-5-7-10(8-6-9)14-11-3-1-2-4-12(11)15(16)17/h1-8,14H
InChIKey RCLKXSIRDRWUGX-UHFFFAOYSA-N
SMILES C1(NC2=CC=C(Cl)C=C2)=CC=CC=C1[N+]([O-])=O
CAS DataBase Reference 23008-56-2(CAS DataBase Reference)

SAFETY

Risk and Safety Statements

Symbol(GHS)  Exclamation Mark (GHS07)
GHS07
Signal word  Warning
Hazard statements  H315-H319-H335
Precautionary statements  P261-P305+P351+P338
Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-36
WGK Germany  3
Hazard Note  Irritant
HS Code  2921490090

N-(4-Chlorophenyl)-2-nitrobenzenamine price More Price(46)

Manufacturer Product number Product description CAS number Packaging Price Updated Buy
Apolloscientific OR4253 4'-Chloro-2-nitrodiphenylamine 98% 23008-56-2 1g $21 2026-06-04 Buy
Apolloscientific OR4253 4'-Chloro-2-nitrodiphenylamine 98% 23008-56-2 5g $24 2026-06-04 Buy
Apolloscientific OR4253 4'-Chloro-2-nitrodiphenylamine 98% 23008-56-2 25g $49 2026-06-04 Buy
Apolloscientific OR4253 4'-Chloro-2-nitrodiphenylamine 98% 23008-56-2 100g $81 2026-06-04 Buy
Apolloscientific OR4253 4'-Chloro-2-nitrodiphenylamine 98% 23008-56-2 500g $349 2026-06-04 Buy
Product number Packaging Price Buy
OR4253 1g $21 Buy
OR4253 5g $24 Buy
OR4253 25g $49 Buy
OR4253 100g $81 Buy
OR4253 500g $349 Buy

N-(4-Chlorophenyl)-2-nitrobenzenamine Chemical Properties, Uses, Production

Uses

2-Nitro-4''-chlorodiphenylamine is a reagent used in the synthesis of novel 4-phenoxyquinoline derivatives as c-Met kinase inhibitors. Intermediate for Clofazimine.

Preparation

4-Chlorobenzenamine and 1-Chloro-2-nitrobenzenecondensation

Synthesis

4-Chloroaniline

106-47-8

1-Fluoro-2-nitrobenzene

1493-27-2

N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE

23008-56-2

GENERAL METHOD: Suspend NaH (75 mmol) in DMF (60 mL) at 0°C and slowly add 4-chloroaniline (50 mmol). After stirring for 30 min at 0°C, a solution of 1-fluoro-2-nitrobenzene (60 mmol) in DMF (30 mL) was added dropwise. The reaction mixture was gradually warmed to room temperature and stirred continuously for 16 hours. Upon completion of the reaction, the mixture was carefully poured into a stirred saturated NH4Cl solution (500 mL) and the precipitate was collected by filtration. The filter cake was washed with water and purified by recrystallization from methanol to give the target product N-(4-chlorophenyl)-2-nitroaniline (15h). The product was an orange solid with a yield of 72.3% and a melting point of 135.1-137.0 °C. 1H NMR (400 MHz, DMSO-d6) δ 9.31 (s, 1H), 8.12 (d, J = 8.0 Hz, 1H), 7.53 (t, J = 7.6 Hz, 1H), 7.44 (d, J = 8.8 Hz, 2H), 7.34 (d, J = 8.8 Hz, 2H), 7.22 (d, J = 8.4 Hz, 1H), 6.93 (t, J = 7.6 Hz, 1H).MS (ESI) m/z (%): 247.2 [M-H]-.

Properties and Applications

Brilliant yellow

StandardVinegar fiber Ironing Fastness Light Fastness Persperation Fastness Washing Fastness
Fading Stain Fading Stain Fading Stain
ISO 7 4 4 3 2

References

[1] Patent: CN106916069, 2017, A. Location in patent: Paragraph 0016; 0017; 0018; 0019; 0020; 0021; 0022-0024
[2] Organic Process Research and Development, 2016, vol. 20, # 2, p. 452 - 464
[3] Molecules, 2012, vol. 17, # 4, p. 4545 - 4559
[4] Synlett, 2003, # 4, p. 564 - 566
[5] Bioorganic and Medicinal Chemistry, 2017, vol. 25, # 16, p. 4475 - 4486

N-(4-Chlorophenyl)-2-nitrobenzenamine synthesis

106-47-8
1493-27-2
23008-56-2
Synthesis of N-(4-Chlorophenyl)-2-nitrobenzenamine from 4-Chloroaniline and 1-Fluoro-2-nitrobenzene

N-(4-Chlorophenyl)-2-nitrobenzenamine Preparation Products And Raw materials

Raw materials

2-Nitrochlorobenzene 4-Chloroaniline 1-Fluoro-2-nitrobenzene Sodium hydride N,N-Dimethylformamide

Preparation Products

N1-(4-Chlorophenyl)benzene-1,2-diamine

N-(4-Chlorophenyl)-2-nitrobenzenamine Suppliers

Global Suppliers ( 108)
Supplier Tel Email Country ProdList Advantage
Hangzhou Copiore Chemical Co., Ltd. 17300981287 13757145729 sales@copiore.com China 291 58
Shandong RuiYue Biotechnology Co., Ltd. 0531-88581623 18805314509 1456922171@126.com China 63 50
J & K SCIENTIFIC LTD. 18210857532 18210857532 jkinfo@jkchemical.com China 96815 76
JinYan Chemicals(ShangHai) Co.,Ltd. 13817811078 sales@jingyan-chemical.com China 9963 60
Shandong Xiya Chemical Co., Ltd 13355009207 13355009207 3007715519@qq.com China 18722 57
Nanjing King-pharm Co.,LTD. 025-58748998 18951874644 elsa.cheng@chemsigma.com China 137 65
Beijing Taiya Jie Technology Development Co., Ltd. 021-33690831-8001 13552411790;18616022633 postmaster@tyjchem.cn China 1541 55
Shanghai Meishui Chemical Technology Co., Ltd 021-60549325 18616193163 China 4518 56
Bide Pharmatech Ltd. 400-164-7117 18317119277 product02@bidepharm.com China 40000 60
Chengdu HuaXia Chemical Reagent Co. Ltd 400-1166-196 13458535857 cdhxsj@163.com China 13323 58
Supplier Advantage
Hangzhou Copiore Chemical Co., Ltd. 58
Shandong RuiYue Biotechnology Co., Ltd. 50
J & K SCIENTIFIC LTD. 76
JinYan Chemicals(ShangHai) Co.,Ltd. 60
Shandong Xiya Chemical Co., Ltd 57
Nanjing King-pharm Co.,LTD. 65
Beijing Taiya Jie Technology Development Co., Ltd. 55
Shanghai Meishui Chemical Technology Co., Ltd 56
Bide Pharmatech Ltd. 60
Chengdu HuaXia Chemical Reagent Co. Ltd 58

View Latest Price from N-(4-Chlorophenyl)-2-nitrobenzenamine manufacturers

Image Update time Product Price Min. Order Purity Supply Ability Manufacturer
N-(4-chlorophenyl)-2-nitroaniline pictures 2022-01-15 N-(4-chlorophenyl)-2-nitroaniline
23008-56-2
 1KG 98.1% 100 tons Honest Joy Holdings Limited
N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE pictures 2021-08-12 N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE
23008-56-2
 $10.00-15.00 1KG 99%+ HPLC Zhuozhou Wenxi import and Export Co., Ltd
N-(4-CHLOROPHENYL)-2-NITROBENZENAMINEE pictures 2019-09-04 N-(4-CHLOROPHENYL)-2-NITROBENZENAMINEE
23008-56-2
 $1.00 1KG 97%-98% 200KG Career Henan Chemical Co

N-(4-Chlorophenyl)-2-nitrobenzenamine Spectrum

N-(4-CHLOROPHENYL)-2-NITROBENZENAMINE(23008-56-2)1HNMR

23008-56-2 (N-(4-Chlorophenyl)-2-nitrobenzenamine) Related Search:

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N1-(4-Chlorophenyl)benzene-1,2-diamine

1of4

2-NITRO-4'-CHLORO DIPHENYLAMINE 2-NITRO-4'-CHLORDIPHENYLAMIN N-(4-CHLOROPHENYL)-2-NITROBENZENAMINEE 4'-CHLORO-2-NITRODIPHENYLAMINE 4-Chloro-N-(2-nitrophenyl)aniline C.I.10336 C.I.Disperse Yellow 22 SRA Fast Golden Yellow XII (4-chlorophenyl)-(2-nitrophenyl)amine TIMTEC-BB SBB003165 N-(4-chlorophenyl)-2-nitroaniline 4'-Chloro-2-nitrodiphenylamine98% 2-(4-Chlorophenylamino)-1-nitrobenzene N-(4-Chloropheny)-2-NitrobenzenamineI Benzenamine, N-(4-chlorophenyl)-2-nitro- C.I.Disperse Yellow 22:C.I.1033 Disperse Yellow 22 4-Chloro-2'-nitrodiphenylamine 2-Nitro-4′-chlorodiphenylamine, CAS 23008-56-2 N-(4-chlorophenyl)-2-nitroaniline 95% N-(4-Chlorophenyl)-2-nitrobenzenamine 23008-56-2 ClC6H4NHC6H4NO2